Report of the CCQM-K130 : Nitrogen mass fraction measurements in glycine

Autores
Medvedevskikh, M.; Jury, B.; Krasheninina, M.; Acco García, S. A.; Haraldsson, C.; Rodríguez, M. A.; Rodríguez, G.; Salvo, K.; Gavrilkin, V.; Kulik, S.; Samuel, L.; Rego, E. C. P. do.; Wollinger, W.; Monteiro, T. M.; Carvalho, L. J. de.
Año de publicación
2017
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
Mass fraction of nitrogen is very important pointer because the results of these measurements are often used for determination of protein mass fraction that is an important indicator of the quality of the vast majority of food products and raw materials, in particular dry milk powder. Proteins-enzymes catalyze chemical reactions, protein along with fats and carbohydrates is one of the indicators characterizing the energy value of food, so its definition is mandatory for all food products. The aim of this key comparison CCQM-K130 and pilot study P166 is to support National Measurement Institutes (NMIs) and Designated Institutes (DIs) to demonstrate the validity of the procedures the employed for determination of nitrogen mass fraction in glycine. The study material for this key comparison and pilot study has been selected to be representative as one of the aminoacid – the simplest part of the protein. Glycine is an amino acid, single acid that does not have any isomers (melting point –290 °C; specific heat of evaporation − 528,6 J/kg; specific melting heat − 981,1 J/kg; pKa − 2,34, molar mass - 75,07 g/mol, density - 1,607 g/cm3). Ural Scientific Research Institute for Metrology (UNIIM) acted as the coordinating laboratory of this comparison and pilot study. Eight NMIs participated in this key comparison and two NMIs participated in Pilot study. The results of Pilot study are excluded from the Report B.
Fil: Medvedevskikh, M. Ural Scientific Research Institute for Metrology (UNIIM); Rusia
Fil: Jury, B. Ural Scientific Research Institute for Metrology (UNIIM); Rusia
Fil: Krasheninina, M. Ural Scientific Research Institute for Metrology (UNIIM); Rusia
Fil: Acco García, S. A. (INACAL); Perú
Fil: Haraldsson, C. SP Technical Research Institute of Sweden; Suecia
Fil: Rodríguez, M. A. Instituto Nacional de Tecnología Industrial (INTI); Argentina
Fil: Rodríguez, G. Instituto Nacional de Tecnología Industrial (INTI); Argentina
Fil: Salvo, K. Laboratorio Tecnológico del Uruguay (LATU); Uruguay
Fil: Gavrilkin, V. (UkrCSM); Ucrania
Fil: Kulik, S. (UkrCSM); Ucrania
Fil: Samuel, L. (MSL); Nueva Zelanda
Fil: Rego, E. C. P. do. Instituto Nacional de Metrologia, Qualidade e Tecnologia (INMetro); Brasil
Fil: Wollinger, W. Instituto Nacional de Metrologia, Qualidade e Tecnologia (INMetro); Brasil
Fil: Monteiro, T. M. Instituto Nacional de Metrologia, Qualidade e Tecnologia (INMetro); Brasil
Fil: Carvalho, L. J. de. Instituto Nacional de Metrologia, Qualidade e Tecnologia (INMetro); Brasil
Fuente
Metrología, 54(1A)
Materia
Mediciones
Metrología
Masa
Nitrógeno
Leche en polvo
Alimentos
Materias primas
Proteínas
Encimas
Aminoácidos
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by/3.0/
Repositorio
Repositorio Institucional del Instituto Nacional de Tecnología Industrial (INTI)
Institución
Instituto Nacional de Tecnología Industrial
OAI Identificador
nuevadc:Rodriguez2017CCQM_pdf

id RIINTI_cdc88ae8340275a9184e5f59bf9358fa
oai_identifier_str nuevadc:Rodriguez2017CCQM_pdf
network_acronym_str RIINTI
repository_id_str
network_name_str Repositorio Institucional del Instituto Nacional de Tecnología Industrial (INTI)
