Obtaining Phenolic-Enriched Liquid Fractions and Compostable Pomace for Agriculture from Alperujo Using Standard Two-Phase Olive Oil Mill Equipment

Autores
Rodriguez, Manuel; Rodríguez Gutiérrez, Guillermo; Giménez, Marianela; Rizzo, Pedro Federico; Bueno, Luis; Deiana, Ana Cristina; Monetta, Pablo Miguel
Año de publicación
2024
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
Olive oil extraction by two-phase systems generates a by-product called “alperujo” which presents several difficulties for its valorization. The present work evaluated an industrial approach, based on the application of thermal treatments to alperujo followed by solid/liquid separation using standard two-phase olive oil mill equipment. Treatments consisted of the thermo-malaxation of alperujo at 70 °C for 45 or 90 min, with or without acid addition, followed by solid/liquid separa-tion in an industrial decanter. The solid was characterized concerning subsequent use for com-posting, while total and hydrophilic phenolics were analyzed in liquid for their recovery. Addi-tionally, a laboratory-scale trial to compare phenolic purification by ethylic acetate extraction with chromatographic procedures was also included. The static respiration index showed that solid fractions presented higher susceptibility to biodegradation processes than raw alperujo. The phe-nolic content of treated liquid fractions was higher than in raw alperujo. Total phenolics were maximum at the longest exposure time without acid addition, while hydrophilic phenolics were highest at the shortest exposure time in acidified samples. The use of non-ionic resins seemed attractive for obtaining highly concentrated phenolic fractions. The proposed thermal treatments can be applied in olive oil industries, allowing in situ pomace valorization and the recovery of phenolic-enriched liquid fractions.
Fil: Rodriguez, Manuel. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina. Instituto Nacional de Tecnología Agropecuaria. Centro Regional Mendoza - San Juan. Estación Experimental Agropecuaria San Juan; Argentina
Fil: Rodríguez Gutiérrez, Guillermo. Consejo Superior de Investigaciones Científicas; España
Fil: Giménez, Marianela. Universidad Nacional de San Juan. Facultad de Ingeniería. Instituto de Ingeniería Química; Argentina
Fil: Rizzo, Pedro Federico. Instituto Nacional de Tecnología Agropecuaria; Argentina
Fil: Bueno, Luis. Instituto Nacional de Tecnología Agropecuaria. Centro Regional Mendoza - San Juan. Estación Experimental Agropecuaria San Juan; Argentina
Fil: Deiana, Ana Cristina. Universidad Nacional de San Juan. Facultad de Ingeniería. Instituto de Ingeniería Química; Argentina
Fil: Monetta, Pablo Miguel. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina. Instituto Nacional de Tecnología Agropecuaria. Centro Regional Mendoza - San Juan. Estación Experimental Agropecuaria San Juan; Argentina
Materia
Hydroxytyrosol
Alperujo
Phenolics
Bioactive compounds
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/248184
Acceder
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network_acronym_str CONICETDig
repository_id_str 3498
network_name_str CONICET Digital (CONICET)
spelling Obtaining Phenolic-Enriched Liquid Fractions and Compostable Pomace for Agriculture from Alperujo Using Standard Two-Phase Olive Oil Mill EquipmentRodriguez, ManuelRodríguez Gutiérrez, GuillermoGiménez, MarianelaRizzo, Pedro FedericoBueno, LuisDeiana, Ana CristinaMonetta, Pablo MiguelHydroxytyrosolAlperujoPhenolicsBioactive compoundshttps://purl.org/becyt/ford/4.4https://purl.org/becyt/ford/4Olive oil extraction by two-phase systems generates a by-product called “alperujo” which presents several difficulties for its valorization. The present work evaluated an industrial approach, based on the application of thermal treatments to alperujo followed by solid/liquid separation using standard two-phase olive oil mill equipment. Treatments consisted of the thermo-malaxation of alperujo at 70 °C for 45 or 90 min, with or without acid addition, followed by solid/liquid separa-tion in an industrial decanter. The solid was characterized concerning subsequent use for com-posting, while total and hydrophilic phenolics were analyzed in liquid for their recovery. Addi-tionally, a laboratory-scale trial to compare phenolic purification by ethylic acetate extraction with chromatographic procedures was also included. The static respiration index showed that solid fractions presented higher susceptibility to biodegradation processes than raw alperujo. The phe-nolic content of treated liquid fractions was higher than in raw alperujo. Total phenolics were maximum at the longest exposure time without acid addition, while hydrophilic phenolics were highest at the shortest exposure time in acidified samples. The use of non-ionic resins seemed attractive for obtaining highly concentrated phenolic fractions. The proposed thermal treatments can be applied in olive oil industries, allowing in situ pomace valorization and the recovery of phenolic-enriched liquid fractions.Fil: Rodriguez, Manuel. