Mechanical characterization of nano-reinforced silica based sol-gel hybrid coatings on AISI 316L stainless steel using nanoindentation techniques

Autores
Ballarre, Josefina; Jimenez Pique, Emilio; Anglada, Marc; Pellice, Sergio Antonio; Cavalieri, Ana Lia
Año de publicación
2009
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
One way to enhance the surface properties of metals used as surgical implants such as wear or protective behaviour is to use hybrid organic-inorganic sol-gel coatings. The addition of SiO2 colloidal particles to some hybrid formulation is thought to give films with bigger thickness than the coatings without particles, acting as mechanical reinforcement and to make an adequate surface to resist the extreme surgical procedures taking place in orthopaedic replacements. Coatings made by sol-gel with tetraethoxysilane (TEOS) and methyltriethoxysilane (MTES) with the addition of silica nanoparticles were applied onto surgical grade stainless steel. One of the most recent techniques used to study the mechanical properties of thin films is the instrumented indentation, known as nanoindentation, was used to evaluate elastic modulus, hardness and friction coefficient. This is a superficial technique used to measure quasi-statically the penetration of an indenter at increasing loads applied to very little volumes of material. The mechanical properties values found for the TEOS-MTES-10%SiO2 coating are smaller than for the 30% filled coating, and higher that the coating without nanoparticles. In the scratch test of the TEOS-MTES-SiO2 30 wt.% coating it can be seen that in this case the failure takes place at higher applied load than for the less silica reinforced one, indicating a much better adhesion than the system with 10% of SiO2 nanoparticles. © 2009 Elsevier B.V. All rights reserved.
Fil: Ballarre, Josefina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Fil: Jimenez Pique, Emilio. Universidad Politécnica de Catalunya; España
Fil: Anglada, Marc. Universidad Politécnica de Catalunya; España
Fil: Pellice, Sergio Antonio. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Fil: Cavalieri, Ana Lia. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Materia
Mechanical Properties
Nanoindentation
Orthopaedic Stainless Steel
Silica Coatings
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/66115
Acceder
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oai_identifier_str oai:ri.conicet.gov.ar:11336/66115
network_acronym_str CONICETDig
repository_id_str 3498
network_name_str CONICET Digital (CONICET)
spelling Mechanical characterization of nano-reinforced silica based sol-gel hybrid coatings on AISI 316L stainless steel using nanoindentation techniquesBallarre, JosefinaJimenez Pique, EmilioAnglada, MarcPellice, Sergio AntonioCavalieri, Ana LiaMechanical PropertiesNanoindentationOrthopaedic Stainless SteelSilica Coatingshttps://purl.org/becyt/ford/2.10https://purl.org/becyt/ford/2One way to enhance the surface properties of metals used as surgical implants such as wear or protective behaviour is to use hybrid organic-inorganic sol-gel coatings. The addition of SiO2 colloidal particles to some hybrid formulation is thought to give films with bigger thickness than the coatings without particles, acting as mechanical reinforcement and to make an adequate surface to resist the extreme surgical procedures taking place in orthopaedic replacements. Coatings made by sol-gel with tetraethoxysilane (TEOS) and methyltriethoxysilane (MTES) with the addition of silica nanoparticles were applied onto surgical grade stainless steel. One of the most recent techniques used to study the mechanical properties of thin films is the instrumented indentation, known as nanoindentation, was used to evaluate elastic modulus, hardness and friction coefficient. This is a superficial technique used to measure quasi-statically the penetration of an indenter at increasing loads applied to very little volumes of material. The mechanical properties values found for the TEOS-MTES-10%SiO2 coating are smaller than for the 30% filled coating, and higher that the coating without nanoparticles. In the scratch test of the TEOS-MTES-SiO2 30 wt.% coating it can be seen that in this case the failure takes place at higher applied load than for the less silica reinforced one, indicating a much better adhesion than the system with 10% of SiO2 nanoparticles. © 2009 Elsevier B.V. All rights reserved.Fil: Ballarre, Josefina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; ArgentinaFil: Jimenez Pique, Emilio. Universidad Politécnica de Catalunya; EspañaFil: Anglada, Marc. Universidad Politécnica de Catalunya; EspañaFil: Pellice, Sergio Antonio. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; ArgentinaFil: Cavalieri, Ana Lia. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; ArgentinaElsevier Science Sa2009-07info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/66115Ballarre, Josefina; Jimenez Pique, Emilio; Anglada, Marc; Pellice, Sergio Antonio; Cavalieri, Ana Lia; Mechanical characterization of nano-reinforced silica based sol-gel hybrid coatings on AISI 316L stainless steel using nanoindentation techniques; Elsevier Science Sa; Surface and Coatings Technology; 203; 20-21; 7-2009; 3325-33310257-8972CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/doi/10.1016/j.surfcoat.2009.04.014info:eu-repo/semantics/altIdentifier/url/https://linkinghub.elsevier.com/retrieve/pii/S0257897209003594info:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-sa/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-09-29T09:39:57Zoai:ri.conicet.gov.ar:11336/66115instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-09-29 09:39:57.711CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Mechanical characterization of nano-reinforced silica based sol-gel hybrid coatings on AISI 316L stainless steel using nanoindentation techniques
title Mechanical characterization of nano-reinforced silica based sol-gel hybrid coatings on AISI 316L stainless steel using nanoindentation techniques
spellingShingle Mechanical characterization of nano-reinforced silica based sol-gel hybrid coatings on AISI 316L stainless steel using nanoindentation techniques
Ballarre, Josefina
Mechanical Properties
Nanoindentation
Orthopaedic Stainless Steel
Silica Coatings
title_short Mechanical characterization of nano-reinforced silica based sol-gel hybrid coatings on AISI 316L stainless steel using nanoindentation techniques
title_full Mechanical characterization of nano-reinforced silica based sol-gel hybrid coatings on AISI 316L stainless steel using nanoindentation techniques
title_fullStr Mechanical characterization of nano-reinforced silica based sol-gel hybrid coatings on AISI 316L stainless steel using nanoindentation techniques
title_full_unstemmed Mechanical characterization of nano-reinforced silica based sol-gel hybrid coatings on AISI 316L stainless steel using nanoindentation techniques
title_sort Mechanical characterization of nano-reinforced silica based sol-gel hybrid coatings on AISI 316L stainless steel using nanoindentation techniques
dc.creator.none.fl_str_mv Ballarre, Josefina
Jimenez Pique, Emilio
Anglada, Marc
Pellice, Sergio Antonio
Cavalieri, Ana Lia
author Ballarre, Josefina
author_facet Ballarre, Josefina
Jimenez Pique, Emilio
Anglada, Marc
Pellice, Sergio Antonio
Cavalieri, Ana Lia
author_role author
author2 Jimenez Pique, Emilio
Anglada, Marc
Pellice, Sergio Antonio
Cavalieri, Ana Lia
author2_role author
author
author
author
dc.subject.none.fl_str_mv Mechanical Properties
Nanoindentation
Orthopaedic Stainless Steel
Silica Coatings
topic Mechanical Properties
Nanoindentation
Orthopaedic Stainless Steel
Silica Coatings
purl_subject.fl_str_mv https://purl.org/becyt/ford/2.10
https://purl.org/becyt/ford/2
dc.description.none.fl_txt_mv One way to enhance the surface properties of metals used as surgical implants such as wear or protective behaviour is to use hybrid organic-inorganic sol-gel coatings. The addition of SiO2 colloidal particles to some hybrid formulation is thought to give films with bigger thickness than the coatings without particles, acting as mechanical reinforcement and to make an adequate surface to resist the extreme surgical procedures taking place in orthopaedic replacements. Coatings made by sol-gel with tetraethoxysilane (TEOS) and methyltriethoxysilane (MTES) with the addition of silica nanoparticles were applied onto surgical grade stainless steel. One of the most recent techniques used to study the mechanical properties of thin films is the instrumented indentation, known as nanoindentation, was used to evaluate elastic modulus, hardness and friction coefficient. This is a superficial technique used to measure quasi-statically the penetration of an indenter at increasing loads applied to very little volumes of material. The mechanical properties values found for the TEOS-MTES-10%SiO2 coating are smaller than for the 30% filled coating, and higher that the coating without nanoparticles. In the scratch test of the TEOS-MTES-SiO2 30 wt.% coating it can be seen that in this case the failure takes place at higher applied load than for the less silica reinforced one, indicating a much better adhesion than the system with 10% of SiO2 nanoparticles. © 2009 Elsevier B.V. All rights reserved.
