Porous cordierite-based ceramics processed by starch consolidation casting – Microstructure and high-temperature mechanical behavior

Autores
Sandoval, María Laura; Talou, Mariano H.; Tomba Martinez, Analía G.; Camerucci, M. Andrea; Gregorová, Eva; Pabst, Willi
Año de publicación
2018
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
Porous cordierite-based ceramics with different microstructural features and mechanical behavior were formed by starch consolidation casting (SCC) using native potato and corn starches and sintered at 1275, 1300 and 1330 °C. The composition and microstructure of the ceramic materials were investigated via quantitative phase analysis using X-ray diffraction (with Rietveld refinement), the Archimedes method, mercury porosimetry, scanning electron microscopy and optical microscopy with stereology-based image analysis. The mechanical behavior of samples was evaluated by diametral compression tests at room temperature, 1000 and 1100 °C. The type of starch used and the sintering temperatures were the main factors determining the characteristics of the developed porous microstructures. Materials prepared with corn starch achieved the lowest porosity and the lowest values of mean chord length, mean pore distance and pore throat size. Because of these features, these materials thus presented, in general, higher values of apparent Young´s modulus, elastic limit and mechanical strength than those prepared with potato starch. Despite the presence of a silicate glassy phase, both porous materials, mainly those prepared with corn starch, still enhanced the basic mechanical properties at high temperature, in particular, the mechanical strength and the apparent Young´s modulus due to the special combination of the porous microstructure features.
Fil: Sandoval, María Laura. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Fil: Talou, Mariano H.. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Fil: Tomba Martinez, Analía G.. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Fil: Camerucci, M. Andrea. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Fil: Gregorová, Eva. University of Chemistry and Technology; República Checa
Fil: Pabst, Willi. University of Chemistry and Technology; República Checa
Materia
Cordierite
Porosity
Microstructure-Final
Mechanical Properties
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/45092
Acceder
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oai_identifier_str oai:ri.conicet.gov.ar:11336/45092
network_acronym_str CONICETDig
repository_id_str 3498
network_name_str CONICET Digital (CONICET)
spelling Porous cordierite-based ceramics processed by starch consolidation casting – Microstructure and high-temperature mechanical behaviorSandoval, María LauraTalou, Mariano H.Tomba Martinez, Analía G.Camerucci, M. AndreaGregorová, EvaPabst, WilliCordieritePorosityMicrostructure-FinalMechanical Propertieshttps://purl.org/becyt/ford/2.5https://purl.org/becyt/ford/2https://purl.org/becyt/ford/2.5https://purl.org/becyt/ford/2Porous cordierite-based ceramics with different microstructural features and mechanical behavior were formed by starch consolidation casting (SCC) using native potato and corn starches and sintered at 1275, 1300 and 1330 °C. The composition and microstructure of the ceramic materials were investigated via quantitative phase analysis using X-ray diffraction (with Rietveld refinement), the Archimedes method, mercury porosimetry, scanning electron microscopy and optical microscopy with stereology-based image analysis. The mechanical behavior of samples was evaluated by diametral compression tests at room temperature, 1000 and 1100 °C. The type of starch used and the sintering temperatures were the main factors determining the characteristics of the developed porous microstructures. Materials prepared with corn starch achieved the lowest porosity and the lowest values of mean chord length, mean pore distance and pore throat size. Because of these features, these materials thus presented, in general, higher values of apparent Young´s modulus, elastic limit and mechanical strength than those prepared with potato starch. Despite the presence of a silicate glassy phase, both porous materials, mainly those prepared with corn starch, still enhanced the basic mechanical properties at high temperature, in particular, the mechanical strength and the apparent Young´s modulus due to the special combination of the porous microstructure features.Fil: Sandoval, María Laura. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; ArgentinaFil: Talou, Mariano H.. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; ArgentinaFil: Tomba Martinez, Analía G.. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; ArgentinaFil: Camerucci, M. Andrea. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; ArgentinaFil: Gregorová, Eva. University of Chemistry and Technology; República ChecaFil: Pabst, Willi. University of Chemistry and Technology; República ChecaElsevier2018-03info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/45092Sandoval, María Laura; Talou, Mariano H.; Tomba Martinez, Analía G.; Camerucci, M. Andrea; Gregorová, Eva; et al.; Porous cordierite-based ceramics processed by starch consolidation casting – Microstructure and high-temperature mechanical behavior; Elsevier; Ceramics International; 44; 4; 3-2018; 3893-39030272-8842CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/doi/10.1016/j.ceramint.2017.11.180info:eu-repo/semantics/altIdentifier/url/https://www.sciencedirect.com/science/article/pii/S0272884217326494info:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-nd/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-09-29T09:51:00Zoai:ri.conicet.gov.ar:11336/45092instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-09-29 09:51:01.018CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Porous cordierite-based ceramics processed by starch consolidation casting – Microstructure and high-temperature mechanical behavior
title Porous cordierite-based ceramics processed by starch consolidation casting – Microstructure and high-temperature mechanical behavior
spellingShingle Porous cordierite-based ceramics processed by starch consolidation casting – Microstructure and high-temperature mechanical behavior
Sandoval, María Laura
Cordierite
Porosity
Microstructure-Final
Mechanical Properties
title_short Porous cordierite-based ceramics processed by starch consolidation casting – Microstructure and high-temperature mechanical behavior
title_full Porous cordierite-based ceramics processed by starch consolidation casting – Microstructure and high-temperature mechanical behavior
title_fullStr Porous cordierite-based ceramics processed by starch consolidation casting – Microstructure and high-temperature mechanical behavior
title_full_unstemmed Porous cordierite-based ceramics processed by starch consolidation casting – Microstructure and high-temperature mechanical behavior
title_sort Porous cordierite-based ceramics processed by starch consolidation casting – Microstructure and high-temperature mechanical behavior
dc.creator.none.fl_str_mv Sandoval, María Laura
Talou, Mariano H.
