Influence of microstructure on the corrosion behavior of nitrocarburized AISI H13 tool steel obtained by pulsed DC plasma

Autores
Basso, R. L. O.; Candal, Roberto Jorge; Figueroa, C. A.; Wisnivesky, D.; Alvarez, F.
Año de publicación
2009
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
The influence of microstructure on the corrosion behavior of pulsed plasma nitrocarburized AISI H13 tool steel in NaCl 0.9 wt/V % solution is reported. The samples were prepared with different nitrocarburizing treatment times using a constant [CH4/H2 + N2] gaseous mixture by a DC pulsed plasma system. The microstructure of the nitrocarburized layers was analyzed by scanning electron microscopy (SEM), X-ray photoelectron spectroscopy (XPS) and X-ray diffraction. The corrosion behavior was evaluated by potentiodynamic polarization experiments. The nitrocarburizing process considerably improves the corrosion resistance of the material in a NaCl environment as compared to the untreated H13 steel. The modified surface layer mainly consisting of ε-Fe2-3(C,N) and γ′-Fe4N phases confers this outstanding behavior. The corrosion resistance dependence on specific nitrocarburizing processes is reported and the role of the surface porosity is discussed.
Fil: Basso, R. L. O.. Universidade Estadual de Campinas; Brasil
Fil: Candal, Roberto Jorge. Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Ciudad Universitaria. Instituto de Química, Física de los Materiales, Medioambiente y Energía. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales. Instituto de Química, Física de los Materiales, Medioambiente y Energía; Argentina
Fil: Figueroa, C. A.. Universidade Estadual de Campinas; Brasil
Fil: Wisnivesky, D.. Universidade Estadual de Campinas; Brasil
Fil: Alvarez, F.. Universidade Estadual de Campinas; Brasil
Materia
Plasma Nitrocarburizing
Porosity Analysis
Steel Corrosion
Surface Porosity
Tool Steel
X-Ray Diffraction
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/75274
Acceder
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oai_identifier_str oai:ri.conicet.gov.ar:11336/75274
network_acronym_str CONICETDig
repository_id_str 3498
network_name_str CONICET Digital (CONICET)
spelling Influence of microstructure on the corrosion behavior of nitrocarburized AISI H13 tool steel obtained by pulsed DC plasmaBasso, R. L. O.Candal, Roberto JorgeFigueroa, C. A.Wisnivesky, D.Alvarez, F.Plasma NitrocarburizingPorosity AnalysisSteel CorrosionSurface PorosityTool SteelX-Ray Diffractionhttps://purl.org/becyt/ford/1.4https://purl.org/becyt/ford/1The influence of microstructure on the corrosion behavior of pulsed plasma nitrocarburized AISI H13 tool steel in NaCl 0.9 wt/V % solution is reported. The samples were prepared with different nitrocarburizing treatment times using a constant [CH4/H2 + N2] gaseous mixture by a DC pulsed plasma system. The microstructure of the nitrocarburized layers was analyzed by scanning electron microscopy (SEM), X-ray photoelectron spectroscopy (XPS) and X-ray diffraction. The corrosion behavior was evaluated by potentiodynamic polarization experiments. The nitrocarburizing process considerably improves the corrosion resistance of the material in a NaCl environment as compared to the untreated H13 steel. The modified surface layer mainly consisting of ε-Fe2-3(C,N) and γ′-Fe4N phases confers this outstanding behavior. The corrosion resistance dependence on specific nitrocarburizing processes is reported and the role of the surface porosity is discussed.Fil: Basso, R. L. O.. Universidade Estadual de Campinas; BrasilFil: Candal, Roberto Jorge. Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Ciudad Universitaria. Instituto de Química, Física de los Materiales, Medioambiente y Energía. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales. Instituto de Química, Física de los Materiales, Medioambiente y Energía; ArgentinaFil: Figueroa, C. A.. Universidade Estadual de Campinas; BrasilFil: Wisnivesky, D.. Universidade Estadual de Campinas; BrasilFil: Alvarez, F.. Universidade Estadual de Campinas; BrasilElsevier Science Sa2009-02info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/75274Basso, R. L. O.; Candal, Roberto Jorge; Figueroa, C. A.; Wisnivesky, D.; Alvarez, F.; Influence of microstructure on the corrosion behavior of nitrocarburized AISI H13 tool steel obtained by pulsed DC plasma; Elsevier Science Sa; Surface and Coatings Technology; 203; 10-11; 2-2009; 1293-12970257-8972CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/doi/10.1016/j.surfcoat.2008.10.006info:eu-repo/semantics/altIdentifier/url/https://www.sciencedirect.com/science/article/pii/S0257897208009687info:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-nd/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-09-29T09:35:24Zoai:ri.conicet.gov.ar:11336/75274instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-09-29 09:35:25.03CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Influence of microstructure on the corrosion behavior of nitrocarburized AISI H13 tool steel obtained by pulsed DC plasma
title Influence of microstructure on the corrosion behavior of nitrocarburized AISI H13 tool steel obtained by pulsed DC plasma
spellingShingle Influence of microstructure on the corrosion behavior of nitrocarburized AISI H13 tool steel obtained by pulsed DC plasma
Basso, R. L. O.
