Report of the CCQM-K130 : Nitrogen mass fraction measurements in glycine
- Autores
- Medvedevskikh, M.; Jury, B.; Krasheninina, M.; Acco García, S. A.; Haraldsson, C.; Rodríguez, M. A.; Rodríguez, G.; Salvo, K.; Gavrilkin, V.; Kulik, S.; Samuel, L.; Rego, E. C. P. do.; Wollinger, W.; Monteiro, T. M.; Carvalho, L. J. de.
- Año de publicación
- 2017
- Idioma
- inglés
- Tipo de recurso
- artículo
- Estado
- versión publicada
- Descripción
- Mass fraction of nitrogen is very important pointer because the results of these measurements are often used for determination of protein mass fraction that is an important indicator of the quality of the vast majority of food products and raw materials, in particular dry milk powder. Proteins-enzymes catalyze chemical reactions, protein along with fats and carbohydrates is one of the indicators characterizing the energy value of food, so its definition is mandatory for all food products. The aim of this key comparison CCQM-K130 and pilot study P166 is to support National Measurement Institutes (NMIs) and Designated Institutes (DIs) to demonstrate the validity of the procedures the employed for determination of nitrogen mass fraction in glycine. The study material for this key comparison and pilot study has been selected to be representative as one of the aminoacid – the simplest part of the protein. Glycine is an amino acid, single acid that does not have any isomers (melting point –290 °C; specific heat of evaporation − 528,6 J/kg; specific melting heat − 981,1 J/kg; pKa − 2,34, molar mass - 75,07 g/mol, density - 1,607 g/cm3). Ural Scientific Research Institute for Metrology (UNIIM) acted as the coordinating laboratory of this comparison and pilot study. Eight NMIs participated in this key comparison and two NMIs participated in Pilot study. The results of Pilot study are excluded from the Report B.
Fil: Medvedevskikh, M. Ural Scientific Research Institute for Metrology (UNIIM); Rusia
Fil: Jury, B. Ural Scientific Research Institute for Metrology (UNIIM); Rusia
Fil: Krasheninina, M. Ural Scientific Research Institute for Metrology (UNIIM); Rusia
Fil: Acco García, S. A. (INACAL); Perú
Fil: Haraldsson, C. SP Technical Research Institute of Sweden; Suecia
Fil: Rodríguez, M. A. Instituto Nacional de Tecnología Industrial (INTI); Argentina
Fil: Rodríguez, G. Instituto Nacional de Tecnología Industrial (INTI); Argentina
Fil: Salvo, K. Laboratorio Tecnológico del Uruguay (LATU); Uruguay
Fil: Gavrilkin, V. (UkrCSM); Ucrania
Fil: Kulik, S. (UkrCSM); Ucrania
Fil: Samuel, L. (MSL); Nueva Zelanda
Fil: Rego, E. C. P. do. Instituto Nacional de Metrologia, Qualidade e Tecnologia (INMetro); Brasil
Fil: Wollinger, W. Instituto Nacional de Metrologia, Qualidade e Tecnologia (INMetro); Brasil
Fil: Monteiro, T. M. Instituto Nacional de Metrologia, Qualidade e Tecnologia (INMetro); Brasil
Fil: Carvalho, L. J. de. Instituto Nacional de Metrologia, Qualidade e Tecnologia (INMetro); Brasil - Fuente
- Metrología, 54(1A)
- Materia
-
Mediciones
Metrología
Masa
Nitrógeno
Leche en polvo
Alimentos
Materias primas
Proteínas
Encimas
Aminoácidos - Nivel de accesibilidad
- acceso abierto
- Condiciones de uso
- https://creativecommons.org/licenses/by/3.0/
- Repositorio
- Institución
- Instituto Nacional de Tecnología Industrial
- OAI Identificador
- nuevadc:Rodriguez2017CCQM_pdf
Ver los metadatos del registro completo
