Solid-Phase Microextraction—Gas Chromatography Analytical Strategies for Pesticide Analysis

Autores
Aspromonte, Juan; Lancioni, Carlina; Purcaro, Giorgia
Año de publicación
2022
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
Due to their extensive use and the globalized commerce of agricultural goods, pesticides have become a global concern. Despite the undoubtful advantages of their use in agricultural practices, their misuse is a threat to the environment and human health. Their analysis in environmental samples and in food products continues to gain interest in the analytical chemistry community as they are challenging matrices, and legal concentration limits are particularly low (in the order of ppb). In particular, the use of solid-phase microextraction (SPME) has gained special attention in this field thanks to its potential to minimize the matrix effect, while enriching its concentration, allowing very low limits of detection, and without the need of a large amount of solvents or lengthy procedures. Moreover, its combination with gas chromatography (GC) can be easily automated, making it a very interesting approach for routine analysis. In this review, advances and analytical strategies for the use of SPME coupled with GC are discussed and compared for the analysis of pesticides in food and environmental samples, hopefully encouraging its further development and routine application in this field.
Fil: Aspromonte, Juan. Universidad Nacional de la Plata. Facultad de Cs.exactas. Laboratorio de Investigacion y Desarrollo de Metodos Analiticos. - Comision de Investigaciones Cientificas de la Provincia de Buenos Aires. Laboratorio de Investigacion y Desarrollo de Metodos Analiticos.; Argentina
Fil: Lancioni, Carlina. Universidad Nacional de la Plata. Facultad de Cs.exactas. Laboratorio de Investigacion y Desarrollo de Metodos Analiticos. - Comision de Investigaciones Cientificas de la Provincia de Buenos Aires. Laboratorio de Investigacion y Desarrollo de Metodos Analiticos.; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata; Argentina
Fil: Purcaro, Giorgia. Université de Liège; Bélgica
Materia
ENVIRONMENTAL
FOOD
GAS CHROMATOGRAPHY
MASS SPECTROMETRY
PESTICIDE
SPME
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/217954
Acceder
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network_name_str CONICET Digital (CONICET)
spelling Solid-Phase Microextraction—Gas Chromatography Analytical Strategies for Pesticide AnalysisAspromonte, JuanLancioni, CarlinaPurcaro, GiorgiaENVIRONMENTALFOODGAS CHROMATOGRAPHYMASS SPECTROMETRYPESTICIDESPMEhttps://purl.org/becyt/ford/1.4https://purl.org/becyt/ford/1Due to their extensive use and the globalized commerce of agricultural goods, pesticides have become a global concern. Despite the undoubtful advantages of their use in agricultural practices, their misuse is a threat to the environment and human health. Their analysis in environmental samples and in food products continues to gain interest in the analytical chemistry community as they are challenging matrices, and legal concentration limits are particularly low (in the order of ppb). In particular, the use of solid-phase microextraction (SPME) has gained special attention in this field thanks to its potential to minimize the matrix effect, while enriching its concentration, allowing very low limits of detection, and without the need of a large amount of solvents or lengthy procedures. Moreover, its combination with gas chromatography (GC) can be easily automated, making it a very interesting approach for routine analysis. In this review, advances and analytical strategies for the use of SPME coupled with GC are discussed and compared for the analysis of pesticides in food and environmental samples, hopefully encouraging its further development and routine application in this field.Fil: Aspromonte, Juan. Universidad Nacional de la Plata. Facultad de Cs.exactas. Laboratorio de Investigacion y Desarrollo de Metodos Analiticos. - Comision de Investigaciones Cientificas de la Provincia de Buenos Aires. Laboratorio de Investigacion y Desarrollo de Metodos Analiticos.; ArgentinaFil: Lancioni, Carlina. Universidad Nacional de la Plata. Facultad de Cs.exactas. Laboratorio de Investigacion y Desarrollo de Metodos Analiticos. - Comision de Investigaciones Cientificas de la Provincia de Buenos Aires. Laboratorio de Investigacion y Desarrollo de Metodos Analiticos.; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata; ArgentinaFil: Purcaro, Giorgia. Université de Liège; BélgicaMultidisciplinary Digital Publishing Institute2022-10info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/217954Aspromonte, Juan; Lancioni, Carlina; Purcaro, Giorgia; Solid-Phase Microextraction—Gas Chromatography Analytical Strategies for Pesticide Analysis; Multidisciplinary Digital Publishing Institute; Methods and Protocols; 5; 5; 10-2022; 1-172409-9279CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/doi/10.3390/mps5050082info:eu-repo/semantics/altIdentifier/url/https://www.mdpi.com/2409-9279/5/5/82info:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-09-10T13:04:09Zoai:ri.conicet.gov.ar:11336/217954instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-09-10 13:04:09.983CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Solid-Phase Microextraction—Gas Chromatography Analytical Strategies for Pesticide Analysis
title Solid-Phase Microextraction—Gas Chromatography Analytical Strategies for Pesticide Analysis
spellingShingle Solid-Phase Microextraction—Gas Chromatography Analytical Strategies for Pesticide Analysis
