Operation of a Batch Stripping Distillation Column

Autores
Xu, Sonling; Espinosa, Hector Jose Maria; Salomone, Hector Enrique; Iribarren, Oscar Alberto
Año de publicación
2001
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
Batch process is becoming more popular as chemical process industries move toward manufacturing fine and specialty chemicals, where flexibility is a key issue due to the frequent change of product demand[ 1 ]. Batch distillation columns are inherently flexible, as a single column can separate many different components from a multicomponent feed. Thus the use of batch distillation is becoming more important for the seperation and purification of high-value chemicals in many chemical, food, and pharmaceutical industries.      Traditionally, the most popular kind of batch distillation column is the so-called rectifying column, which has a large reboiler, to which all the feed is charged, and different products are removed from the top. There are three ways to operate a rectifying column[ 2,3 ]. They are: (1) constant reflux and variable distillate composition,  (2) variable reflux and constant distillate composition of key component, (3) optimal reflux policy which trades off (1) and (2) and is based on  the most profitable operation. Batch stripping column is opposed to a batch rectifier. It has its storage vessel at the top and the products leave the column at the bottom. A stripping batch distillation column is preferred when the amount of the light component in the feed is small and the products are to be recovered at high purity[ 4,5 ] .    The operation modes of a batch stripping are believed to be the same as those of a rectifier. However, the control system of  a  stripper is different. In this paper, we explore three different control methods with Hysys (Hyprotech Ltd. 1997) for a batch stripper. The control schemes are  shown in Fig. 1. The  main difference is the control scheme for reboiler liquid level: (a) controlled by reflux flow, (b) controlled by reboiler heat duty, (c)  controlled by bottom product flow. The main characterics of operating a batch stripper with different control scheme are presented in this paper. Guidlines are provided for the startup and the effect of some control tuning parameters on the column performance are discussed.
Fil: Xu, Sonling. Tianjing University; China
Fil: Espinosa, Hector Jose Maria. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Santa Fe. Instituto de Desarrollo y Diseño. Universidad Tecnológica Nacional. Facultad Regional Santa Fe. Instituto de Desarrollo y Diseño; Argentina
Fil: Salomone, Hector Enrique. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Santa Fe. Instituto de Desarrollo y Diseño. Universidad Tecnológica Nacional. Facultad Regional Santa Fe. Instituto de Desarrollo y Diseño; Argentina
Fil: Iribarren, Oscar Alberto. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Santa Fe. Instituto de Desarrollo y Diseño. Universidad Tecnológica Nacional. Facultad Regional Santa Fe. Instituto de Desarrollo y Diseño; Argentina
Materia
BATCH
STRIPPER
CONTROL
OPERATION
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/186529

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spelling Operation of a Batch Stripping Distillation ColumnXu, SonlingEspinosa, Hector Jose MariaSalomone, Hector EnriqueIribarren, Oscar AlbertoBATCHSTRIPPERCONTROLOPERATIONhttps://purl.org/becyt/ford/2.4https://purl.org/becyt/ford/2Batch process is becoming more popular as chemical process industries move toward manufacturing fine and specialty chemicals, where flexibility is a key issue due to the frequent change of product demand[ 1 ]. Batch distillation columns are inherently flexible, as a single column can separate many different components from a multicomponent feed. Thus the use of batch distillation is becoming more important for the seperation and purification of high-value chemicals in many chemical, food, and pharmaceutical industries.      Traditionally, the most popular kind of batch distillation column is the so-called rectifying column, which has a large reboiler, to which all the feed is charged, and different products are removed from the top. There are three ways to operate a rectifying column[ 2,3 ]. They are: (1) constant reflux and variable distillate composition,  (2) variable reflux and constant distillate composition of key component, (3) optimal reflux policy which trades off (1) and (2) and is based on  the most profitable operation. Batch stripping column is opposed to a batch rectifier. It has its storage vessel at the top and the products leave the column at the bottom. A stripping batch distillation column is preferred when the amount of the light component in the feed is small and the products are to be recovered at high purity[ 4,5 ] .    