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Report of the CCQM-K130 : Nitrogen mass fraction measurements in glycineMedvedevskikh, M.Jury, B.Krasheninina, M.Acco García, S. A.Haraldsson, C.Rodríguez, M. A.Rodríguez, G.Salvo, K.Gavrilkin, V.Kulik, S.Samuel, L.Rego, E. C. P. do.Wollinger, W.Monteiro, T. M.Carvalho, L. J. de.MedicionesMetrologíaMasaNitrógenoLeche en polvoAlimentosMaterias primasProteínasEncimasAminoácidosMass fraction of nitrogen is very important pointer because the results of these measurements are often used for determination of protein mass fraction that is an important indicator of the quality of the vast majority of food products and raw materials, in particular dry milk powder. Proteins-enzymes catalyze chemical reactions, protein along with fats and carbohydrates is one of the indicators characterizing the energy value of food, so its definition is mandatory for all food products. The aim of this key comparison CCQM-K130 and pilot study P166 is to support National Measurement Institutes (NMIs) and Designated Institutes (DIs) to demonstrate the validity of the procedures the employed for determination of nitrogen mass fraction in glycine. The study material for this key comparison and pilot study has been selected to be representative as one of the aminoacid – the simplest part of the protein. Glycine is an amino acid, single acid that does not have any isomers (melting point –290 °C; specific heat of evaporation − 528,6 J/kg; specific melting heat − 981,1 J/kg; pKa − 2,34, molar mass - 75,07 g/mol, density - 1,607 g/cm3). Ural Scientific Research Institute for Metrology (UNIIM) acted as the coordinating laboratory of this comparison and pilot study. Eight NMIs participated in this key comparison and two NMIs participated in Pilot study. The results of Pilot study are excluded from the Report B.Fil: Medvedevskikh, M. Ural Scientific Research Institute for Metrology (UNIIM); RusiaFil: Jury, B. Ural Scientific Research Institute for Metrology (UNIIM); RusiaFil: Krasheninina, M. Ural Scientific Research Institute for Metrology (UNIIM); RusiaFil: Acco García, S. A. (INACAL); PerúFil: Haraldsson, C. SP Technical Research Institute of Sweden; SueciaFil: Rodríguez, M. A. Instituto Nacional de Tecnología Industrial (INTI); ArgentinaFil: Rodríguez, G. Instituto Nacional de Tecnología Industrial (INTI); ArgentinaFil: Salvo, K. Laboratorio Tecnológico del Uruguay (LATU); UruguayFil: Gavrilkin, V. (UkrCSM); UcraniaFil: Kulik, S. (UkrCSM); UcraniaFil: Samuel, L. (MSL); Nueva ZelandaFil: Rego, E. C. P. do. Instituto Nacional de Metrologia, Qualidade e Tecnologia (INMetro); BrasilFil: Wollinger, W. Instituto Nacional de Metrologia, Qualidade e Tecnologia (INMetro); BrasilFil: Monteiro, T. M. Instituto Nacional de Metrologia, Qualidade e Tecnologia (INMetro); BrasilFil: Carvalho, L. J. de. Instituto Nacional de Metrologia, Qualidade e Tecnologia (INMetro); BrasilIOP Publishing2017info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfRodriguez2017CCQM.pdfhttps://app.inti.gob.ar/greenstone3/sites/localsite/collect/nuevadc/index/assoc/Rodrigue.dir/doc.pdfMetrología, 54(1A)reponame:Repositorio Institucional del Instituto Nacional de Tecnología Industrial (INTI)instname:Instituto Nacional de Tecnología Industrialenginfo:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by/3.0/openAccess2025-10-16T10:46:42Znuevadc:Rodriguez2017CCQM_pdfinstacron:INTIInstitucionalhttps://app.inti.gob.ar/greenstone3/biblioOrganismo científico-tecnológicohttps://argentina.gob.ar/intihttps://app.inti.gob.ar/greenstone3/oaiserver?verb=Identifypfalcato@inti.gob.arArgentinaopendoar:2025-10-16 10:46:42.83Repositorio Institucional del Instituto Nacional de Tecnología Industrial (INTI) - Instituto Nacional de Tecnología Industrialfalse |
dc.title.none.fl_str_mv |
Report of the CCQM-K130 : Nitrogen mass fraction measurements in glycine |
title |
Report of the CCQM-K130 : Nitrogen mass fraction measurements in glycine |
spellingShingle |
Report of the CCQM-K130 : Nitrogen mass fraction measurements in glycine Medvedevskikh, M. Mediciones Metrología Masa Nitrógeno Leche en polvo Alimentos Materias primas Proteínas Encimas Aminoácidos |
