CCQM key comparison – organic solutions : CCQM-K47 volatile organic compounds in methanol. Final Report

Autores
Pérez Urquiza, M.; Maldonado Torres, M.; Mitani, Y.; Schantz, M. M.; Duewer, D. L.; May, W. E.; Parris, R. M.; Wise, S. A.; Kaminski, K.; Philipp, R.; Win, T.; Rosso, A.; Kim, D. H.; Ishikawa, K.; Krylov, A. I.; Kustikov, Y. A.; Baldan, A.
Año de publicación
2013
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
At the October 2005 CCQM Organic Analysis Working Group Meeting (IRMM, Belgium), the decision was made to proceed with a Key Comparison study (CCQM-K47) addressing the calibration function for the determination of volatile organic compounds (VOCs) used for water quality monitoring. This was coordinated by CENAM and NIST. Benzene, o-xylene, m-xylene and p-xylene were chosen as representative VOCs. The solvent of choice was methanol. Key Comparison CCQM-K47 demonstrated the capabilities of participating NMIs to identify and measure the four target VOCs in a calibration solution using GC-based methods. The measurement challenges in CCQM-K47, such as avoiding volatility loss, achieving adequate chromatographic resolution and isolating potential interferences, are typical of those required for value-assigning volatile reference materials. Participants achieving comparable measurements for all four VOCs in this Key Comparison should be capable of providing reference materials and measurements for VOCs in solutions when present at concentration levels greater than 10 µg/g.
Fil: Pérez Urquiza, M. Centro Nacional de Metrología (CENAM); México
Fil: Maldonado Torres, M. Centro Nacional de Metrología (CENAM); México
Fil: Mitani, Y. Centro Nacional de Metrología (CENAM); México
Fil: Schantz, M. M. National Institute of Standards and Technology (NIST); Argentina
Fil: Duewer, D. L. National Institute of Standards and Technology (NIST); Argentina
Fil: May, W. E. National Institute of Standards and Technology (NIST); Argentina
Fil: Parris, R. M. National Institute of Standards and Technology (NIST); Argentina
Fil: Wise, S. A. National Institute of Standards and Technology (NIST); Argentina
Fil: Kaminski, K. Federal Institute for Materials Research and Testing (BAM); Alemania
Fil: Philipp, R. Federal Institute for Materials Research and Testing (BAM); Alemania
Fil: Win, T. Federal Institute for Materials Research and Testing (BAM); Alemania
Fil: Rosso, A. Instituto Nacional de Tecnología Industrial (INTI); Argentina
Fil: Kim, D. H. Korea Research Institute of Standards and Science (KRISS); Corea del Sur
Fil: Ishikawa, K. National Metrology Institute of Japan (NMIJ); Japón
Fil: Krylov, A. I. D. I. Mendeleev Institute for Metrology (VNIIM); Rusia
Fil: Kustikov, Y. A. D. I. Mendeleev Institute for Metrology (VNIIM); Rusia
Fil: Baldan, A. Van Swinden Laboratorium (VS); Países Bajos
Fuente
Metrología, 50
Materia
Metrología
Alcohol metílico
Compuestos orgánicos
Calibración
Compuestos volátiles
Interferencia
Soluciones
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by/4.0/
Repositorio
Repositorio Institucional del Instituto Nacional de Tecnología Industrial (INTI)
Institución
Instituto Nacional de Tecnología Industrial
OAI Identificador
nuevadc:Rosso2013CCQM_pdf
Acceder
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oai_identifier_str nuevadc:Rosso2013CCQM_pdf
network_acronym_str RIINTI
repository_id_str
network_name_str Repositorio Institucional del Instituto Nacional de Tecnología Industrial (INTI)
spelling CCQM key comparison – organic solutions : CCQM-K47 volatile organic compounds in methanol. Final ReportPérez Urquiza, M.Maldonado Torres, M.Mitani, Y.Schantz, M. M.Duewer, D. L.May, W. E.Parris, R. M.Wise, S. A.Kaminski, K.Philipp, R.Win, T.Rosso, A.Kim, D. H.Ishikawa, K.Krylov, A. I.Kustikov, Y. A.Baldan, A.MetrologíaAlcohol metílicoCompuestos orgánicosCalibraciónCompuestos volátilesInterferenciaSolucionesAt the October 2005 CCQM Organic Analysis Working Group Meeting (IRMM, Belgium), the decision was made to proceed with a Key Comparison study (CCQM-K47) addressing the calibration function for the determination of volatile organic compounds (VOCs) used for water quality monitoring. This was coordinated by CENAM and NIST. Benzene, o-xylene, m-xylene and p-xylene were chosen as representative VOCs. The solvent of choice was methanol. Key Comparison CCQM-K47 demonstrated the capabilities of participating NMIs to identify and measure the four target VOCs in a calibration solution