Synthesis and characterisation of mesoporous silicate nanoparticles for use as nanobiocatalysts
- Autores
- Bujedo, Agustín Anibal; Perillo, Maria Angelica; Burgos, Martha Ines
- Año de publicación
- 2023
- Idioma
- inglés
- Tipo de recurso
- documento de conferencia
- Estado
- versión publicada
- Descripción
- Nano-biocatalysts are defined as those nanoparticles (NPs) that are capable of entrapping enzymes, transporting them and ultimately allowing catalysis to occur within the nanopores or releasing the enzyme in a controlled manner at the target site. NPs have the ability to interact with cells and tissues at the molecular level. It has been proposed that encapsulation in nanocarriers protects the bioactive components from unfavourable environmental conditions and also increases their solubility and bioavailability. We have synthesised mesoporous silicate nanoparticles using the method described by Nandiyanto et al1. It uses polystyrene as a template for the mesoporous structure and a surfactant and hydrocarbon solvent to control particle size. Different synthesis conditions were tested and the structural characteristics such as NP diameter and specific surface area (SSA) were analysed by SEM microscopy and dynamic vapour sorption, respectively. It was observed that NPs ranging from 52 to 98 nm were obtained and the SSA is compatible with mesoporous materials (194 m2 /g). Adsorption of the enzyme b-galactosidase from Kluyveromyces lactis was achieved at 48%. The chemical composition was analysed by EDS and mainly SO2 materials were observed.
Fil: Bujedo, Agustín Anibal. Universidad Nacional de Córdoba. Facultad de Ciencias Exactas, Físicas y Naturales. Departamento de Química. Cátedra de Química Biológica; Argentina
Fil: Perillo, Maria Angelica. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Instituto de Investigaciones Biológicas y Tecnológicas. Universidad Nacional de Córdoba. Facultad de Ciencias Exactas, Físicas y Naturales. Instituto de Investigaciones Biológicas y Tecnológicas; Argentina
Fil: Burgos, Martha Ines. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Instituto de Investigaciones Biológicas y Tecnológicas. Universidad Nacional de Córdoba. Facultad de Ciencias Exactas, Físicas y Naturales. Instituto de Investigaciones Biológicas y Tecnológicas; Argentina
LI Reunión Anual de la Sociedad Argentina de Biofísica
Córdoba
Argentina
Sociedad Argentina de Biofísica - Materia
-
Mesoporous silica
Nanoparticles
Nanobiocatalyst - Nivel de accesibilidad
- acceso abierto
- Condiciones de uso
- https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
- Repositorio
- Institución
- Consejo Nacional de Investigaciones Científicas y Técnicas
- OAI Identificador
- oai:ri.conicet.gov.ar:11336/257086
Ver los metadatos del registro completo
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Synthesis and characterisation of mesoporous silicate nanoparticles for use as nanobiocatalystsBujedo, Agustín AnibalPerillo, Maria AngelicaBurgos, Martha InesMesoporous silicaNanoparticlesNanobiocatalysthttps://purl.org/becyt/ford/1.6https://purl.org/becyt/ford/1Nano-biocatalysts are defined as those nanoparticles (NPs) that are capable of entrapping enzymes, transporting them and ultimately allowing catalysis to occur within the nanopores or releasing the enzyme in a controlled manner at the target site. NPs have the ability to interact with cells and tissues at the molecular level. It has been proposed that encapsulation in nanocarriers protects the bioactive components from unfavourable environmental conditions and also increases their solubility and bioavailability. We have synthesised mesoporous silicate nanoparticles using the method described by Nandiyanto et al1. It uses polystyrene as a template for the mesoporous structure and a surfactant and hydrocarbon solvent to control particle size. Different synthesis conditions were tested and the structural characteristics such as NP diameter and specific surface area (SSA) were analysed by SEM microscopy and dynamic vapour sorption, respectively. It was observed that NPs ranging from 52 to 98 nm were obtained and the SSA is compatible with mesoporous materials (194 m2 /g). Adsorption of the enzyme b-galactosidase from Kluyveromyces lactis was achieved at 48%. The chemical composition was analysed by EDS and mainly SO2 materials were observed.Fil: Bujedo, Agustín Anibal. Universidad Nacional de Córdoba. Facultad de Ciencias Exactas, Físicas y Naturales. Departamento de Química. Cátedra de Química Biológica; ArgentinaFil: Perillo, Maria Angelica. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Instituto de Investigaciones Biológicas y Tecnológicas. Universidad Nacional de Córdoba. Facultad de Ciencias Exactas, Físicas y Naturales. Instituto de Investigaciones Biológicas y Tecnológicas; ArgentinaFil: Burgos, Martha Ines. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Instituto de Investigaciones Biológicas y Tecnológicas. Universidad Nacional de Córdoba. Facultad de Ciencias Exactas, Físicas y Naturales. Instituto de Investigaciones Biológicas y Tecnológicas; ArgentinaLI Reunión Anual de la Sociedad Argentina de BiofísicaCórdobaArgentinaSociedad Argentina de BiofísicaSociedad Argentina de BiofísicaAcierno, Juan PabloCelej, Maria SoledadVazquez, Diego Sebastian2023info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/conferenceObjectReuniónBookhttp://purl.org/coar/resource_type/c_5794info:ar-repo/semantics/documentoDeConferenciaapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/257086Synthesis and characterisation of mesoporous silicate nanoparticles for use as nanobiocatalysts; LI Reunión Anual de la Sociedad Argentina de Biofísica; Córdoba; Argentina; 2023; 76-76978-987-48938-1-9CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/url/https://biofisica.org.ar/reuniones-cientificas/reunionsab-previas/Nacionalinfo:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-sa/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-09-03T09:48:14Zoai:ri.conicet.gov.ar:11336/257086instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-09-03 09:48:14.434CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse |
dc.title.none.fl_str_mv |
Synthesis and characterisation of mesoporous silicate nanoparticles for use as nanobiocatalysts |
title |
Synthesis and characterisation of mesoporous silicate nanoparticles for use as nanobiocatalysts |
spellingShingle |
Synthesis and characterisation of mesoporous silicate nanoparticles for use as nanobiocatalysts Bujedo, Agustín Anibal Mesoporous silica Nanoparticles Nanobiocatalyst |
title_short |
Synthesis and characterisation of mesoporous silicate nanoparticles for use as nanobiocatalysts |
title_full |
Synthesis and characterisation of mesoporous silicate nanoparticles for use as nanobiocatalysts |
title_fullStr |
Synthesis and characterisation of mesoporous silicate nanoparticles for use as nanobiocatalysts |
title_full_unstemmed |
Synthesis and characterisation of mesoporous silicate nanoparticles for use as nanobiocatalysts |
title_sort |
Synthesis and characterisation of mesoporous silicate nanoparticles for use as nanobiocatalysts |
dc.creator.none.fl_str_mv |
Bujedo, Agustín Anibal Perillo, Maria Angelica Burgos, Martha Ines |
author |
Bujedo, Agustín Anibal |
author_facet |
Bujedo, Agustín Anibal Perillo, Maria Angelica Burgos, Martha Ines |
author_role |
author |
author2 |
Perillo, Maria Angelica Burgos, Martha Ines |
author2_role |
author author |
dc.contributor.none.fl_str_mv |
Acierno, Juan Pablo Celej, Maria Soledad Vazquez, Diego Sebastian |
dc.subject.none.fl_str_mv |
Mesoporous silica Nanoparticles Nanobiocatalyst |
topic |
Mesoporous silica Nanoparticles Nanobiocatalyst |
purl_subject.fl_str_mv |
https://purl.org/becyt/ford/1.6 https://purl.org/becyt/ford/1 |
dc.description.none.fl_txt_mv |
Nano-biocatalysts are defined as those nanoparticles (NPs) that are capable of entrapping enzymes, transporting them and ultimately allowing catalysis to occur within the nanopores or releasing the enzyme in a controlled manner at the target site. NPs have the ability to interact with cells and tissues at the molecular level. It has been proposed that encapsulation in nanocarriers protects the bioactive components from unfavourable environmental conditions and also increases their solubility and bioavailability. We have synthesised mesoporous silicate nanoparticles using the method described by Nandiyanto et al1. It uses polystyrene as a template for the mesoporous structure and a surfactant and hydrocarbon solvent to control particle size. Different synthesis conditions were tested and the structural characteristics such as NP diameter and specific surface area (SSA) were analysed by SEM microscopy and dynamic vapour sorption, respectively. It was observed that NPs ranging from 52 to 98 nm were obtained and the SSA is compatible with mesoporous materials (194 m2 /g). Adsorption of the enzyme b-galactosidase from Kluyveromyces lactis was achieved at 48%. The chemical composition was analysed by EDS and mainly SO2 materials were observed. Fil: Bujedo, Agustín Anibal. Universidad Nacional de Córdoba. Facultad de Ciencias Exactas, Físicas y Naturales. Departamento de Química. Cátedra de Química Biológica; Argentina Fil: Perillo, Maria Angelica. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Instituto de Investigaciones Biológicas y Tecnológicas. Universidad Nacional de Córdoba. Facultad de Ciencias Exactas, Físicas y Naturales. Instituto de Investigaciones Biológicas y Tecnológicas; Argentina Fil: Burgos, Martha Ines. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Instituto de Investigaciones Biológicas y Tecnológicas. Universidad Nacional de Córdoba. Facultad de Ciencias Exactas, Físicas y Naturales. Instituto de Investigaciones Biológicas y Tecnológicas; Argentina LI Reunión Anual de la Sociedad Argentina de Biofísica Córdoba Argentina Sociedad Argentina de Biofísica |
description |
Nano-biocatalysts are defined as those nanoparticles (NPs) that are capable of entrapping enzymes, transporting them and ultimately allowing catalysis to occur within the nanopores or releasing the enzyme in a controlled manner at the target site. NPs have the ability to interact with cells and tissues at the molecular level. It has been proposed that encapsulation in nanocarriers protects the bioactive components from unfavourable environmental conditions and also increases their solubility and bioavailability. We have synthesised mesoporous silicate nanoparticles using the method described by Nandiyanto et al1. It uses polystyrene as a template for the mesoporous structure and a surfactant and hydrocarbon solvent to control particle size. Different synthesis conditions were tested and the structural characteristics such as NP diameter and specific surface area (SSA) were analysed by SEM microscopy and dynamic vapour sorption, respectively. It was observed that NPs ranging from 52 to 98 nm were obtained and the SSA is compatible with mesoporous materials (194 m2 /g). Adsorption of the enzyme b-galactosidase from Kluyveromyces lactis was achieved at 48%. The chemical composition was analysed by EDS and mainly SO2 materials were observed. |
publishDate |
2023 |
dc.date.none.fl_str_mv |
2023 |
dc.type.none.fl_str_mv |
info:eu-repo/semantics/publishedVersion info:eu-repo/semantics/conferenceObject Reunión Book http://purl.org/coar/resource_type/c_5794 info:ar-repo/semantics/documentoDeConferencia |
status_str |
publishedVersion |
format |
conferenceObject |
dc.identifier.none.fl_str_mv |
http://hdl.handle.net/11336/257086 Synthesis and characterisation of mesoporous silicate nanoparticles for use as nanobiocatalysts; LI Reunión Anual de la Sociedad Argentina de Biofísica; Córdoba; Argentina; 2023; 76-76 978-987-48938-1-9 CONICET Digital CONICET |
url |
http://hdl.handle.net/11336/257086 |
identifier_str_mv |
Synthesis and characterisation of mesoporous silicate nanoparticles for use as nanobiocatalysts; LI Reunión Anual de la Sociedad Argentina de Biofísica; Córdoba; Argentina; 2023; 76-76 978-987-48938-1-9 CONICET Digital CONICET |
dc.language.none.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
info:eu-repo/semantics/altIdentifier/url/https://biofisica.org.ar/reuniones-cientificas/reunionsab-previas/ |
dc.rights.none.fl_str_mv |
info:eu-repo/semantics/openAccess https://creativecommons.org/licenses/by-nc-sa/2.5/ar/ |
eu_rights_str_mv |
openAccess |
rights_invalid_str_mv |
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/ |
dc.format.none.fl_str_mv |
application/pdf application/pdf |
dc.coverage.none.fl_str_mv |
Nacional |
dc.publisher.none.fl_str_mv |
Sociedad Argentina de Biofísica |
publisher.none.fl_str_mv |
Sociedad Argentina de Biofísica |
dc.source.none.fl_str_mv |
reponame:CONICET Digital (CONICET) instname:Consejo Nacional de Investigaciones Científicas y Técnicas |
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CONICET Digital (CONICET) |
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CONICET Digital (CONICET) |
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Consejo Nacional de Investigaciones Científicas y Técnicas |
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CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas |
repository.mail.fl_str_mv |
dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar |
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13.13397 |