The operation modes of a batch stripping are believed to be the same as those of a rectifier. However, the control system of  a  stripper is different. In this paper, we explore three different control methods with Hysys (Hyprotech Ltd. 1997) for a batch stripper. The control schemes are  shown in Fig. 1. The  main difference is the control scheme for reboiler liquid level: (a) controlled by reflux flow, (b) controlled by reboiler heat duty, (c)  controlled by bottom product flow. The main characterics of operating a batch stripper with different control scheme are presented in this paper. Guidlines are provided for the startup and the effect of some control tuning parameters on the column performance are discussed.Fil: Xu, Sonling. Tianjing University; ChinaFil: Espinosa, Hector Jose Maria. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Santa Fe. Instituto de Desarrollo y Diseño. Universidad Tecnológica Nacional. Facultad Regional Santa Fe. Instituto de Desarrollo y Diseño; ArgentinaFil: Salomone, Hector Enrique. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Santa Fe. Instituto de Desarrollo y Diseño. Universidad Tecnológica Nacional. Facultad Regional Santa Fe. Instituto de Desarrollo y Diseño; ArgentinaFil: Iribarren, Oscar Alberto. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Santa Fe. Instituto de Desarrollo y Diseño. Universidad Tecnológica Nacional. Facultad Regional Santa Fe. Instituto de Desarrollo y Diseño; ArgentinaElsevier2001-12info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/186529Xu, Sonling; Espinosa, Hector Jose Maria; Salomone, Hector Enrique; Iribarren, Oscar Alberto; Operation of a Batch Stripping Distillation Column; Elsevier; Chinese Journal Of Chemical Engineering; 9; 2; 12-2001; 141-1441004-9541CONICET DigitalCONICETenginfo:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-sa/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-09-03T09:59:34Zoai:ri.conicet.gov.ar:11336/186529instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-09-03 09:59:34.428CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Operation of a Batch Stripping Distillation Column
title Operation of a Batch Stripping Distillation Column
spellingShingle Operation of a Batch Stripping Distillation Column
Xu, Sonling
BATCH
STRIPPER
CONTROL
OPERATION
title_short Operation of a Batch Stripping Distillation Column
title_full Operation of a Batch Stripping Distillation Column
title_fullStr Operation of a Batch Stripping Distillation Column
title_full_unstemmed Operation of a Batch Stripping Distillation Column
title_sort Operation of a Batch Stripping Distillation Column
dc.creator.none.fl_str_mv Xu, Sonling
Espinosa, Hector Jose Maria
Salomone, Hector Enrique
Iribarren, Oscar Alberto
author Xu, Sonling
author_facet Xu, Sonling
Espinosa, Hector Jose Maria
Salomone, Hector Enrique
Iribarren, Oscar Alberto
author_role author
author2 Espinosa, Hector Jose Maria
Salomone, Hector Enrique
Iribarren, Oscar Alberto
author2_role author
author
author
dc.subject.none.fl_str_mv BATCH
STRIPPER
CONTROL
OPERATION
topic BATCH
STRIPPER
CONTROL
OPERATION
purl_subject.fl_str_mv https://purl.org/becyt/ford/2.4
https://purl.org/becyt/ford/2
dc.description.none.fl_txt_mv Batch process is becoming more popular as chemical process industries move toward manufacturing fine and specialty chemicals, where flexibility is a key issue due to the frequent change of product demand[ 1 ]. Batch distillation columns are inherently flexible, as a single column can separate many different components from a multicomponent feed. Thus the use of batch distillation is becoming more important for the seperation and purification of high-value chemicals in many chemical, food, and pharmaceutical industries.      Traditionally, the most popular kind of batch distillation column is the so-called rectifying column, which has a large reboiler, to which all the feed is charged, and different products are removed from the top. There are three ways to operate a rectifying column[ 2,3 ]. They are: (1) constant reflux and variable distillate composition,  (2) variable reflux and constant distillate composition of key component, (3) optimal reflux policy which trades off (1) and (2) and is based on  the most profitable operation. Batch stripping column is opposed to a batch rectifier. It has its storage vessel at the top and the products leave the column at the bottom. A stripping batch distillation column is preferred when the amount of the light component in the feed is small and the products are to be recovered at high purity[ 4,5 ] .    The operation modes of a batch stripping are believed to be the same as those of a rectifier. However, the control system of  a  stripper is different. In this paper, we explore three different control methods with Hysys (Hyprotech Ltd. 1997) for a batch stripper. The control schemes are  shown in Fig. 1. The  main difference is the control scheme for reboiler liquid level: (a) controlled by reflux flow, (b) controlled by reboiler heat duty, (c)  controlled by bottom product flow. The main characterics of operating a batch stripper with different control scheme are presented in this paper. Guidlines are provided for the startup and the effect of some control tuning parameters on the column performance are discussed.