using GC-based methods. The measurement challenges in CCQM-K47, such as avoiding volatility loss, achieving adequate chromatographic resolution and isolating potential interferences, are typical of those required for value-assigning volatile reference materials. Participants achieving comparable measurements for all four VOCs in this Key Comparison should be capable of providing reference materials and measurements for VOCs in solutions when present at concentration levels greater than 10 µg/g.Fil: Pérez Urquiza, M. Centro Nacional de Metrología (CENAM); MéxicoFil: Maldonado Torres, M. Centro Nacional de Metrología (CENAM); MéxicoFil: Mitani, Y. Centro Nacional de Metrología (CENAM); MéxicoFil: Schantz, M. M. National Institute of Standards and Technology (NIST); ArgentinaFil: Duewer, D. L. National Institute of Standards and Technology (NIST); ArgentinaFil: May, W. E. National Institute of Standards and Technology (NIST); ArgentinaFil: Parris, R. M. National Institute of Standards and Technology (NIST); ArgentinaFil: Wise, S. A. National Institute of Standards and Technology (NIST); ArgentinaFil: Kaminski, K. Federal Institute for Materials Research and Testing (BAM); AlemaniaFil: Philipp, R. Federal Institute for Materials Research and Testing (BAM); AlemaniaFil: Win, T. Federal Institute for Materials Research and Testing (BAM); AlemaniaFil: Rosso, A. Instituto Nacional de Tecnología Industrial (INTI); ArgentinaFil: Kim, D. H. Korea Research Institute of Standards and Science (KRISS); Corea del SurFil: Ishikawa, K. National Metrology Institute of Japan (NMIJ); JapónFil: Krylov, A. I. D. I. Mendeleev Institute for Metrology (VNIIM); RusiaFil: Kustikov, Y. A. D. I. Mendeleev Institute for Metrology (VNIIM); RusiaFil: Baldan, A. Van Swinden Laboratorium (VS); Países BajosIOP Publishing2013info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfRosso2013CCQM.pdfhttps://app.inti.gob.ar/greenstone3/sites/localsite/collect/nuevadc/index/assoc/Rosso201/3CCQM_pd.dir/doc.pdfMetrología, 50reponame:Repositorio Institucional del Instituto Nacional de Tecnología Industrial (INTI)instname:Instituto Nacional de Tecnología Industrialenginfo:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by/4.0/openAccess2025-09-04T11:42:52Znuevadc:Rosso2013CCQM_pdfinstacron:INTIInstitucionalhttps://app.inti.gob.ar/greenstone3/biblioOrganismo científico-tecnológicohttps://argentina.gob.ar/intihttps://app.inti.gob.ar/greenstone3/oaiserver?verb=Identifypfalcato@inti.gob.arArgentinaopendoar:2025-09-04 11:42:54.907Repositorio Institucional del Instituto Nacional de Tecnología Industrial (INTI) - Instituto Nacional de Tecnología Industrialfalse
dc.title.none.fl_str_mv CCQM key comparison – organic solutions : CCQM-K47 volatile organic compounds in methanol. Final Report
title CCQM key comparison – organic solutions : CCQM-K47 volatile organic compounds in methanol. Final Report
spellingShingle CCQM key comparison – organic solutions : CCQM-K47 volatile organic compounds in methanol. Final Report
Pérez Urquiza, M.
Metrología
Alcohol metílico
Compuestos orgánicos
Calibración
Compuestos volátiles
Interferencia
Soluciones
title_short CCQM key comparison – organic solutions : CCQM-K47 volatile organic compounds in methanol. Final Report
title_full CCQM key comparison – organic solutions : CCQM-K47 volatile organic compounds in methanol. Final Report
title_fullStr CCQM key comparison – organic solutions : CCQM-K47 volatile organic compounds in methanol. Final Report
title_full_unstemmed CCQM key comparison – organic solutions : CCQM-K47 volatile organic compounds in methanol. Final Report
title_sort CCQM key comparison – organic solutions : CCQM-K47 volatile organic compounds in methanol. Final Report
dc.creator.none.fl_str_mv Pérez Urquiza, M.
Maldonado Torres, M.
Mitani, Y.
Schantz, M. M.
Duewer, D. L.
May, W. E.
Parris, R. M.
Wise, S. A.
Kaminski, K.
Philipp, R.
Win, T.
Rosso, A.
Kim, D. H.
Ishikawa, K.
Krylov, A. I.
Kustikov, Y. A.
Baldan, A.
author Pérez Urquiza, M.
author_facet Pérez Urquiza, M.
Maldonado Torres, M.
Mitani, Y.
Schantz, M. M.
Duewer, D. L.
May, W. E.
Parris, R. M.
Wise, S. A.
Kaminski, K.
Philipp, R.
Win, T.
Rosso, A.
Kim, D. H.
Ishikawa, K.
Krylov, A. I.
Kustikov, Y. A.
Baldan, A.
author_role author
author2 Maldonado Torres, M.
Mitani, Y.
Schantz, M. M.
Duewer, D. L.
May, W. E.
Parris, R. M.
Wise, S. A.
Kaminski, K.
Philipp, R.
Win, T.
Rosso, A.
Kim, D. H.
Ishikawa, K.
Krylov, A. I.
Kustikov, Y. A.
