Headspace solid-phase microextraction: Fundamentals and recent advances

Autores
Lancioni, Carlina; Castells, Cecilia Beatriz Marta; Candal, Roberto Jorge; Tascon, Marcos
Año de publicación
2022
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
Solid-phase microextraction (SPME) has become a powerful sample preparation technique which allows to efficiently isolate and enrich analytes from complex matrixes. One of the most widespread SPME modes, consists of the extraction directly from the headspace (HS) which is equilibrated with the sample. In this sense, HS-SPME provides one of the best platforms for sample preparation, especially for the analysis of volatile and semi-volatile organic compounds. Furthermore, this technique has demonstrated to be versatile, sensitive, robust, and environmentally friendly when applied to samples coming from a diverse variety of fields such as bioanalysis, environmental sciences, food and cultural heritage. Moreover, during last years, the implementation of HS-SPME has dramatically grown along with the need to monitor complex systems over time using in situ and in vivo approaches, taking advantage of its noninvasive nature. In this review article, the authors present the fundamentals of this technique aiming to critically understand its advantages and limitations, highlighting the recent advances published in the last ten years. To this aim, special sections dealing with extractive phase development, technological advances and relevant applications in different fields have been carefully designed. Finally, some thoughts and perspectives about the future of the technique are also discussed.
Fil: Lancioni, Carlina. Universidad Nacional de La Plata. Facultad de Ciencias Exactas. Laboratorio de Investigación y Desarrollo de Métodos Analíticos. - Comisión de Investigaciones Científicas de la Provincia de Buenos Aires. Laboratorio de Investigación y Desarrollo de Métodos Analíticos; Argentina
Fil: Castells, Cecilia Beatriz Marta. Universidad Nacional de La Plata. Facultad de Ciencias Exactas. Laboratorio de Investigación y Desarrollo de Métodos Analíticos. - Comisión de Investigaciones Científicas de la Provincia de Buenos Aires. Laboratorio de Investigación y Desarrollo de Métodos Analíticos; Argentina
Fil: Candal, Roberto Jorge. Universidad Nacional de San Martín. Instituto de Investigación en Ingeniería Ambiental; Argentina. Universidad Nacional de San Martín. Instituto de Investigación e Ingeniería Ambiental. - Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Parque Centenario. Instituto de Investigación e Ingeniería Ambiental; Argentina
Fil: Tascon, Marcos. Universidad Nacional de San Martín. Instituto de Investigación en Ingeniería Ambiental; Argentina. Universidad Nacional de San Martín. Instituto de Investigación e Ingeniería Ambiental. - Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Parque Centenario. Instituto de Investigación e Ingeniería Ambiental; Argentina
Materia
HEDSPACE
SOLID PHASE MICROEXTRACTION
BIOANALYSIS
FOOD
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/203977
Acceder
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oai_identifier_str oai:ri.conicet.gov.ar:11336/203977
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network_name_str CONICET Digital (CONICET)
spelling Headspace solid-phase microextraction: Fundamentals and recent advancesLancioni, CarlinaCastells, Cecilia Beatriz MartaCandal, Roberto JorgeTascon, MarcosHEDSPACESOLID PHASE MICROEXTRACTIONBIOANALYSISFOODhttps://purl.org/becyt/ford/1.4https://purl.org/becyt/ford/1Solid-phase microextraction (SPME) has become a powerful sample preparation technique which allows to efficiently isolate and enrich analytes from complex matrixes. One of the most widespread SPME modes, consists of the extraction directly from the headspace (HS) which is equilibrated with the sample. In this sense, HS-SPME provides one of the best platforms for sample preparation, especially for the analysis of volatile and semi-volatile organic compounds. Furthermore, this technique has demonstrated to be versatile, sensitive, robust, and environmentally friendly when applied to samples coming from a diverse variety of fields such as bioanalysis, environmental sciences, food and cultural heritage. Moreover, during last years, the implementation of HS-SPME has dramatically grown along with the need to monitor complex systems over time using in situ and in vivo approaches, taking advantage of its noninvasive nature. In this review article, the authors present the fundamentals of this technique aiming to critically understand its advantages and limitations, highlighting the recent advances published in the last ten years. To this aim, special sections dealing with extractive phase development, technological advances and relevant applications in different fields have been carefully designed. Finally, some thoughts and perspectives about