title_short |
Report of the CCQM-K130 : Nitrogen mass fraction measurements in glycine |
title_full |
Report of the CCQM-K130 : Nitrogen mass fraction measurements in glycine |
title_fullStr |
Report of the CCQM-K130 : Nitrogen mass fraction measurements in glycine |
title_full_unstemmed |
Report of the CCQM-K130 : Nitrogen mass fraction measurements in glycine |
title_sort |
Report of the CCQM-K130 : Nitrogen mass fraction measurements in glycine |
dc.creator.none.fl_str_mv |
Medvedevskikh, M. Jury, B. Krasheninina, M. Acco García, S. A. Haraldsson, C. Rodríguez, M. A. Rodríguez, G. Salvo, K. Gavrilkin, V. Kulik, S. Samuel, L. Rego, E. C. P. do. Wollinger, W. Monteiro, T. M. Carvalho, L. J. de. |
author |
Medvedevskikh, M. |
author_facet |
Medvedevskikh, M. Jury, B. Krasheninina, M. Acco García, S. A. Haraldsson, C. Rodríguez, M. A. Rodríguez, G. Salvo, K. Gavrilkin, V. Kulik, S. Samuel, L. Rego, E. C. P. do. Wollinger, W. Monteiro, T. M. Carvalho, L. J. de. |
author_role |
author |
author2 |
Jury, B. Krasheninina, M. Acco García, S. A. Haraldsson, C. Rodríguez, M. A. Rodríguez, G. Salvo, K. Gavrilkin, V. Kulik, S. Samuel, L. Rego, E. C. P. do. Wollinger, W. Monteiro, T. M. Carvalho, L. J. de. |
author2_role |
author author author author author author author author author author author author author author |
dc.subject.none.fl_str_mv |
Mediciones Metrología Masa Nitrógeno Leche en polvo Alimentos Materias primas Proteínas Encimas Aminoácidos |
topic |
Mediciones Metrología Masa Nitrógeno Leche en polvo Alimentos Materias primas Proteínas Encimas Aminoácidos |
dc.description.none.fl_txt_mv |
Mass fraction of nitrogen is very important pointer because the results of these measurements are often used for determination of protein mass fraction that is an important indicator of the quality of the vast majority of food products and raw materials, in particular dry milk powder. Proteins-enzymes catalyze chemical reactions, protein along with fats and carbohydrates is one of the indicators characterizing the energy value of food, so its definition is mandatory for all food products. The aim of this key comparison CCQM-K130 and pilot study P166 is to support National Measurement Institutes (NMIs) and Designated Institutes (DIs) to demonstrate the validity of the procedures the employed for determination of nitrogen mass fraction in glycine. The study material for this key comparison and pilot study has been selected to be representative as one of the aminoacid – the simplest part of the protein. Glycine is an amino acid, single acid that does not have any isomers (melting point –290 °C; specific heat of evaporation − 528,6 J/kg; specific melting heat − 981,1 J/kg; pKa − 2,34, molar mass - 75,07 g/mol, density - 1,607 g/cm3). Ural Scientific Research Institute for Metrology (UNIIM) acted as the coordinating laboratory of this comparison and pilot study. Eight NMIs participated in this key comparison and two NMIs participated in Pilot study. The results of Pilot study are excluded from the Report B. Fil: Medvedevskikh, M. Ural Scientific Research Institute for Metrology (UNIIM); Rusia Fil: Jury, B. Ural Scientific Research Institute for Metrology (UNIIM); Rusia Fil: Krasheninina, M. Ural Scientific Research Institute for Metrology (UNIIM); Rusia Fil: Acco García, S. A. (INACAL); Perú Fil: Haraldsson, C. SP Technical Research Institute of Sweden; Suecia Fil: Rodríguez, M. A. Instituto Nacional de Tecnología Industrial (INTI); Argentina Fil: Rodríguez, G. Instituto Nacional de Tecnología Industrial (INTI); Argentina Fil: Salvo, K. Laboratorio Tecnológico del Uruguay (LATU); Uruguay Fil: Gavrilkin, V. (UkrCSM); Ucrania Fil: Kulik, S. (UkrCSM); Ucrania Fil: Samuel, L. (MSL); Nueva Zelanda Fil: Rego, E. C. P. do. Instituto Nacional de Metrologia, Qualidade e Tecnologia (INMetro); Brasil Fil: Wollinger, W. Instituto Nacional de Metrologia, Qualidade e Tecnologia (INMetro); Brasil Fil: Monteiro, T. M. Instituto Nacional de Metrologia, Qualidade e Tecnologia (INMetro); Brasil Fil: Carvalho, L. J. de. Instituto Nacional de Metrologia, Qualidade e Tecnologia (INMetro); Brasil |