Baldan, A.
author2_role author
author
author
author
author
author
author
author
author
author
author
author
author
author
author
author
dc.subject.none.fl_str_mv Metrología
Alcohol metílico
Compuestos orgánicos
Calibración
Compuestos volátiles
Interferencia
Soluciones
topic Metrología
Alcohol metílico
Compuestos orgánicos
Calibración
Compuestos volátiles
Interferencia
Soluciones
dc.description.none.fl_txt_mv At the October 2005 CCQM Organic Analysis Working Group Meeting (IRMM, Belgium), the decision was made to proceed with a Key Comparison study (CCQM-K47) addressing the calibration function for the determination of volatile organic compounds (VOCs) used for water quality monitoring. This was coordinated by CENAM and NIST. Benzene, o-xylene, m-xylene and p-xylene were chosen as representative VOCs. The solvent of choice was methanol. Key Comparison CCQM-K47 demonstrated the capabilities of participating NMIs to identify and measure the four target VOCs in a calibration solution using GC-based methods. The measurement challenges in CCQM-K47, such as avoiding volatility loss, achieving adequate chromatographic resolution and isolating potential interferences, are typical of those required for value-assigning volatile reference materials. Participants achieving comparable measurements for all four VOCs in this Key Comparison should be capable of providing reference materials and measurements for VOCs in solutions when present at concentration levels greater than 10 µg/g.
Fil: Pérez Urquiza, M. Centro Nacional de Metrología (CENAM); México
Fil: Maldonado Torres, M. Centro Nacional de Metrología (CENAM); México
Fil: Mitani, Y. Centro Nacional de Metrología (CENAM); México
Fil: Schantz, M. M. National Institute of Standards and Technology (NIST); Argentina
Fil: Duewer, D. L. National Institute of Standards and Technology (NIST); Argentina
Fil: May, W. E. National Institute of Standards and Technology (NIST); Argentina
Fil: Parris, R. M. National Institute of Standards and Technology (NIST); Argentina
Fil: Wise, S. A. National Institute of Standards and Technology (NIST); Argentina
Fil: Kaminski, K. Federal Institute for Materials Research and Testing (BAM); Alemania
Fil: Philipp, R. Federal Institute for Materials Research and Testing (BAM); Alemania
Fil: Win, T. Federal Institute for Materials Research and Testing (BAM); Alemania
Fil: Rosso, A. Instituto Nacional de Tecnología Industrial (INTI); Argentina
Fil: Kim, D. H. Korea Research Institute of Standards and Science (KRISS); Corea del Sur
Fil: Ishikawa, K. National Metrology Institute of Japan (NMIJ); Japón
Fil: Krylov, A. I. D. I. Mendeleev Institute for Metrology (VNIIM); Rusia
Fil: Kustikov, Y. A. D. I. Mendeleev Institute for Metrology (VNIIM); Rusia
Fil: Baldan, A. Van Swinden Laboratorium (VS); Países Bajos
description At the October 2005 CCQM Organic Analysis Working Group Meeting (IRMM, Belgium), the decision was made to proceed with a Key Comparison study (CCQM-K47) addressing the calibration function for the determination of volatile organic compounds (VOCs) used for water quality monitoring. This was coordinated by CENAM and NIST. Benzene, o-xylene, m-xylene and p-xylene were chosen as representative VOCs. The solvent of choice was methanol. Key Comparison CCQM-K47 demonstrated the capabilities of participating NMIs to identify and measure the four target VOCs in a calibration solution using GC-based methods. The measurement challenges in CCQM-K47, such as avoiding volatility loss, achieving adequate chromatographic resolution and isolating potential interferences, are typical of those required for value-assigning volatile reference materials. Participants achieving comparable measurements for all four VOCs in this Key Comparison should be capable of providing reference materials and measurements for VOCs in solutions when present at concentration levels greater than 10 µg/g.
publishDate 2013
dc.date.none.fl_str_mv 2013
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv Rosso2013CCQM.pdf
https://app.inti.gob.ar/greenstone3/sites/localsite/collect/nuevadc/index/assoc/Rosso201/3CCQM_pd.dir/doc.pdf
identifier_str_mv Rosso2013CCQM.pdf
url https://app.inti.gob.ar/greenstone3/sites/localsite/collect/nuevadc/index/assoc/Rosso201/3CCQM_pd.dir/doc.pdf
dc.language.none.fl_str_mv eng
language eng
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by/4.0/
openAccess
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by/4.0/
openAccess
dc.format.none.fl_str_mv application/pdf
dc.publisher.none.fl_str_mv IOP Publishing
publisher.none.fl_str_mv IOP Publishing
dc.source.none.fl_str_mv Metrología, 50
reponame:Repositorio Institucional del Instituto Nacional de Tecnología Industrial (INTI)
instname:Instituto Nacional de Tecnología Industrial
reponame_str Repositorio Institucional del Instituto Nacional de Tecnología Industrial (INTI)
collection Repositorio Institucional del Instituto Nacional de Tecnología Industrial (INTI)
instname_str Instituto Nacional de Tecnología Industrial
repository.name.fl_str_mv Repositorio Institucional del Instituto Nacional de Tecnología Industrial (INTI) - Instituto Nacional de Tecnología Industrial
repository.mail.fl_str_mv pfalcato@inti.gob.ar
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score 12.623145

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