Simplified analytical methodology for glucosinolate hydrolysis products: A miniaturized extraction technique and multivariate optimization

Autores
Fusari Gómez, Cecilia Mara; Ramirez, Daniela Andrea; Camargo, Alejandra Beatriz
Año de publicación
2019
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
Miniaturized extraction techniques are one of the most significant advances in analytical chemistry today. Nowadays there is a growing tendency among food researchers to develop simpler and robust methodologies that allow the determination of multiple analytes in different samples. Based on this concept, the aim of this work was to develop an optimized and validated methodology for the determination of four isothiocyanates (ITCs) and one indole: allyl ITC, erucin, sulforaphane, phenyl ITC and indole-3-carbinol present in Brassicaceae vegetables. Experimental design and multivariate analysis were the statistical tools used during the process. The dispersive liquid-liquid microextraction (DLLME) technique developed in this work was successfully applied to the analysis of nine Brassicaceae species.
Fil: Fusari Gómez, Cecilia Mara. Universidad Nacional de Cuyo. Facultad de Ciencias Agrarias; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mendoza. Instituto de Biología Agrícola de Mendoza. Universidad Nacional de Cuyo. Facultad de Ciencias Agrarias. Instituto de Biología Agrícola de Mendoza; Argentina
Fil: Ramirez, Daniela Andrea. Universidad Nacional de Cuyo. Facultad de Ciencias Agrarias; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mendoza. Instituto de Biología Agrícola de Mendoza. Universidad Nacional de Cuyo. Facultad de Ciencias Agrarias. Instituto de Biología Agrícola de Mendoza; Argentina
Fil: Camargo, Alejandra Beatriz. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mendoza. Instituto de Biología Agrícola de Mendoza. Universidad Nacional de Cuyo. Facultad de Ciencias Agrarias. Instituto de Biología Agrícola de Mendoza; Argentina. Universidad Nacional de Cuyo. Facultad de Ciencias Exactas y Naturales; Argentina
Materia
Brassicaceae,
Isothiocyanates
DLLME,
Experimental Design
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/92450
Acceder
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oai_identifier_str oai:ri.conicet.gov.ar:11336/92450
network_acronym_str CONICETDig
repository_id_str 3498
network_name_str CONICET Digital (CONICET)
spelling Simplified analytical methodology for glucosinolate hydrolysis products: A miniaturized extraction technique and multivariate optimizationFusari Gómez, Cecilia MaraRamirez, Daniela AndreaCamargo, Alejandra BeatrizBrassicaceae,IsothiocyanatesDLLME,Experimental Designhttps://purl.org/becyt/ford/1.4https://purl.org/becyt/ford/1Miniaturized extraction techniques are one of the most significant advances in analytical chemistry today. Nowadays there is a growing tendency among food researchers to develop simpler and robust methodologies that allow the determination of multiple analytes in different samples. Based on this concept, the aim of this work was to develop an optimized and validated methodology for the determination of four isothiocyanates (ITCs) and one indole: allyl ITC, erucin, sulforaphane, phenyl ITC and indole-3-carbinol present in Brassicaceae vegetables. Experimental design and multivariate analysis were the statistical tools used during the process. The dispersive liquid-liquid microextraction (DLLME) technique developed in this work was successfully applied to the analysis of nine Brassicaceae species.Fil: Fusari Gómez, Cecilia Mara. Universidad Nacional de Cuyo. Facultad de Ciencias Agrarias; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mendoza. Instituto de Biología Agrícola de Mendoza. Universidad Nacional de Cuyo. Facultad de Ciencias Agrarias. Instituto de Biología Agrícola de Mendoza; ArgentinaFil: Ramirez, Daniela Andrea. Universidad Nacional de Cuyo. Facultad de Ciencias Agrarias; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mendoza. Instituto de Biología Agrícola de Mendoza. Universidad Nacional de Cuyo. Facultad de Ciencias Agrarias. Instituto de Biología Agrícola de Mendoza; ArgentinaFil: Camargo, Alejandra Beatriz. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mendoza. Instituto de Biología Agrícola de Mendoza. Universidad Nacional de Cuyo. Facultad de Ciencias Agrarias. Instituto de Biología Agrícola de Mendoza; Argentina. Universidad Nacional de Cuyo. Facultad de Ciencias Exactas y Naturales; ArgentinaRoyal Society of Chemistry2019-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/92450Fusari Gómez, Cecilia Mara; Ramirez, Daniela Andrea; Camargo, Alejandra Beatriz; Simplified analytical methodology for glucosinolate hydrolysis products: A miniaturized extraction technique and multivariate optimization; Royal Society of Chemistry; Analytical Methods; 11; 3; 1-2019; 309-3161759-9679CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/doi/10.1039/c8ay02442ainfo:eu-repo/semantics/altIdentifier/url/https://pubs.rsc.org/en/content/articlelanding/2019/AY/C8AY02442A#!divAbstractinfo:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-sa/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-09-29T09:37:45Zoai:ri.conicet.gov.ar:11336/92450instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-09-29 09:37:45.607CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Simplified analytical methodology for glucosinolate hydrolysis products: A miniaturized extraction technique and multivariate optimization
title Simplified analytical methodology for glucosinolate hydrolysis products: A miniaturized extraction technique and multivariate optimization
