Protocol for the preparation of TiO2-modified boron-doped diamond photoelectrode via electrophoretic deposition and its photoelectrochemical study

Autores
Quilumbaquin Orbe, Wendy Karina; Castillo Cabrera, G. Xavier; Borrero González, Luis J.; Espinoza Montero, Patricio J.
Año de publicación
2024
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
Electrophoretic deposition is a straightforward method for synthesizing high-quality photoanodes. We present a protocol for synthesizing a TiO2-modified boron-doped diamond photoanode (BDD/TiO2) via electrophoretic deposition, detailing the chemical and electrochemical treatments applied to the bare BDD electrode prior to use. We provide a step-by-step guide for performing photoelectrochemical characterization under both dark and light conditions and describe an optical technique for investigating band-gap energy. For complete details on the use and execution of this protocol, please refer to Quilumbaquin et al.1.
Fil: Quilumbaquin Orbe, Wendy Karina. Pontificia Universidad Catolica del Ecuador. Facultad de Cs Exactas y Naturales; Ecuador. Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Houssay. Instituto de Bioquímica y Medicina Molecular. Universidad de Buenos Aires. Facultad Medicina. Instituto de Bioquímica y Medicina Molecular; Argentina
Fil: Castillo Cabrera, G. Xavier. Pontificia Universidad Catolica del Ecuador. Facultad de Cs Exactas y Naturales; Ecuador
Fil: Borrero González, Luis J.. Pontificia Universidad Catolica del Ecuador. Facultad de Cs Exactas y Naturales; Ecuador
Fil: Espinoza Montero, Patricio J.. Pontificia Universidad Catolica del Ecuador. Facultad de Cs Exactas y Naturales; Ecuador
Materia
Material sciences
BDD
Chemistry
Environmental sciences
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/261560
Acceder
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network_name_str CONICET Digital (CONICET)
spelling Protocol for the preparation of TiO2-modified boron-doped diamond photoelectrode via electrophoretic deposition and its photoelectrochemical studyQuilumbaquin Orbe, Wendy KarinaCastillo Cabrera, G. XavierBorrero González, Luis J.Espinoza Montero, Patricio J.Material sciencesBDDChemistryEnvironmental scienceshttps://purl.org/becyt/ford/1.4https://purl.org/becyt/ford/1Electrophoretic deposition is a straightforward method for synthesizing high-quality photoanodes. We present a protocol for synthesizing a TiO2-modified boron-doped diamond photoanode (BDD/TiO2) via electrophoretic deposition, detailing the chemical and electrochemical treatments applied to the bare BDD electrode prior to use. We provide a step-by-step guide for performing photoelectrochemical characterization under both dark and light conditions and describe an optical technique for investigating band-gap energy. For complete details on the use and execution of this protocol, please refer to Quilumbaquin et al.1.Fil: Quilumbaquin Orbe, Wendy Karina. Pontificia Universidad Catolica del Ecuador. Facultad de Cs Exactas y Naturales; Ecuador. Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Houssay. Instituto de Bioquímica y Medicina Molecular. Universidad de Buenos Aires. Facultad Medicina. Instituto de Bioquímica y Medicina Molecular; ArgentinaFil: Castillo Cabrera, G. Xavier. Pontificia Universidad Catolica del Ecuador. Facultad de Cs Exactas y Naturales; EcuadorFil: Borrero González, Luis J.. Pontificia Universidad Catolica del Ecuador. Facultad de Cs Exactas y Naturales; EcuadorFil: Espinoza Montero, Patricio J.. Pontificia Universidad Catolica del Ecuador. Facultad de Cs Exactas y Naturales; EcuadorCell Press2024-09info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/261560Quilumbaquin Orbe, Wendy Karina; Castillo Cabrera, G. Xavier; Borrero González, Luis J.; Espinoza Montero, Patricio J.; Protocol for the preparation of TiO2-modified boron-doped diamond photoelectrode via electrophoretic deposition and its photoelectrochemical study; Cell Press; STAR Protocols; 5; 3; 9-2024; 1-142666-1667CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/url/https://linkinghub.elsevier.com/retrieve/pii/S2666166724004246info:eu-repo/semantics/altIdentifier/doi/10.1016/j.xpro.2024.103259info:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-09-29T09:52:49Zoai:ri.conicet.gov.ar:11336/261560instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-09-29 09:52:49.951CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Protocol for the preparation of TiO2-modified boron-doped diamond photoelectrode via electrophoretic deposition and its photoelectrochemical study
title Protocol for the preparation of TiO2-modified boron-doped diamond photoelectrode via electrophoretic deposition and its photoelectrochemical study
spellingShingle Protocol for the preparation of TiO2-modified boron-doped diamond photoelectrode via electrophoretic deposition and its photoelectrochemical study
Quilumbaquin Orbe, Wendy Karina
Material sciences
BDD
Chemistry
Environmental sciences
title_short Protocol for the preparation of TiO2-modified boron-doped diamond photoelectrode via electrophoretic deposition and its photoelectrochemical study
title_full Protocol for the preparation of TiO2-modified boron-doped diamond photoelectrode via electrophoretic deposition and its photoelectrochemical study
title_fullStr Protocol for the preparation of TiO2-modified boron-doped diamond photoelectrode via electrophoretic deposition and its photoelectrochemical study
title_full_unstemmed Protocol for the preparation of TiO2-modified boron-doped diamond photoelectrode via electrophoretic deposition and its photoelectrochemical study
title_sort Protocol for the preparation of TiO2-modified boron-doped diamond photoelectrode via electrophoretic deposition and its photoelectrochemical study
dc.creator.none.fl_str_mv Quilumbaquin Orbe, Wendy Karina
Castillo Cabrera, G. Xavier
Borrero González, Luis J.
