Effect of loading strain rate on nano-indentation response of an aerospace grade epoxy polymer

Autores
Fasce, Laura Alejandra; Sanchez Fellay, Lucas; Frontini, Patricia Maria
Año de publicación
2023
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
Depth sensing indentation holds the promise of local mechanical properties determination. However, the number of studies for materials that exhibit time dependent and hydrostatic pressure dependent behavior is still scarce. This paper aims to understand the effect of loading strain rate on the nanoindentation response of an aerospace epoxy resin by combining physical measurements and numerical simulations. Physical nanoindentation tests were carried out using a Berkovich indenter at different constant loading strain rates (0.01 to 1.25 s-1). It was observed that as the loading strain rate increases, the penetration displacement at which the target load is reached decreases while the maximum displacement attained at the end of the load-hold period increases. To get insight into the phenomenon, indentation response was numerically simulated by finite element analysis. The polymer behavior was described by a nine-parameter elastic-viscoplastic constitutive model (EVP-9). Constitutive parameters were calibrated from uniaxial tensile and compression experimental data. Simulations agreed reasonably well with physical experiments being able to reproduce the loading strain rate effect observed in physical nanoindentation tests.
Fil: Fasce, Laura Alejandra. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Fil: Sanchez Fellay, Lucas. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Fil: Frontini, Patricia Maria. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Materia
THERMOSETTING RESINS
MATERIAL TESTING
NANOINDENTATION
MECHANICAL PROPERTIES
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/250075

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spelling Effect of loading strain rate on nano-indentation response of an aerospace grade epoxy polymerFasce, Laura AlejandraSanchez Fellay, LucasFrontini, Patricia MariaTHERMOSETTING RESINSMATERIAL TESTINGNANOINDENTATIONMECHANICAL PROPERTIEShttps://purl.org/becyt/ford/2.5https://purl.org/becyt/ford/2Depth sensing indentation holds the promise of local mechanical properties determination. However, the number of studies for materials that exhibit time dependent and hydrostatic pressure dependent behavior is still scarce. This paper aims to understand the effect of loading strain rate on the nanoindentation response of an aerospace epoxy resin by combining physical measurements and numerical simulations. Physical nanoindentation tests were carried out using a Berkovich indenter at different constant loading strain rates (0.01 to 1.25 s-1). It was observed that as the loading strain rate increases, the penetration displacement at which the target load is reached decreases while the maximum displacement attained at the end of the load-hold period increases. To get insight into the phenomenon, indentation response was numerically simulated by finite element analysis. The polymer behavior was described by a nine-parameter elastic-viscoplastic constitutive model (EVP-9). Constitutive parameters were calibrated from uniaxial tensile and compression experimental data. Simulations agreed reasonably well with physical experiments being able to reproduce the loading strain rate effect observed in physical nanoindentation tests.Fil: Fasce, Laura Alejandra. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; ArgentinaFil: Sanchez Fellay, Lucas. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; ArgentinaFil: Frontini, Patricia Maria. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; ArgentinaBudapest University of Technology and Economics2023-04info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/250075Fasce, Laura Alejandra; Sanchez Fellay, Lucas; Frontini, Patricia Maria; Effect of loading strain rate on nano-indentation response of an aerospace grade epoxy polymer; Budapest University of Technology and Economics; Express Polymer Letters; 17; 6; 4-2023; 647-6591788-618XCONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/doi/10.3144/expresspolymlett.2023.47info:eu-repo/semantics/altIdentifier/url/http://www.expresspolymlett.com/search.phpinfo:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-sa/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-11-12T09:36:21Zoai:ri.conicet.gov.ar:11336/250075instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-11-12 09:36:21.688CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Effect of loading strain rate on nano-indentation response of an aerospace grade epoxy polymer
title Effect of loading strain rate on nano-indentation response of an aerospace grade epoxy polymer
spellingShingle Effect of loading strain rate on nano-indentation response of an aerospace grade epoxy polymer
Fasce, Laura Alejandra
THERMOSETTING RESINS
MATERIAL TESTING
NANOINDENTATION
MECHANICAL PROPERTIES
title_short Effect of loading strain rate on nano-indentation response of an aerospace grade epoxy polymer