the future of the technique are also discussed.Fil: Lancioni, Carlina. Universidad Nacional de La Plata. Facultad de Ciencias Exactas. Laboratorio de Investigación y Desarrollo de Métodos Analíticos. - Comisión de Investigaciones Científicas de la Provincia de Buenos Aires. Laboratorio de Investigación y Desarrollo de Métodos Analíticos; ArgentinaFil: Castells, Cecilia Beatriz Marta. Universidad Nacional de La Plata. Facultad de Ciencias Exactas. Laboratorio de Investigación y Desarrollo de Métodos Analíticos. - Comisión de Investigaciones Científicas de la Provincia de Buenos Aires. Laboratorio de Investigación y Desarrollo de Métodos Analíticos; ArgentinaFil: Candal, Roberto Jorge. Universidad Nacional de San Martín. Instituto de Investigación en Ingeniería Ambiental; Argentina. Universidad Nacional de San Martín. Instituto de Investigación e Ingeniería Ambiental. - Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Parque Centenario. Instituto de Investigación e Ingeniería Ambiental; ArgentinaFil: Tascon, Marcos. Universidad Nacional de San Martín. Instituto de Investigación en Ingeniería Ambiental; Argentina. Universidad Nacional de San Martín. Instituto de Investigación e Ingeniería Ambiental. - Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Parque Centenario. Instituto de Investigación e Ingeniería Ambiental; ArgentinaElsevier2022-08info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfapplication/pdfapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/203977Lancioni, Carlina; Castells, Cecilia Beatriz Marta; Candal, Roberto Jorge; Tascon, Marcos; Headspace solid-phase microextraction: Fundamentals and recent advances; Elsevier; Advances in Sample Preparation; 3; 8-2022; 1-152772-5820CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/url/https://linkinghub.elsevier.com/retrieve/pii/S2772582022000328info:eu-repo/semantics/altIdentifier/doi/10.1016/j.sampre.2022.100035info:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-09-29T10:38:58Zoai:ri.conicet.gov.ar:11336/203977instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-09-29 10:38:59.182CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Headspace solid-phase microextraction: Fundamentals and recent advances
title Headspace solid-phase microextraction: Fundamentals and recent advances
spellingShingle Headspace solid-phase microextraction: Fundamentals and recent advances
Lancioni, Carlina
HEDSPACE
SOLID PHASE MICROEXTRACTION
BIOANALYSIS
FOOD
title_short Headspace solid-phase microextraction: Fundamentals and recent advances
title_full Headspace solid-phase microextraction: Fundamentals and recent advances
title_fullStr Headspace solid-phase microextraction: Fundamentals and recent advances
title_full_unstemmed Headspace solid-phase microextraction: Fundamentals and recent advances
title_sort Headspace solid-phase microextraction: Fundamentals and recent advances
dc.creator.none.fl_str_mv Lancioni, Carlina
Castells, Cecilia Beatriz Marta
Candal, Roberto Jorge
Tascon, Marcos
author Lancioni, Carlina
author_facet Lancioni, Carlina
Castells, Cecilia Beatriz Marta
Candal, Roberto Jorge
Tascon, Marcos
author_role author
author2 Castells, Cecilia Beatriz Marta
Candal, Roberto Jorge
Tascon, Marcos
author2_role author
author
author
dc.subject.none.fl_str_mv HEDSPACE
SOLID PHASE MICROEXTRACTION
BIOANALYSIS
FOOD
topic HEDSPACE
SOLID PHASE MICROEXTRACTION
BIOANALYSIS
FOOD
purl_subject.fl_str_mv https://purl.org/becyt/ford/1.4
https://purl.org/becyt/ford/1
dc.description.none.fl_txt_mv Solid-phase microextraction (SPME) has become a powerful sample preparation technique which allows to efficiently isolate and enrich analytes from complex matrixes. One of the most widespread SPME modes, consists of the extraction directly from the headspace (HS) which is equilibrated with the sample. In this sense, HS-SPME provides one of the best platforms for sample preparation, especially for the analysis of volatile and semi-volatile organic compounds. Furthermore, this technique has demonstrated to be versatile, sensitive, robust, and environmentally friendly when applied to samples coming from a diverse variety of fields such as bioanalysis, environmental sciences, food and cultural heritage. Moreover, during last years, the implementation of HS-SPME has dramatically grown along with the need to monitor complex systems over time using in situ and in vivo approaches, taking advantage of its noninvasive nature. In this review article, the authors present the fundamentals of this technique aiming to critically understand its advantages and limitations, highlighting the recent advances published in the last ten years. To this aim, special sections dealing with extractive phase development, technological advances and relevant applications in different fields have been carefully designed. Finally, some thoughts and perspectives about the future of the technique are also discussed.