spelling Report of the CCQM-K130 : Nitrogen mass fraction measurements in glycineMedvedevskikh, M.Jury, B.Krasheninina, M.Acco García, S. A.Haraldsson, C.Rodríguez, M. A.Rodríguez, G.Salvo, K.Gavrilkin, V.Kulik, S.Samuel, L.Rego, E. C. P. do.Wollinger, W.Monteiro, T. M.Carvalho, L. J. de.MedicionesMetrologíaMasaNitrógenoLeche en polvoAlimentosMaterias primasProteínasEncimasAminoácidosMass fraction of nitrogen is very important pointer because the results of these measurements are often used for determination of protein mass fraction that is an important indicator of the quality of the vast majority of food products and raw materials, in particular dry milk powder. Proteins-enzymes catalyze chemical reactions, protein along with fats and carbohydrates is one of the indicators characterizing the energy value of food, so its definition is mandatory for all food products. The aim of this key comparison CCQM-K130 and pilot study P166 is to support National Measurement Institutes (NMIs) and Designated Institutes (DIs) to demonstrate the validity of the procedures the employed for determination of nitrogen mass fraction in glycine. The study material for this key comparison and pilot study has been selected to be representative as one of the aminoacid – the simplest part of the protein. Glycine is an amino acid, single acid that does not have any isomers (melting point –290 °C; specific heat of evaporation − 528,6 J/kg; specific melting heat − 981,1 J/kg; pKa − 2,34, molar mass - 75,07 g/mol, density - 1,607 g/cm3). Ural Scientific Research Institute for Metrology (UNIIM) acted as the coordinating laboratory of this comparison and pilot study. Eight NMIs participated in this key comparison and two NMIs participated in Pilot study. The results of Pilot study are excluded from the Report B.Fil: Medvedevskikh, M. Ural Scientific Research Institute for Metrology (UNIIM); RusiaFil: Jury, B. Ural Scientific Research Institute for Metrology (UNIIM); RusiaFil: Krasheninina, M. Ural Scientific Research Institute for Metrology (UNIIM); RusiaFil: Acco García, S. A. (INACAL); PerúFil: Haraldsson, C. SP Technical Research Institute of Sweden; SueciaFil: Rodríguez, M. A. Instituto Nacional de Tecnología Industrial (INTI); ArgentinaFil: Rodríguez, G. Instituto Nacional de Tecnología Industrial (INTI); ArgentinaFil: Salvo, K. Laboratorio Tecnológico del Uruguay (LATU); UruguayFil: Gavrilkin, V. (UkrCSM); UcraniaFil: Kulik, S. (UkrCSM); UcraniaFil: Samuel, L. (MSL); Nueva ZelandaFil: Rego, E. C. P. do. Instituto Nacional de Metrologia, Qualidade e Tecnologia (INMetro); BrasilFil: Wollinger, W. Instituto Nacional de Metrologia, Qualidade e Tecnologia (INMetro); BrasilFil: Monteiro, T. M. Instituto Nacional de Metrologia, Qualidade e Tecnologia (INMetro); BrasilFil: Carvalho, L. J. de. Instituto Nacional de Metrologia, Qualidade e Tecnologia (INMetro); BrasilIOP Publishing2017info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfRodriguez2017CCQM.pdfhttps://app.inti.gob.ar/greenstone3/sites/localsite/collect/nuevadc/index/assoc/Rodrigue.dir/doc.pdfMetrología, 54(1A)reponame:Repositorio Institucional del Instituto Nacional de Tecnología Industrial (INTI)instname:Instituto Nacional de Tecnología Industrialenginfo:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by/3.0/openAccess2025-10-16T10:46:42Znuevadc:Rodriguez2017CCQM_pdfinstacron:INTIInstitucionalhttps://app.inti.gob.ar/greenstone3/biblioOrganismo científico-tecnológicohttps://argentina.gob.ar/intihttps://app.inti.gob.ar/greenstone3/oaiserver?verb=Identifypfalcato@inti.gob.arArgentinaopendoar:2025-10-16 10:46:42.83Repositorio Institucional del Instituto Nacional de Tecnología Industrial (INTI) - Instituto Nacional de Tecnología Industrialfalse
dc.title.none.fl_str_mv Report of the CCQM-K130 : Nitrogen mass fraction measurements in glycine
title Report of the CCQM-K130 : Nitrogen mass fraction measurements in glycine
spellingShingle Report of the CCQM-K130 : Nitrogen mass fraction measurements in glycine
Medvedevskikh, M.