title_full Effect of loading strain rate on nano-indentation response of an aerospace grade epoxy polymer
title_fullStr Effect of loading strain rate on nano-indentation response of an aerospace grade epoxy polymer
title_full_unstemmed Effect of loading strain rate on nano-indentation response of an aerospace grade epoxy polymer
title_sort Effect of loading strain rate on nano-indentation response of an aerospace grade epoxy polymer
dc.creator.none.fl_str_mv Fasce, Laura Alejandra
Sanchez Fellay, Lucas
Frontini, Patricia Maria
author Fasce, Laura Alejandra
author_facet Fasce, Laura Alejandra
Sanchez Fellay, Lucas
Frontini, Patricia Maria
author_role author
author2 Sanchez Fellay, Lucas
Frontini, Patricia Maria
author2_role author
author
dc.subject.none.fl_str_mv THERMOSETTING RESINS
MATERIAL TESTING
NANOINDENTATION
MECHANICAL PROPERTIES
topic THERMOSETTING RESINS
MATERIAL TESTING
NANOINDENTATION
MECHANICAL PROPERTIES
purl_subject.fl_str_mv https://purl.org/becyt/ford/2.5
https://purl.org/becyt/ford/2
dc.description.none.fl_txt_mv Depth sensing indentation holds the promise of local mechanical properties determination. However, the number of studies for materials that exhibit time dependent and hydrostatic pressure dependent behavior is still scarce. This paper aims to understand the effect of loading strain rate on the nanoindentation response of an aerospace epoxy resin by combining physical measurements and numerical simulations. Physical nanoindentation tests were carried out using a Berkovich indenter at different constant loading strain rates (0.01 to 1.25 s-1). It was observed that as the loading strain rate increases, the penetration displacement at which the target load is reached decreases while the maximum displacement attained at the end of the load-hold period increases. To get insight into the phenomenon, indentation response was numerically simulated by finite element analysis. The polymer behavior was described by a nine-parameter elastic-viscoplastic constitutive model (EVP-9). Constitutive parameters were calibrated from uniaxial tensile and compression experimental data. Simulations agreed reasonably well with physical experiments being able to reproduce the loading strain rate effect observed in physical nanoindentation tests.
Fil: Fasce, Laura Alejandra. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Fil: Sanchez Fellay, Lucas. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Fil: Frontini, Patricia Maria. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
description Depth sensing indentation holds the promise of local mechanical properties determination. However, the number of studies for materials that exhibit time dependent and hydrostatic pressure dependent behavior is still scarce. This paper aims to understand the effect of loading strain rate on the nanoindentation response of an aerospace epoxy resin by combining physical measurements and numerical simulations. Physical nanoindentation tests were carried out using a Berkovich indenter at different constant loading strain rates (0.01 to 1.25 s-1). It was observed that as the loading strain rate increases, the penetration displacement at which the target load is reached decreases while the maximum displacement attained at the end of the load-hold period increases. To get insight into the phenomenon, indentation response was numerically simulated by finite element analysis. The polymer behavior was described by a nine-parameter elastic-viscoplastic constitutive model (EVP-9). Constitutive parameters were calibrated from uniaxial tensile and compression experimental data. Simulations agreed reasonably well with physical experiments being able to reproduce the loading strain rate effect observed in physical nanoindentation tests.
publishDate 2023
dc.date.none.fl_str_mv 2023-04
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/250075
Fasce, Laura Alejandra; Sanchez Fellay, Lucas; Frontini, Patricia Maria; Effect of loading strain rate on nano-indentation response of an aerospace grade epoxy polymer; Budapest University of Technology and Economics; Express Polymer Letters; 17; 6; 4-2023; 647-659
1788-618X
CONICET Digital
CONICET
url http://hdl.handle.net/11336/250075
identifier_str_mv Fasce, Laura Alejandra; Sanchez Fellay, Lucas; Frontini, Patricia Maria; Effect of loading strain rate on nano-indentation response of an aerospace grade epoxy polymer; Budapest University of Technology and Economics; Express Polymer Letters; 17; 6; 4-2023; 647-659
1788-618X
CONICET Digital
CONICET
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/doi/10.3144/expresspolymlett.2023.47
info:eu-repo/semantics/altIdentifier/url/http://www.expresspolymlett.com/search.php
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
application/pdf
dc.publisher.none.fl_str_mv Budapest University of Technology and Economics
publisher.none.fl_str_mv Budapest University of Technology and Economics
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
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