Aspromonte, Juan
ENVIRONMENTAL
FOOD
GAS CHROMATOGRAPHY
MASS SPECTROMETRY
PESTICIDE
SPME
title_short Solid-Phase Microextraction—Gas Chromatography Analytical Strategies for Pesticide Analysis
title_full Solid-Phase Microextraction—Gas Chromatography Analytical Strategies for Pesticide Analysis
title_fullStr Solid-Phase Microextraction—Gas Chromatography Analytical Strategies for Pesticide Analysis
title_full_unstemmed Solid-Phase Microextraction—Gas Chromatography Analytical Strategies for Pesticide Analysis
title_sort Solid-Phase Microextraction—Gas Chromatography Analytical Strategies for Pesticide Analysis
dc.creator.none.fl_str_mv Aspromonte, Juan
Lancioni, Carlina
Purcaro, Giorgia
author Aspromonte, Juan
author_facet Aspromonte, Juan
Lancioni, Carlina
Purcaro, Giorgia
author_role author
author2 Lancioni, Carlina
Purcaro, Giorgia
author2_role author
author
dc.subject.none.fl_str_mv ENVIRONMENTAL
FOOD
GAS CHROMATOGRAPHY
MASS SPECTROMETRY
PESTICIDE
SPME
topic ENVIRONMENTAL
FOOD
GAS CHROMATOGRAPHY
MASS SPECTROMETRY
PESTICIDE
SPME
purl_subject.fl_str_mv https://purl.org/becyt/ford/1.4
https://purl.org/becyt/ford/1
dc.description.none.fl_txt_mv Due to their extensive use and the globalized commerce of agricultural goods, pesticides have become a global concern. Despite the undoubtful advantages of their use in agricultural practices, their misuse is a threat to the environment and human health. Their analysis in environmental samples and in food products continues to gain interest in the analytical chemistry community as they are challenging matrices, and legal concentration limits are particularly low (in the order of ppb). In particular, the use of solid-phase microextraction (SPME) has gained special attention in this field thanks to its potential to minimize the matrix effect, while enriching its concentration, allowing very low limits of detection, and without the need of a large amount of solvents or lengthy procedures. Moreover, its combination with gas chromatography (GC) can be easily automated, making it a very interesting approach for routine analysis. In this review, advances and analytical strategies for the use of SPME coupled with GC are discussed and compared for the analysis of pesticides in food and environmental samples, hopefully encouraging its further development and routine application in this field.
Fil: Aspromonte, Juan. Universidad Nacional de la Plata. Facultad de Cs.exactas. Laboratorio de Investigacion y Desarrollo de Metodos Analiticos. - Comision de Investigaciones Cientificas de la Provincia de Buenos Aires. Laboratorio de Investigacion y Desarrollo de Metodos Analiticos.; Argentina
Fil: Lancioni, Carlina. Universidad Nacional de la Plata. Facultad de Cs.exactas. Laboratorio de Investigacion y Desarrollo de Metodos Analiticos. - Comision de Investigaciones Cientificas de la Provincia de Buenos Aires. Laboratorio de Investigacion y Desarrollo de Metodos Analiticos.; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata; Argentina
Fil: Purcaro, Giorgia. Université de Liège; Bélgica
description Due to their extensive use and the globalized commerce of agricultural goods, pesticides have become a global concern. Despite the undoubtful advantages of their use in agricultural practices, their misuse is a threat to the environment and human health. Their analysis in environmental samples and in food products continues to gain interest in the analytical chemistry community as they are challenging matrices, and legal concentration limits are particularly low (in the order of ppb). In particular, the use of solid-phase microextraction (SPME) has gained special attention in this field thanks to its potential to minimize the matrix effect, while enriching its concentration, allowing very low limits of detection, and without the need of a large amount of solvents or lengthy procedures. Moreover, its combination with gas chromatography (GC) can be easily automated, making it a very interesting approach for routine analysis. In this review, advances and analytical strategies for the use of SPME coupled with GC are discussed and compared for the analysis of pesticides in food and environmental samples, hopefully encouraging its further development and routine application in this field.
publishDate 2022
dc.date.none.fl_str_mv 2022-10
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/217954
Aspromonte, Juan; Lancioni, Carlina; Purcaro, Giorgia; Solid-Phase Microextraction—Gas Chromatography Analytical Strategies for Pesticide Analysis; Multidisciplinary Digital Publishing Institute; Methods and Protocols; 5; 5; 10-2022; 1-17
2409-9279
CONICET Digital
CONICET
url http://hdl.handle.net/11336/217954
identifier_str_mv Aspromonte, Juan; Lancioni, Carlina; Purcaro, Giorgia; Solid-Phase Microextraction—Gas Chromatography Analytical Strategies for Pesticide Analysis; Multidisciplinary Digital Publishing Institute; Methods and Protocols; 5; 5; 10-2022; 1-17
2409-9279
CONICET Digital
CONICET
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/doi/10.3390/mps5050082
info:eu-repo/semantics/altIdentifier/url/https://www.mdpi.com/2409-9279/5/5/82
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
dc.publisher.none.fl_str_mv Multidisciplinary Digital Publishing Institute
publisher.none.fl_str_mv Multidisciplinary Digital Publishing Institute
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
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score 12.993085

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