Plasma Nitrocarburizing
Porosity Analysis
Steel Corrosion
Surface Porosity
Tool Steel
X-Ray Diffraction
title_short Influence of microstructure on the corrosion behavior of nitrocarburized AISI H13 tool steel obtained by pulsed DC plasma
title_full Influence of microstructure on the corrosion behavior of nitrocarburized AISI H13 tool steel obtained by pulsed DC plasma
title_fullStr Influence of microstructure on the corrosion behavior of nitrocarburized AISI H13 tool steel obtained by pulsed DC plasma
title_full_unstemmed Influence of microstructure on the corrosion behavior of nitrocarburized AISI H13 tool steel obtained by pulsed DC plasma
title_sort Influence of microstructure on the corrosion behavior of nitrocarburized AISI H13 tool steel obtained by pulsed DC plasma
dc.creator.none.fl_str_mv Basso, R. L. O.
Candal, Roberto Jorge
Figueroa, C. A.
Wisnivesky, D.
Alvarez, F.
author Basso, R. L. O.
author_facet Basso, R. L. O.
Candal, Roberto Jorge
Figueroa, C. A.
Wisnivesky, D.
Alvarez, F.
author_role author
author2 Candal, Roberto Jorge
Figueroa, C. A.
Wisnivesky, D.
Alvarez, F.
author2_role author
author
author
author
dc.subject.none.fl_str_mv Plasma Nitrocarburizing
Porosity Analysis
Steel Corrosion
Surface Porosity
Tool Steel
X-Ray Diffraction
topic Plasma Nitrocarburizing
Porosity Analysis
Steel Corrosion
Surface Porosity
Tool Steel
X-Ray Diffraction
purl_subject.fl_str_mv https://purl.org/becyt/ford/1.4
https://purl.org/becyt/ford/1
dc.description.none.fl_txt_mv The influence of microstructure on the corrosion behavior of pulsed plasma nitrocarburized AISI H13 tool steel in NaCl 0.9 wt/V % solution is reported. The samples were prepared with different nitrocarburizing treatment times using a constant [CH4/H2 + N2] gaseous mixture by a DC pulsed plasma system. The microstructure of the nitrocarburized layers was analyzed by scanning electron microscopy (SEM), X-ray photoelectron spectroscopy (XPS) and X-ray diffraction. The corrosion behavior was evaluated by potentiodynamic polarization experiments. The nitrocarburizing process considerably improves the corrosion resistance of the material in a NaCl environment as compared to the untreated H13 steel. The modified surface layer mainly consisting of ε-Fe2-3(C,N) and γ′-Fe4N phases confers this outstanding behavior. The corrosion resistance dependence on specific nitrocarburizing processes is reported and the role of the surface porosity is discussed.
Fil: Basso, R. L. O.. Universidade Estadual de Campinas; Brasil
Fil: Candal, Roberto Jorge. Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Ciudad Universitaria. Instituto de Química, Física de los Materiales, Medioambiente y Energía. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales. Instituto de Química, Física de los Materiales, Medioambiente y Energía; Argentina
Fil: Figueroa, C. A.. Universidade Estadual de Campinas; Brasil
Fil: Wisnivesky, D.. Universidade Estadual de Campinas; Brasil
Fil: Alvarez, F.. Universidade Estadual de Campinas; Brasil
description The influence of microstructure on the corrosion behavior of pulsed plasma nitrocarburized AISI H13 tool steel in NaCl 0.9 wt/V % solution is reported. The samples were prepared with different nitrocarburizing treatment times using a constant [CH4/H2 + N2] gaseous mixture by a DC pulsed plasma system. The microstructure of the nitrocarburized layers was analyzed by scanning electron microscopy (SEM), X-ray photoelectron spectroscopy (XPS) and X-ray diffraction. The corrosion behavior was evaluated by potentiodynamic polarization experiments. The nitrocarburizing process considerably improves the corrosion resistance of the material in a NaCl environment as compared to the untreated H13 steel. The modified surface layer mainly consisting of ε-Fe2-3(C,N) and γ′-Fe4N phases confers this outstanding behavior. The corrosion resistance dependence on specific nitrocarburizing processes is reported and the role of the surface porosity is discussed.
publishDate 2009
dc.date.none.fl_str_mv 2009-02
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/75274
Basso, R. L. O.; Candal, Roberto Jorge; Figueroa, C. A.; Wisnivesky, D.; Alvarez, F.; Influence of microstructure on the corrosion behavior of nitrocarburized AISI H13 tool steel obtained by pulsed DC plasma; Elsevier Science Sa; Surface and Coatings Technology; 203; 10-11; 2-2009; 1293-1297
0257-8972
CONICET Digital
CONICET
url http://hdl.handle.net/11336/75274
identifier_str_mv Basso, R. L. O.; Candal, Roberto Jorge; Figueroa, C. A.; Wisnivesky, D.; Alvarez, F.; Influence of microstructure on the corrosion behavior of nitrocarburized AISI H13 tool steel obtained by pulsed DC plasma; Elsevier Science Sa; Surface and Coatings Technology; 203; 10-11; 2-2009; 1293-1297
0257-8972
CONICET Digital
CONICET
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/doi/10.1016/j.surfcoat.2008.10.006
info:eu-repo/semantics/altIdentifier/url/https://www.sciencedirect.com/science/article/pii/S0257897208009687
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
dc.publisher.none.fl_str_mv Elsevier Science Sa
publisher.none.fl_str_mv Elsevier Science Sa
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
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score 13.070432

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