spellingShingle Simplified analytical methodology for glucosinolate hydrolysis products: A miniaturized extraction technique and multivariate optimization
Fusari Gómez, Cecilia Mara
Brassicaceae,
Isothiocyanates
DLLME,
Experimental Design
title_short Simplified analytical methodology for glucosinolate hydrolysis products: A miniaturized extraction technique and multivariate optimization
title_full Simplified analytical methodology for glucosinolate hydrolysis products: A miniaturized extraction technique and multivariate optimization
title_fullStr Simplified analytical methodology for glucosinolate hydrolysis products: A miniaturized extraction technique and multivariate optimization
title_full_unstemmed Simplified analytical methodology for glucosinolate hydrolysis products: A miniaturized extraction technique and multivariate optimization
title_sort Simplified analytical methodology for glucosinolate hydrolysis products: A miniaturized extraction technique and multivariate optimization
dc.creator.none.fl_str_mv Fusari Gómez, Cecilia Mara
Ramirez, Daniela Andrea
Camargo, Alejandra Beatriz
author Fusari Gómez, Cecilia Mara
author_facet Fusari Gómez, Cecilia Mara
Ramirez, Daniela Andrea
Camargo, Alejandra Beatriz
author_role author
author2 Ramirez, Daniela Andrea
Camargo, Alejandra Beatriz
author2_role author
author
dc.subject.none.fl_str_mv Brassicaceae,
Isothiocyanates
DLLME,
Experimental Design
topic Brassicaceae,
Isothiocyanates
DLLME,
Experimental Design
purl_subject.fl_str_mv https://purl.org/becyt/ford/1.4
https://purl.org/becyt/ford/1
dc.description.none.fl_txt_mv Miniaturized extraction techniques are one of the most significant advances in analytical chemistry today. Nowadays there is a growing tendency among food researchers to develop simpler and robust methodologies that allow the determination of multiple analytes in different samples. Based on this concept, the aim of this work was to develop an optimized and validated methodology for the determination of four isothiocyanates (ITCs) and one indole: allyl ITC, erucin, sulforaphane, phenyl ITC and indole-3-carbinol present in Brassicaceae vegetables. Experimental design and multivariate analysis were the statistical tools used during the process. The dispersive liquid-liquid microextraction (DLLME) technique developed in this work was successfully applied to the analysis of nine Brassicaceae species.
Fil: Fusari Gómez, Cecilia Mara. Universidad Nacional de Cuyo. Facultad de Ciencias Agrarias; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mendoza. Instituto de Biología Agrícola de Mendoza. Universidad Nacional de Cuyo. Facultad de Ciencias Agrarias. Instituto de Biología Agrícola de Mendoza; Argentina
Fil: Ramirez, Daniela Andrea. Universidad Nacional de Cuyo. Facultad de Ciencias Agrarias; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mendoza. Instituto de Biología Agrícola de Mendoza. Universidad Nacional de Cuyo. Facultad de Ciencias Agrarias. Instituto de Biología Agrícola de Mendoza; Argentina
Fil: Camargo, Alejandra Beatriz. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mendoza. Instituto de Biología Agrícola de Mendoza. Universidad Nacional de Cuyo. Facultad de Ciencias Agrarias. Instituto de Biología Agrícola de Mendoza; Argentina. Universidad Nacional de Cuyo. Facultad de Ciencias Exactas y Naturales; Argentina
description Miniaturized extraction techniques are one of the most significant advances in analytical chemistry today. Nowadays there is a growing tendency among food researchers to develop simpler and robust methodologies that allow the determination of multiple analytes in different samples. Based on this concept, the aim of this work was to develop an optimized and validated methodology for the determination of four isothiocyanates (ITCs) and one indole: allyl ITC, erucin, sulforaphane, phenyl ITC and indole-3-carbinol present in Brassicaceae vegetables. Experimental design and multivariate analysis were the statistical tools used during the process. The dispersive liquid-liquid microextraction (DLLME) technique developed in this work was successfully applied to the analysis of nine Brassicaceae species.
publishDate 2019
dc.date.none.fl_str_mv 2019-01
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/92450
Fusari Gómez, Cecilia Mara; Ramirez, Daniela Andrea; Camargo, Alejandra Beatriz; Simplified analytical methodology for glucosinolate hydrolysis products: A miniaturized extraction technique and multivariate optimization; Royal Society of Chemistry; Analytical Methods; 11; 3; 1-2019; 309-316
1759-9679
CONICET Digital
CONICET
url http://hdl.handle.net/11336/92450
identifier_str_mv Fusari Gómez, Cecilia Mara; Ramirez, Daniela Andrea; Camargo, Alejandra Beatriz; Simplified analytical methodology for glucosinolate hydrolysis products: A miniaturized extraction technique and multivariate optimization; Royal Society of Chemistry; Analytical Methods; 11; 3; 1-2019; 309-316
1759-9679
CONICET Digital
CONICET
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/doi/10.1039/c8ay02442a
info:eu-repo/semantics/altIdentifier/url/https://pubs.rsc.org/en/content/articlelanding/2019/AY/C8AY02442A#!divAbstract
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
dc.publisher.none.fl_str_mv Royal Society of Chemistry
publisher.none.fl_str_mv Royal Society of Chemistry
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
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score 13.070432

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