Fil: Xu, Sonling. Tianjing University; China
Fil: Espinosa, Hector Jose Maria. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Santa Fe. Instituto de Desarrollo y Diseño. Universidad Tecnológica Nacional. Facultad Regional Santa Fe. Instituto de Desarrollo y Diseño; Argentina
Fil: Salomone, Hector Enrique. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Santa Fe. Instituto de Desarrollo y Diseño. Universidad Tecnológica Nacional. Facultad Regional Santa Fe. Instituto de Desarrollo y Diseño; Argentina
Fil: Iribarren, Oscar Alberto. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Santa Fe. Instituto de Desarrollo y Diseño. Universidad Tecnológica Nacional. Facultad Regional Santa Fe. Instituto de Desarrollo y Diseño; Argentina
description Batch process is becoming more popular as chemical process industries move toward manufacturing fine and specialty chemicals, where flexibility is a key issue due to the frequent change of product demand[ 1 ]. Batch distillation columns are inherently flexible, as a single column can separate many different components from a multicomponent feed. Thus the use of batch distillation is becoming more important for the seperation and purification of high-value chemicals in many chemical, food, and pharmaceutical industries.      Traditionally, the most popular kind of batch distillation column is the so-called rectifying column, which has a large reboiler, to which all the feed is charged, and different products are removed from the top. There are three ways to operate a rectifying column[ 2,3 ]. They are: (1) constant reflux and variable distillate composition,  (2) variable reflux and constant distillate composition of key component, (3) optimal reflux policy which trades off (1) and (2) and is based on  the most profitable operation. Batch stripping column is opposed to a batch rectifier. It has its storage vessel at the top and the products leave the column at the bottom. A stripping batch distillation column is preferred when the amount of the light component in the feed is small and the products are to be recovered at high purity[ 4,5 ] .    The operation modes of a batch stripping are believed to be the same as those of a rectifier. However, the control system of  a  stripper is different. In this paper, we explore three different control methods with Hysys (Hyprotech Ltd. 1997) for a batch stripper. The control schemes are  shown in Fig. 1. The  main difference is the control scheme for reboiler liquid level: (a) controlled by reflux flow, (b) controlled by reboiler heat duty, (c)  controlled by bottom product flow. The main characterics of operating a batch stripper with different control scheme are presented in this paper. Guidlines are provided for the startup and the effect of some control tuning parameters on the column performance are discussed.
publishDate 2001
dc.date.none.fl_str_mv 2001-12
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/186529
Xu, Sonling; Espinosa, Hector Jose Maria; Salomone, Hector Enrique; Iribarren, Oscar Alberto; Operation of a Batch Stripping Distillation Column; Elsevier; Chinese Journal Of Chemical Engineering; 9; 2; 12-2001; 141-144
1004-9541
CONICET Digital
CONICET
url http://hdl.handle.net/11336/186529
identifier_str_mv Xu, Sonling; Espinosa, Hector Jose Maria; Salomone, Hector Enrique; Iribarren, Oscar Alberto; Operation of a Batch Stripping Distillation Column; Elsevier; Chinese Journal Of Chemical Engineering; 9; 2; 12-2001; 141-144
1004-9541
CONICET Digital
CONICET
dc.language.none.fl_str_mv eng
language eng
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
application/pdf
dc.publisher.none.fl_str_mv Elsevier
publisher.none.fl_str_mv Elsevier
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
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instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
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