Tomba Martinez, Analía G.
Camerucci, M. Andrea
Gregorová, Eva
Pabst, Willi
author Sandoval, María Laura
author_facet Sandoval, María Laura
Talou, Mariano H.
Tomba Martinez, Analía G.
Camerucci, M. Andrea
Gregorová, Eva
Pabst, Willi
author_role author
author2 Talou, Mariano H.
Tomba Martinez, Analía G.
Camerucci, M. Andrea
Gregorová, Eva
Pabst, Willi
author2_role author
author
author
author
author
dc.subject.none.fl_str_mv Cordierite
Porosity
Microstructure-Final
Mechanical Properties
topic Cordierite
Porosity
Microstructure-Final
Mechanical Properties
purl_subject.fl_str_mv https://purl.org/becyt/ford/2.5
https://purl.org/becyt/ford/2
https://purl.org/becyt/ford/2.5
https://purl.org/becyt/ford/2
dc.description.none.fl_txt_mv Porous cordierite-based ceramics with different microstructural features and mechanical behavior were formed by starch consolidation casting (SCC) using native potato and corn starches and sintered at 1275, 1300 and 1330 °C. The composition and microstructure of the ceramic materials were investigated via quantitative phase analysis using X-ray diffraction (with Rietveld refinement), the Archimedes method, mercury porosimetry, scanning electron microscopy and optical microscopy with stereology-based image analysis. The mechanical behavior of samples was evaluated by diametral compression tests at room temperature, 1000 and 1100 °C. The type of starch used and the sintering temperatures were the main factors determining the characteristics of the developed porous microstructures. Materials prepared with corn starch achieved the lowest porosity and the lowest values of mean chord length, mean pore distance and pore throat size. Because of these features, these materials thus presented, in general, higher values of apparent Young´s modulus, elastic limit and mechanical strength than those prepared with potato starch. Despite the presence of a silicate glassy phase, both porous materials, mainly those prepared with corn starch, still enhanced the basic mechanical properties at high temperature, in particular, the mechanical strength and the apparent Young´s modulus due to the special combination of the porous microstructure features.
Fil: Sandoval, María Laura. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Fil: Talou, Mariano H.. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Fil: Tomba Martinez, Analía G.. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Fil: Camerucci, M. Andrea. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Fil: Gregorová, Eva. University of Chemistry and Technology; República Checa
Fil: Pabst, Willi. University of Chemistry and Technology; República Checa
description Porous cordierite-based ceramics with different microstructural features and mechanical behavior were formed by starch consolidation casting (SCC) using native potato and corn starches and sintered at 1275, 1300 and 1330 °C. The composition and microstructure of the ceramic materials were investigated via quantitative phase analysis using X-ray diffraction (with Rietveld refinement), the Archimedes method, mercury porosimetry, scanning electron microscopy and optical microscopy with stereology-based image analysis. The mechanical behavior of samples was evaluated by diametral compression tests at room temperature, 1000 and 1100 °C. The type of starch used and the sintering temperatures were the main factors determining the characteristics of the developed porous microstructures. Materials prepared with corn starch achieved the lowest porosity and the lowest values of mean chord length, mean pore distance and pore throat size. Because of these features, these materials thus presented, in general, higher values of apparent Young´s modulus, elastic limit and mechanical strength than those prepared with potato starch. Despite the presence of a silicate glassy phase, both porous materials, mainly those prepared with corn starch, still enhanced the basic mechanical properties at high temperature, in particular, the mechanical strength and the apparent Young´s modulus due to the special combination of the porous microstructure features.
publishDate 2018
dc.date.none.fl_str_mv 2018-03
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/45092
Sandoval, María Laura; Talou, Mariano H.; Tomba Martinez, Analía G.; Camerucci, M. Andrea; Gregorová, Eva; et al.; Porous cordierite-based ceramics processed by starch consolidation casting – Microstructure and high-temperature mechanical behavior; Elsevier; Ceramics International; 44; 4; 3-2018; 3893-3903
0272-8842
CONICET Digital
CONICET
url http://hdl.handle.net/11336/45092
identifier_str_mv Sandoval, María Laura; Talou, Mariano H.; Tomba Martinez, Analía G.; Camerucci, M. Andrea; Gregorová, Eva; et al.; Porous cordierite-based ceramics processed by starch consolidation casting – Microstructure and high-temperature mechanical behavior; Elsevier; Ceramics International; 44; 4; 3-2018; 3893-3903
0272-8842
CONICET Digital
CONICET
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/doi/10.1016/j.ceramint.2017.11.180
info:eu-repo/semantics/altIdentifier/url/https://www.sciencedirect.com/science/article/pii/S0272884217326494
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
dc.publisher.none.fl_str_mv Elsevier
publisher.none.fl_str_mv Elsevier
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
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score 13.070432

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