Fil: Lancioni, Carlina. Universidad Nacional de La Plata. Facultad de Ciencias Exactas. Laboratorio de Investigación y Desarrollo de Métodos Analíticos. - Comisión de Investigaciones Científicas de la Provincia de Buenos Aires. Laboratorio de Investigación y Desarrollo de Métodos Analíticos; Argentina
Fil: Castells, Cecilia Beatriz Marta. Universidad Nacional de La Plata. Facultad de Ciencias Exactas. Laboratorio de Investigación y Desarrollo de Métodos Analíticos. - Comisión de Investigaciones Científicas de la Provincia de Buenos Aires. Laboratorio de Investigación y Desarrollo de Métodos Analíticos; Argentina
Fil: Candal, Roberto Jorge. Universidad Nacional de San Martín. Instituto de Investigación en Ingeniería Ambiental; Argentina. Universidad Nacional de San Martín. Instituto de Investigación e Ingeniería Ambiental. - Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Parque Centenario. Instituto de Investigación e Ingeniería Ambiental; Argentina
Fil: Tascon, Marcos. Universidad Nacional de San Martín. Instituto de Investigación en Ingeniería Ambiental; Argentina. Universidad Nacional de San Martín. Instituto de Investigación e Ingeniería Ambiental. - Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Parque Centenario. Instituto de Investigación e Ingeniería Ambiental; Argentina
description Solid-phase microextraction (SPME) has become a powerful sample preparation technique which allows to efficiently isolate and enrich analytes from complex matrixes. One of the most widespread SPME modes, consists of the extraction directly from the headspace (HS) which is equilibrated with the sample. In this sense, HS-SPME provides one of the best platforms for sample preparation, especially for the analysis of volatile and semi-volatile organic compounds. Furthermore, this technique has demonstrated to be versatile, sensitive, robust, and environmentally friendly when applied to samples coming from a diverse variety of fields such as bioanalysis, environmental sciences, food and cultural heritage. Moreover, during last years, the implementation of HS-SPME has dramatically grown along with the need to monitor complex systems over time using in situ and in vivo approaches, taking advantage of its noninvasive nature. In this review article, the authors present the fundamentals of this technique aiming to critically understand its advantages and limitations, highlighting the recent advances published in the last ten years. To this aim, special sections dealing with extractive phase development, technological advances and relevant applications in different fields have been carefully designed. Finally, some thoughts and perspectives about the future of the technique are also discussed.
publishDate 2022
dc.date.none.fl_str_mv 2022-08
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/203977
Lancioni, Carlina; Castells, Cecilia Beatriz Marta; Candal, Roberto Jorge; Tascon, Marcos; Headspace solid-phase microextraction: Fundamentals and recent advances; Elsevier; Advances in Sample Preparation; 3; 8-2022; 1-15
2772-5820
CONICET Digital
CONICET
url http://hdl.handle.net/11336/203977
identifier_str_mv Lancioni, Carlina; Castells, Cecilia Beatriz Marta; Candal, Roberto Jorge; Tascon, Marcos; Headspace solid-phase microextraction: Fundamentals and recent advances; Elsevier; Advances in Sample Preparation; 3; 8-2022; 1-15
2772-5820
CONICET Digital
CONICET
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/url/https://linkinghub.elsevier.com/retrieve/pii/S2772582022000328
info:eu-repo/semantics/altIdentifier/doi/10.1016/j.sampre.2022.100035
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
application/pdf
application/pdf
application/pdf
dc.publisher.none.fl_str_mv Elsevier
publisher.none.fl_str_mv Elsevier
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
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score 13.070432

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