Mediciones
Metrología
Masa
Nitrógeno
Leche en polvo
Alimentos
Materias primas
Proteínas
Encimas
Aminoácidos
title_short Report of the CCQM-K130 : Nitrogen mass fraction measurements in glycine
title_full Report of the CCQM-K130 : Nitrogen mass fraction measurements in glycine
title_fullStr Report of the CCQM-K130 : Nitrogen mass fraction measurements in glycine
title_full_unstemmed Report of the CCQM-K130 : Nitrogen mass fraction measurements in glycine
title_sort Report of the CCQM-K130 : Nitrogen mass fraction measurements in glycine
dc.creator.none.fl_str_mv Medvedevskikh, M.
Jury, B.
Krasheninina, M.
Acco García, S. A.
Haraldsson, C.
Rodríguez, M. A.
Rodríguez, G.
Salvo, K.
Gavrilkin, V.
Kulik, S.
Samuel, L.
Rego, E. C. P. do.
Wollinger, W.
Monteiro, T. M.
Carvalho, L. J. de.
author Medvedevskikh, M.
author_facet Medvedevskikh, M.
Jury, B.
Krasheninina, M.
Acco García, S. A.
Haraldsson, C.
Rodríguez, M. A.
Rodríguez, G.
Salvo, K.
Gavrilkin, V.
Kulik, S.
Samuel, L.
Rego, E. C. P. do.
Wollinger, W.
Monteiro, T. M.
Carvalho, L. J. de.
author_role author
author2 Jury, B.
Krasheninina, M.
Acco García, S. A.
Haraldsson, C.
Rodríguez, M. A.
Rodríguez, G.
Salvo, K.
Gavrilkin, V.
Kulik, S.
Samuel, L.
Rego, E. C. P. do.
Wollinger, W.
Monteiro, T. M.
Carvalho, L. J. de.
author2_role author
author
author
author
author
author
author
author
author
author
author
author
author
author
dc.subject.none.fl_str_mv Mediciones
Metrología
Masa
Nitrógeno
Leche en polvo
Alimentos
Materias primas
Proteínas
Encimas
Aminoácidos
topic Mediciones
Metrología
Masa
Nitrógeno
Leche en polvo
Alimentos
Materias primas
Proteínas
Encimas
Aminoácidos
dc.description.none.fl_txt_mv Mass fraction of nitrogen is very important pointer because the results of these measurements are often used for determination of protein mass fraction that is an important indicator of the quality of the vast majority of food products and raw materials, in particular dry milk powder. Proteins-enzymes catalyze chemical reactions, protein along with fats and carbohydrates is one of the indicators characterizing the energy value of food, so its definition is mandatory for all food products. The aim of this key comparison CCQM-K130 and pilot study P166 is to support National Measurement Institutes (NMIs) and Designated Institutes (DIs) to demonstrate the validity of the procedures the employed for determination of nitrogen mass fraction in glycine. The study material for this key comparison and pilot study has been selected to be representative as one of the aminoacid – the simplest part of the protein. Glycine is an amino acid, single acid that does not have any isomers (melting point –290 °C; specific heat of evaporation − 528,6 J/kg; specific melting heat − 981,1 J/kg; pKa − 2,34, molar mass - 75,07 g/mol, density - 1,607 g/cm3). Ural Scientific Research Institute for Metrology (UNIIM) acted as the coordinating laboratory of this comparison and pilot study. Eight NMIs participated in this key comparison and two NMIs participated in Pilot study. The results of Pilot study are excluded from the Report B.
