Processing of porous mullite ceramics using novel routes by starch consolidation casting

Autores
Talou, Mariano Hernán; Camerucci, Maria Andrea
Año de publicación
2015
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
In this article, the development and characterization of porous mullite bodies prepared using two novel forming routes with native starches were studied with the aim of developing bodies without deformation and with homogeneous porous microstructures. Mullite-starch suspensions specific for each route were prepared by mixing and characterized by measuring viscosity. Mullite green bodies were fabricated by heating the suspensions in metallic molds and by burning out the starch, while final porous materials were obtained by sintering at different temperatures. Bodies obtained before and after the burning-out process, and sintered disks, were characterized with porosity measurements and microstructural analysis by SEM. The phases generated after the sintering process were determined by XRD, and pore size distributions were studied by Hg-porosimetry. The obtained results showed that the use of both routes allowed the shaping of homogeneous mullite bodies without causing cracks or deformations and the consequent development of controlled porous mullite microstructures.
Fil: Talou, Mariano Hernán. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Fil: Camerucci, Maria Andrea. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Materia
Microstructure
Mullite
Porous Ceramics
Starch Consolidation Casting Method
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/50610

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network_name_str CONICET Digital (CONICET)
spelling Processing of porous mullite ceramics using novel routes by starch consolidation castingTalou, Mariano HernánCamerucci, Maria AndreaMicrostructureMullitePorous CeramicsStarch Consolidation Casting Methodhttps://purl.org/becyt/ford/2.5https://purl.org/becyt/ford/2In this article, the development and characterization of porous mullite bodies prepared using two novel forming routes with native starches were studied with the aim of developing bodies without deformation and with homogeneous porous microstructures. Mullite-starch suspensions specific for each route were prepared by mixing and characterized by measuring viscosity. Mullite green bodies were fabricated by heating the suspensions in metallic molds and by burning out the starch, while final porous materials were obtained by sintering at different temperatures. Bodies obtained before and after the burning-out process, and sintered disks, were characterized with porosity measurements and microstructural analysis by SEM. The phases generated after the sintering process were determined by XRD, and pore size distributions were studied by Hg-porosimetry. The obtained results showed that the use of both routes allowed the shaping of homogeneous mullite bodies without causing cracks or deformations and the consequent development of controlled porous mullite microstructures.Fil: Talou, Mariano Hernán. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; ArgentinaFil: Camerucci, Maria Andrea. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; ArgentinaElsevier2015-03info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/50610Talou, Mariano Hernán; Camerucci, Maria Andrea; Processing of porous mullite ceramics using novel routes by starch consolidation casting; Elsevier; Journal of the European Ceramic Society; 35; 3; 3-2015; 1021-10300955-2219CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/doi/10.1016/j.jeurceramsoc.2014.10.011info:eu-repo/semantics/altIdentifier/url/https://www.sciencedirect.com/science/article/pii/S0955221914005469info:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-nd/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-09-29T09:58:01Zoai:ri.conicet.gov.ar:11336/50610instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-09-29 09:58:02.178CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Processing of porous mullite ceramics using novel routes by starch consolidation casting
title Processing of porous mullite ceramics using novel routes by starch consolidation casting
spellingShingle Processing of porous mullite ceramics using novel routes by starch consolidation casting
Talou, Mariano Hernán
Microstructure
Mullite
Porous Ceramics
Starch Consolidation Casting Method
title_short Processing of porous mullite ceramics using novel routes by starch consolidation casting
title_full Processing of porous mullite ceramics using novel routes by starch consolidation casting
title_fullStr Processing of porous mullite ceramics using novel routes by starch consolidation casting
title_full_unstemmed Processing of porous mullite ceramics using novel routes by starch consolidation casting
title_sort Processing of porous mullite ceramics using novel routes by starch consolidation casting
dc.creator.none.fl_str_mv Talou, Mariano Hernán
Camerucci, Maria Andrea
author Talou, Mariano Hernán
author_facet Talou, Mariano Hernán
Camerucci, Maria Andrea
author_role author
author2 Camerucci, Maria Andrea
author2_role author
dc.subject.none.fl_str_mv Microstructure
Mullite
Porous Ceramics
Starch Consolidation Casting Method
topic Microstructure
Mullite
Porous Ceramics
Starch Consolidation Casting Method
purl_subject.fl_str_mv https://purl.org/becyt/ford/2.5
https://purl.org/becyt/ford/2
dc.description.none.fl_txt_mv In this article, the development and characterization of porous mullite bodies prepared using two novel forming routes with native starches were studied with the aim of developing bodies without deformation and with homogeneous porous microstructures. Mullite-starch suspensions specific for each route were prepared by mixing and characterized by measuring viscosity. Mullite green bodies were fabricated by heating the suspensions in metallic molds and by burning out the starch, while final porous materials were obtained by sintering at different temperatures. Bodies obtained before and after the burning-out process, and sintered disks, were characterized with porosity measurements and microstructural analysis by SEM. The phases generated after the sintering process were determined by XRD, and pore size distributions were studied by Hg-porosimetry. The obtained results showed that the use of both routes allowed the shaping of homogeneous mullite bodies without causing cracks or deformations and the consequent development of controlled porous mullite microstructures.
Fil: Talou, Mariano Hernán. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Fil: Camerucci, Maria Andrea. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
description In this article, the development and characterization of porous mullite bodies prepared using two novel forming routes with native starches were studied with the aim of developing bodies without deformation and with homogeneous porous microstructures. Mullite-starch suspensions specific for each route were prepared by mixing and characterized by measuring viscosity. Mullite green bodies were fabricated by heating the suspensions in metallic molds and by burning out the starch, while final porous materials were obtained by sintering at different temperatures. Bodies obtained before and after the burning-out process, and sintered disks, were characterized with porosity measurements and microstructural analysis by SEM. The phases generated after the sintering process were determined by XRD, and pore size distributions were studied by Hg-porosimetry. The obtained results showed that the use of both routes allowed the shaping of homogeneous mullite bodies without causing cracks or deformations and the consequent development of controlled porous mullite microstructures.
publishDate 2015
dc.date.none.fl_str_mv 2015-03
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/50610
Talou, Mariano Hernán; Camerucci, Maria Andrea; Processing of porous mullite ceramics using novel routes by starch consolidation casting; Elsevier; Journal of the European Ceramic Society; 35; 3; 3-2015; 1021-1030
0955-2219
CONICET Digital
CONICET
url http://hdl.handle.net/11336/50610
identifier_str_mv Talou, Mariano Hernán; Camerucci, Maria Andrea; Processing of porous mullite ceramics using novel routes by starch consolidation casting; Elsevier; Journal of the European Ceramic Society; 35; 3; 3-2015; 1021-1030
0955-2219
CONICET Digital
CONICET
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/doi/10.1016/j.jeurceramsoc.2014.10.011
info:eu-repo/semantics/altIdentifier/url/https://www.sciencedirect.com/science/article/pii/S0955221914005469
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
dc.publisher.none.fl_str_mv Elsevier
publisher.none.fl_str_mv Elsevier
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
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