Fil: Ballarre, Josefina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Fil: Jimenez Pique, Emilio. Universidad Politécnica de Catalunya; España
Fil: Anglada, Marc. Universidad Politécnica de Catalunya; España
Fil: Pellice, Sergio Antonio. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Fil: Cavalieri, Ana Lia. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
description One way to enhance the surface properties of metals used as surgical implants such as wear or protective behaviour is to use hybrid organic-inorganic sol-gel coatings. The addition of SiO2 colloidal particles to some hybrid formulation is thought to give films with bigger thickness than the coatings without particles, acting as mechanical reinforcement and to make an adequate surface to resist the extreme surgical procedures taking place in orthopaedic replacements. Coatings made by sol-gel with tetraethoxysilane (TEOS) and methyltriethoxysilane (MTES) with the addition of silica nanoparticles were applied onto surgical grade stainless steel. One of the most recent techniques used to study the mechanical properties of thin films is the instrumented indentation, known as nanoindentation, was used to evaluate elastic modulus, hardness and friction coefficient. This is a superficial technique used to measure quasi-statically the penetration of an indenter at increasing loads applied to very little volumes of material. The mechanical properties values found for the TEOS-MTES-10%SiO2 coating are smaller than for the 30% filled coating, and higher that the coating without nanoparticles. In the scratch test of the TEOS-MTES-SiO2 30 wt.% coating it can be seen that in this case the failure takes place at higher applied load than for the less silica reinforced one, indicating a much better adhesion than the system with 10% of SiO2 nanoparticles. © 2009 Elsevier B.V. All rights reserved.
publishDate 2009
dc.date.none.fl_str_mv 2009-07
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/66115
Ballarre, Josefina; Jimenez Pique, Emilio; Anglada, Marc; Pellice, Sergio Antonio; Cavalieri, Ana Lia; Mechanical characterization of nano-reinforced silica based sol-gel hybrid coatings on AISI 316L stainless steel using nanoindentation techniques; Elsevier Science Sa; Surface and Coatings Technology; 203; 20-21; 7-2009; 3325-3331
0257-8972
CONICET Digital
CONICET
url http://hdl.handle.net/11336/66115
identifier_str_mv Ballarre, Josefina; Jimenez Pique, Emilio; Anglada, Marc; Pellice, Sergio Antonio; Cavalieri, Ana Lia; Mechanical characterization of nano-reinforced silica based sol-gel hybrid coatings on AISI 316L stainless steel using nanoindentation techniques; Elsevier Science Sa; Surface and Coatings Technology; 203; 20-21; 7-2009; 3325-3331
0257-8972
CONICET Digital
CONICET
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/doi/10.1016/j.surfcoat.2009.04.014
info:eu-repo/semantics/altIdentifier/url/https://linkinghub.elsevier.com/retrieve/pii/S0257897209003594
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
application/pdf
dc.publisher.none.fl_str_mv Elsevier Science Sa
publisher.none.fl_str_mv Elsevier Science Sa
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
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score 13.070432

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