description |
Mass fraction of nitrogen is very important pointer because the results of these measurements are often used for determination of protein mass fraction that is an important indicator of the quality of the vast majority of food products and raw materials, in particular dry milk powder. Proteins-enzymes catalyze chemical reactions, protein along with fats and carbohydrates is one of the indicators characterizing the energy value of food, so its definition is mandatory for all food products. The aim of this key comparison CCQM-K130 and pilot study P166 is to support National Measurement Institutes (NMIs) and Designated Institutes (DIs) to demonstrate the validity of the procedures the employed for determination of nitrogen mass fraction in glycine. The study material for this key comparison and pilot study has been selected to be representative as one of the aminoacid – the simplest part of the protein. Glycine is an amino acid, single acid that does not have any isomers (melting point –290 °C; specific heat of evaporation − 528,6 J/kg; specific melting heat − 981,1 J/kg; pKa − 2,34, molar mass - 75,07 g/mol, density - 1,607 g/cm3). Ural Scientific Research Institute for Metrology (UNIIM) acted as the coordinating laboratory of this comparison and pilot study. Eight NMIs participated in this key comparison and two NMIs participated in Pilot study. The results of Pilot study are excluded from the Report B. |
publishDate |
2017 |
dc.date.none.fl_str_mv |
2017 |
dc.type.none.fl_str_mv |
info:eu-repo/semantics/article info:eu-repo/semantics/publishedVersion http://purl.org/coar/resource_type/c_6501 info:ar-repo/semantics/articulo |
format |
article |
status_str |
publishedVersion |
dc.identifier.none.fl_str_mv |
Rodriguez2017CCQM.pdf https://app.inti.gob.ar/greenstone3/sites/localsite/collect/nuevadc/index/assoc/Rodrigue.dir/doc.pdf |
identifier_str_mv |
Rodriguez2017CCQM.pdf |
url |
https://app.inti.gob.ar/greenstone3/sites/localsite/collect/nuevadc/index/assoc/Rodrigue.dir/doc.pdf |
dc.language.none.fl_str_mv |
eng |
language |
eng |
dc.rights.none.fl_str_mv |
info:eu-repo/semantics/openAccess https://creativecommons.org/licenses/by/3.0/ openAccess |
eu_rights_str_mv |
openAccess |
rights_invalid_str_mv |
https://creativecommons.org/licenses/by/3.0/ openAccess |
dc.format.none.fl_str_mv |
application/pdf |
dc.publisher.none.fl_str_mv |
IOP Publishing |
publisher.none.fl_str_mv |
IOP Publishing |
dc.source.none.fl_str_mv |
Metrología, 54(1A) reponame:Repositorio Institucional del Instituto Nacional de Tecnología Industrial (INTI) instname:Instituto Nacional de Tecnología Industrial |
reponame_str |
Repositorio Institucional del Instituto Nacional de Tecnología Industrial (INTI) |
collection |
Repositorio Institucional del Instituto Nacional de Tecnología Industrial (INTI) |
instname_str |
Instituto Nacional de Tecnología Industrial |
repository.name.fl_str_mv |
Repositorio Institucional del Instituto Nacional de Tecnología Industrial (INTI) - Instituto Nacional de Tecnología Industrial |
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pfalcato@inti.gob.ar |
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1846147090670944256 |
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12.712165 |