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina. Instituto Nacional de Tecnología Agropecuaria. Centro Regional Mendoza - San Juan. Estación Experimental Agropecuaria San Juan; ArgentinaFil: Rodríguez Gutiérrez, Guillermo. Consejo Superior de Investigaciones Científicas; EspañaFil: Giménez, Marianela. Universidad Nacional de San Juan. Facultad de Ingeniería. Instituto de Ingeniería Química; ArgentinaFil: Rizzo, Pedro Federico. Instituto Nacional de Tecnología Agropecuaria; ArgentinaFil: Bueno, Luis. Instituto Nacional de Tecnología Agropecuaria. Centro Regional Mendoza - San Juan. Estación Experimental Agropecuaria San Juan; ArgentinaFil: Deiana, Ana Cristina. Universidad Nacional de San Juan. Facultad de Ingeniería. Instituto de Ingeniería Química; ArgentinaFil: Monetta, Pablo Miguel. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina. Instituto Nacional de Tecnología Agropecuaria. Centro Regional Mendoza - San Juan. Estación Experimental Agropecuaria San Juan; ArgentinaMultidisciplinary Digital Publishing Institute2024-08-22info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/248184Rodriguez, Manuel; Rodríguez Gutiérrez, Guillermo; Giménez, Marianela; Rizzo, Pedro Federico; Bueno, Luis; et al.; Obtaining Phenolic-Enriched Liquid Fractions and Compostable Pomace for Agriculture from Alperujo Using Standard Two-Phase Olive Oil Mill Equipment; Multidisciplinary Digital Publishing Institute; Agriculture; 14; 8; 22-8-2024; 1-122077-0472CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/url/https://www.mdpi.com/2077-0472/14/8/1427info:eu-repo/semantics/altIdentifier/doi/10.3390/agriculture14081427info:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-09-29T09:35:21Zoai:ri.conicet.gov.ar:11336/248184instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-09-29 09:35:22.129CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Obtaining Phenolic-Enriched Liquid Fractions and Compostable Pomace for Agriculture from Alperujo Using Standard Two-Phase Olive Oil Mill Equipment
title Obtaining Phenolic-Enriched Liquid Fractions and Compostable Pomace for Agriculture from Alperujo Using Standard Two-Phase Olive Oil Mill Equipment
spellingShingle Obtaining Phenolic-Enriched Liquid Fractions and Compostable Pomace for Agriculture from Alperujo Using Standard Two-Phase Olive Oil Mill Equipment
Rodriguez, Manuel
Hydroxytyrosol
Alperujo
Phenolics
Bioactive compounds
title_short Obtaining Phenolic-Enriched Liquid Fractions and Compostable Pomace for Agriculture from Alperujo Using Standard Two-Phase Olive Oil Mill Equipment
title_full Obtaining Phenolic-Enriched Liquid Fractions and Compostable Pomace for Agriculture from Alperujo Using Standard Two-Phase Olive Oil Mill Equipment
title_fullStr Obtaining Phenolic-Enriched Liquid Fractions and Compostable Pomace for Agriculture from Alperujo Using Standard Two-Phase Olive Oil Mill Equipment
title_full_unstemmed Obtaining Phenolic-Enriched Liquid Fractions and Compostable Pomace for Agriculture from Alperujo Using Standard Two-Phase Olive Oil Mill Equipment
title_sort Obtaining Phenolic-Enriched Liquid Fractions and Compostable Pomace for Agriculture from Alperujo Using Standard Two-Phase Olive Oil Mill Equipment
dc.creator.none.fl_str_mv Rodriguez, Manuel
Rodríguez Gutiérrez, Guillermo
Giménez, Marianela
Rizzo, Pedro Federico
Bueno, Luis
Deiana, Ana Cristina
Monetta, Pablo Miguel
author Rodriguez, Manuel
author_facet Rodriguez, Manuel
Rodríguez Gutiérrez, Guillermo
Giménez, Marianela
Rizzo, Pedro Federico
Bueno, Luis
Deiana, Ana Cristina
Monetta, Pablo Miguel
author_role author
author2 Rodríguez Gutiérrez, Guillermo
Giménez, Marianela
Rizzo, Pedro Federico
Bueno, Luis
Deiana, Ana Cristina
Monetta, Pablo Miguel
author2_role author
author
author
author
author
author
dc.subject.none.fl_str_mv Hydroxytyrosol
Alperujo
Phenolics
Bioactive compounds
topic Hydroxytyrosol
Alperujo
Phenolics
Bioactive compounds
purl_subject.fl_str_mv https://purl.org/becyt/ford/4.4
https://purl.org/becyt/ford/4
dc.description.none.fl_txt_mv Olive oil extraction by two-phase systems generates a by-product called “alperujo” which presents several difficulties for its valorization. The present work evaluated an industrial approach, based on the application of thermal treatments to alperujo followed by solid/liquid separation using standard two-phase olive oil mill equipment. Treatments consisted of the thermo-malaxation of alperujo at 70 °C for 45 or 90 min, with or without acid addition, followed by solid/liquid separa-tion in an industrial decanter. The solid was characterized concerning subsequent use for com-posting, while total and hydrophilic phenolics were analyzed in liquid for their recovery. Addi-tionally, a laboratory-scale trial to compare phenolic purification by ethylic acetate extraction with chromatographic procedures was also included. The static respiration index showed that solid fractions presented higher susceptibility to biodegradation processes than raw alperujo. The phe-nolic content of treated liquid fractions was higher than in raw alperujo. Total phenolics were maximum at the longest exposure time without acid addition, while hydrophilic phenolics were highest at the shortest exposure time in acidified samples. The use of non-ionic resins seemed attractive for obtaining highly concentrated phenolic fractions. The proposed thermal treatments can be applied in olive oil industries, allowing in situ pomace valorization and the recovery of phenolic-enriched liquid fractions.