Fil: Medvedevskikh, M. Ural Scientific Research Institute for Metrology (UNIIM); Rusia
Fil: Jury, B. Ural Scientific Research Institute for Metrology (UNIIM); Rusia
Fil: Krasheninina, M. Ural Scientific Research Institute for Metrology (UNIIM); Rusia
Fil: Acco García, S. A. (INACAL); Perú
Fil: Haraldsson, C. SP Technical Research Institute of Sweden; Suecia
Fil: Rodríguez, M. A. Instituto Nacional de Tecnología Industrial (INTI); Argentina
Fil: Rodríguez, G. Instituto Nacional de Tecnología Industrial (INTI); Argentina
Fil: Salvo, K. Laboratorio Tecnológico del Uruguay (LATU); Uruguay
Fil: Gavrilkin, V. (UkrCSM); Ucrania
Fil: Kulik, S. (UkrCSM); Ucrania
Fil: Samuel, L. (MSL); Nueva Zelanda
Fil: Rego, E. C. P. do. Instituto Nacional de Metrologia, Qualidade e Tecnologia (INMetro); Brasil
Fil: Wollinger, W. Instituto Nacional de Metrologia, Qualidade e Tecnologia (INMetro); Brasil
Fil: Monteiro, T. M. Instituto Nacional de Metrologia, Qualidade e Tecnologia (INMetro); Brasil
Fil: Carvalho, L. J. de. Instituto Nacional de Metrologia, Qualidade e Tecnologia (INMetro); Brasil
description Mass fraction of nitrogen is very important pointer because the results of these measurements are often used for determination of protein mass fraction that is an important indicator of the quality of the vast majority of food products and raw materials, in particular dry milk powder. Proteins-enzymes catalyze chemical reactions, protein along with fats and carbohydrates is one of the indicators characterizing the energy value of food, so its definition is mandatory for all food products. The aim of this key comparison CCQM-K130 and pilot study P166 is to support National Measurement Institutes (NMIs) and Designated Institutes (DIs) to demonstrate the validity of the procedures the employed for determination of nitrogen mass fraction in glycine. The study material for this key comparison and pilot study has been selected to be representative as one of the aminoacid – the simplest part of the protein. Glycine is an amino acid, single acid that does not have any isomers (melting point –290 °C; specific heat of evaporation − 528,6 J/kg; specific melting heat − 981,1 J/kg; pKa − 2,34, molar mass - 75,07 g/mol, density - 1,607 g/cm3). Ural Scientific Research Institute for Metrology (UNIIM) acted as the coordinating laboratory of this comparison and pilot study. Eight NMIs participated in this key comparison and two NMIs participated in Pilot study. The results of Pilot study are excluded from the Report B.
publishDate 2017
dc.date.none.fl_str_mv 2017
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv Rodriguez2017CCQM.pdf
https://app.inti.gob.ar/greenstone3/sites/localsite/collect/nuevadc/index/assoc/Rodrigue.dir/doc.pdf
identifier_str_mv Rodriguez2017CCQM.pdf
url https://app.inti.gob.ar/greenstone3/sites/localsite/collect/nuevadc/index/assoc/Rodrigue.dir/doc.pdf
dc.language.none.fl_str_mv eng
language eng
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by/3.0/
openAccess
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by/3.0/
openAccess
dc.format.none.fl_str_mv application/pdf
dc.publisher.none.fl_str_mv IOP Publishing
publisher.none.fl_str_mv IOP Publishing
dc.source.none.fl_str_mv Metrología, 54(1A)
reponame:Repositorio Institucional del Instituto Nacional de Tecnología Industrial (INTI)
instname:Instituto Nacional de Tecnología Industrial
reponame_str Repositorio Institucional del Instituto Nacional de Tecnología Industrial (INTI)
collection Repositorio Institucional del Instituto Nacional de Tecnología Industrial (INTI)
instname_str Instituto Nacional de Tecnología Industrial
repository.name.fl_str_mv Repositorio Institucional del Instituto Nacional de Tecnología Industrial (INTI) - Instituto Nacional de Tecnología Industrial
repository.mail.fl_str_mv pfalcato@inti.gob.ar
_version_ 1846147090670944256
score 12.712165