Espinoza Montero, Patricio J.
author Quilumbaquin Orbe, Wendy Karina
author_facet Quilumbaquin Orbe, Wendy Karina
Castillo Cabrera, G. Xavier
Borrero González, Luis J.
Espinoza Montero, Patricio J.
author_role author
author2 Castillo Cabrera, G. Xavier
Borrero González, Luis J.
Espinoza Montero, Patricio J.
author2_role author
author
author
dc.subject.none.fl_str_mv Material sciences
BDD
Chemistry
Environmental sciences
topic Material sciences
BDD
Chemistry
Environmental sciences
purl_subject.fl_str_mv https://purl.org/becyt/ford/1.4
https://purl.org/becyt/ford/1
dc.description.none.fl_txt_mv Electrophoretic deposition is a straightforward method for synthesizing high-quality photoanodes. We present a protocol for synthesizing a TiO2-modified boron-doped diamond photoanode (BDD/TiO2) via electrophoretic deposition, detailing the chemical and electrochemical treatments applied to the bare BDD electrode prior to use. We provide a step-by-step guide for performing photoelectrochemical characterization under both dark and light conditions and describe an optical technique for investigating band-gap energy. For complete details on the use and execution of this protocol, please refer to Quilumbaquin et al.1.
Fil: Quilumbaquin Orbe, Wendy Karina. Pontificia Universidad Catolica del Ecuador. Facultad de Cs Exactas y Naturales; Ecuador. Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Houssay. Instituto de Bioquímica y Medicina Molecular. Universidad de Buenos Aires. Facultad Medicina. Instituto de Bioquímica y Medicina Molecular; Argentina
Fil: Castillo Cabrera, G. Xavier. Pontificia Universidad Catolica del Ecuador. Facultad de Cs Exactas y Naturales; Ecuador
Fil: Borrero González, Luis J.. Pontificia Universidad Catolica del Ecuador. Facultad de Cs Exactas y Naturales; Ecuador
Fil: Espinoza Montero, Patricio J.. Pontificia Universidad Catolica del Ecuador. Facultad de Cs Exactas y Naturales; Ecuador
description Electrophoretic deposition is a straightforward method for synthesizing high-quality photoanodes. We present a protocol for synthesizing a TiO2-modified boron-doped diamond photoanode (BDD/TiO2) via electrophoretic deposition, detailing the chemical and electrochemical treatments applied to the bare BDD electrode prior to use. We provide a step-by-step guide for performing photoelectrochemical characterization under both dark and light conditions and describe an optical technique for investigating band-gap energy. For complete details on the use and execution of this protocol, please refer to Quilumbaquin et al.1.
publishDate 2024
dc.date.none.fl_str_mv 2024-09
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/261560
Quilumbaquin Orbe, Wendy Karina; Castillo Cabrera, G. Xavier; Borrero González, Luis J.; Espinoza Montero, Patricio J.; Protocol for the preparation of TiO2-modified boron-doped diamond photoelectrode via electrophoretic deposition and its photoelectrochemical study; Cell Press; STAR Protocols; 5; 3; 9-2024; 1-14
2666-1667
CONICET Digital
CONICET
url http://hdl.handle.net/11336/261560
identifier_str_mv Quilumbaquin Orbe, Wendy Karina; Castillo Cabrera, G. Xavier; Borrero González, Luis J.; Espinoza Montero, Patricio J.; Protocol for the preparation of TiO2-modified boron-doped diamond photoelectrode via electrophoretic deposition and its photoelectrochemical study; Cell Press; STAR Protocols; 5; 3; 9-2024; 1-14
2666-1667
CONICET Digital
CONICET
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/url/https://linkinghub.elsevier.com/retrieve/pii/S2666166724004246
info:eu-repo/semantics/altIdentifier/doi/10.1016/j.xpro.2024.103259
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
dc.publisher.none.fl_str_mv Cell Press
publisher.none.fl_str_mv Cell Press
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
_version_ 1844613618238226432
score 13.070432

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