Fil: Rodriguez, Manuel. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina. Instituto Nacional de Tecnología Agropecuaria. Centro Regional Mendoza - San Juan. Estación Experimental Agropecuaria San Juan; Argentina
Fil: Rodríguez Gutiérrez, Guillermo. Consejo Superior de Investigaciones Científicas; España
Fil: Giménez, Marianela. Universidad Nacional de San Juan. Facultad de Ingeniería. Instituto de Ingeniería Química; Argentina
Fil: Rizzo, Pedro Federico. Instituto Nacional de Tecnología Agropecuaria; Argentina
Fil: Bueno, Luis. Instituto Nacional de Tecnología Agropecuaria. Centro Regional Mendoza - San Juan. Estación Experimental Agropecuaria San Juan; Argentina
Fil: Deiana, Ana Cristina. Universidad Nacional de San Juan. Facultad de Ingeniería. Instituto de Ingeniería Química; Argentina
Fil: Monetta, Pablo Miguel. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina. Instituto Nacional de Tecnología Agropecuaria. Centro Regional Mendoza - San Juan. Estación Experimental Agropecuaria San Juan; Argentina
description Olive oil extraction by two-phase systems generates a by-product called “alperujo” which presents several difficulties for its valorization. The present work evaluated an industrial approach, based on the application of thermal treatments to alperujo followed by solid/liquid separation using standard two-phase olive oil mill equipment. Treatments consisted of the thermo-malaxation of alperujo at 70 °C for 45 or 90 min, with or without acid addition, followed by solid/liquid separa-tion in an industrial decanter. The solid was characterized concerning subsequent use for com-posting, while total and hydrophilic phenolics were analyzed in liquid for their recovery. Addi-tionally, a laboratory-scale trial to compare phenolic purification by ethylic acetate extraction with chromatographic procedures was also included. The static respiration index showed that solid fractions presented higher susceptibility to biodegradation processes than raw alperujo. The phe-nolic content of treated liquid fractions was higher than in raw alperujo. Total phenolics were maximum at the longest exposure time without acid addition, while hydrophilic phenolics were highest at the shortest exposure time in acidified samples. The use of non-ionic resins seemed attractive for obtaining highly concentrated phenolic fractions. The proposed thermal treatments can be applied in olive oil industries, allowing in situ pomace valorization and the recovery of phenolic-enriched liquid fractions.
publishDate 2024
dc.date.none.fl_str_mv 2024-08-22
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/248184
Rodriguez, Manuel; Rodríguez Gutiérrez, Guillermo; Giménez, Marianela; Rizzo, Pedro Federico; Bueno, Luis; et al.; Obtaining Phenolic-Enriched Liquid Fractions and Compostable Pomace for Agriculture from Alperujo Using Standard Two-Phase Olive Oil Mill Equipment; Multidisciplinary Digital Publishing Institute; Agriculture; 14; 8; 22-8-2024; 1-12
2077-0472
CONICET Digital
CONICET
url http://hdl.handle.net/11336/248184
identifier_str_mv Rodriguez, Manuel; Rodríguez Gutiérrez, Guillermo; Giménez, Marianela; Rizzo, Pedro Federico; Bueno, Luis; et al.; Obtaining Phenolic-Enriched Liquid Fractions and Compostable Pomace for Agriculture from Alperujo Using Standard Two-Phase Olive Oil Mill Equipment; Multidisciplinary Digital Publishing Institute; Agriculture; 14; 8; 22-8-2024; 1-12
2077-0472
CONICET Digital
CONICET
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/url/https://www.mdpi.com/2077-0472/14/8/1427
info:eu-repo/semantics/altIdentifier/doi/10.3390/agriculture14081427
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
dc.publisher.none.fl_str_mv Multidisciplinary Digital Publishing Institute
publisher.none.fl_str_mv Multidisciplinary Digital Publishing Institute
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
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score 13.070432

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