On-line preconcentration/determination of lead traces in bee honey by inductively coupled plasma optical emission spectrometry (ICP-OES) using a conical minicolumn packed with acti...
- Autores
- Cerutti, Estela Soledad; Orsi, Ricardo Fernández; Gásquez, José A.; Olsina, Roberto Antonio; Martinez, Luis Dante
- Año de publicación
- 2003
- Idioma
- inglés
- Tipo de recurso
- artículo
- Estado
- versión publicada
- Descripción
- In this study, the preconcentration of Pb2+ using a conical minicolumn packed with activated carbon (AC) was studied for preconcentration of Pb2+. The experiments showed that Pb2+ reacts with 8-hydroxyquinoline to form a complex at pH 10.0 and can be retained "on-line" on a conical minicolumn packed with activated carbon, then eluted with 20% (v/v) nitric acid. The conditions for the quantitative and reproducible preconcentration and subsequent ICP-OES determination with ultrasonic nebulization system (USN) were studied. A total enhancement factor (N) of 500 was obtained with respect to ICP-OES using pneumatic nebulization (10 for USN and 50 for enrichment factor) for a sample volume of 25 mL. The detection limit (DL) was 0.04 μg L-1. The relative standard deviation (RSD) were 3.0%. The optimized procedure was successfully applied to the determination of trace levels of Pb+2 in bee honey samples.
Fil: Cerutti, Estela Soledad. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - San Luis. Instituto de Química de San Luis. Universidad Nacional de San Luis. Facultad de Química, Bioquímica y Farmacia. Instituto de Química de San Luis; Argentina
Fil: Orsi, Ricardo Fernández. Universidad Nacional de San Luis. Facultad de Química, Bioquímica y Farmacia. Departamento de Química Analítica; Argentina
Fil: Gásquez, José A.. Universidad Nacional de San Luis. Facultad de Química, Bioquímica y Farmacia. Departamento de Química Analítica; Argentina
Fil: Olsina, Roberto Antonio. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - San Luis. Instituto de Química de San Luis. Universidad Nacional de San Luis. Facultad de Química, Bioquímica y Farmacia. Instituto de Química de San Luis; Argentina
Fil: Martinez, Luis Dante. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - San Luis. Instituto de Química de San Luis. Universidad Nacional de San Luis. Facultad de Química, Bioquímica y Farmacia. Instituto de Química de San Luis; Argentina - Materia
-
ACTIVATED CARBON
BEE HONEY
LEAD DETERMINATION
ON-LINE PRECONCENTRATION - Nivel de accesibilidad
- acceso abierto
- Condiciones de uso
- https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
- Repositorio
- Institución
- Consejo Nacional de Investigaciones Científicas y Técnicas
- OAI Identificador
- oai:ri.conicet.gov.ar:11336/99337
Ver los metadatos del registro completo
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CONICET Digital (CONICET) |
spelling |
On-line preconcentration/determination of lead traces in bee honey by inductively coupled plasma optical emission spectrometry (ICP-OES) using a conical minicolumn packed with activated carbonCerutti, Estela SoledadOrsi, Ricardo FernándezGásquez, José A.Olsina, Roberto AntonioMartinez, Luis DanteACTIVATED CARBONBEE HONEYLEAD DETERMINATIONON-LINE PRECONCENTRATIONhttps://purl.org/becyt/ford/1.4https://purl.org/becyt/ford/1In this study, the preconcentration of Pb2+ using a conical minicolumn packed with activated carbon (AC) was studied for preconcentration of Pb2+. The experiments showed that Pb2+ reacts with 8-hydroxyquinoline to form a complex at pH 10.0 and can be retained "on-line" on a conical minicolumn packed with activated carbon, then eluted with 20% (v/v) nitric acid. The conditions for the quantitative and reproducible preconcentration and subsequent ICP-OES determination with ultrasonic nebulization system (USN) were studied. A total enhancement factor (N) of 500 was obtained with respect to ICP-OES using pneumatic nebulization (10 for USN and 50 for enrichment factor) for a sample volume of 25 mL. The detection limit (DL) was 0.04 μg L-1. The relative standard deviation (RSD) were 3.0%. The optimized procedure was successfully applied to the determination of trace levels of Pb+2 in bee honey samples.Fil: Cerutti, Estela Soledad. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - San Luis. Instituto de Química de San Luis. Universidad Nacional de San Luis. Facultad de Química, Bioquímica y Farmacia. Instituto de Química de San Luis; ArgentinaFil: Orsi, Ricardo Fernández. Universidad Nacional de San Luis. Facultad de Química, Bioquímica y Farmacia. Departamento de Química Analítica; ArgentinaFil: Gásquez, José A.. Universidad Nacional de San Luis. Facultad de Química, Bioquímica y Farmacia. Departamento de Química Analítica; ArgentinaFil: Olsina, Roberto Antonio. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - San Luis. Instituto de Química de San Luis. Universidad Nacional de San Luis. Facultad de Química, Bioquímica y Farmacia. Instituto de Química de San Luis; ArgentinaFil: Martinez, Luis Dante. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - San Luis. Instituto de Química de San Luis. Universidad Nacional de San Luis. Facultad de Química, Bioquímica y Farmacia. Instituto de Química de San Luis; ArgentinaTaylor & Francis2003-08info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/99337Cerutti, Estela Soledad; Orsi, Ricardo Fernández; Gásquez, José A.; Olsina, Roberto Antonio; Martinez, Luis Dante; On-line preconcentration/determination of lead traces in bee honey by inductively coupled plasma optical emission spectrometry (ICP-OES) using a conical minicolumn packed with activated carbon; Taylor & Francis; Journal Of Trace And Microprobe Techniques; 21; 3; 8-2003; 421-4320733-4680CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/url/https://www.tandfonline.com/doi/abs/10.1081/TMA-120023059info:eu-repo/semantics/altIdentifier/doi/10.1081/TMA-120023059info:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-sa/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-09-03T10:05:37Zoai:ri.conicet.gov.ar:11336/99337instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-09-03 10:05:37.747CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse |
dc.title.none.fl_str_mv |
On-line preconcentration/determination of lead traces in bee honey by inductively coupled plasma optical emission spectrometry (ICP-OES) using a conical minicolumn packed with activated carbon |
title |
On-line preconcentration/determination of lead traces in bee honey by inductively coupled plasma optical emission spectrometry (ICP-OES) using a conical minicolumn packed with activated carbon |
spellingShingle |
On-line preconcentration/determination of lead traces in bee honey by inductively coupled plasma optical emission spectrometry (ICP-OES) using a conical minicolumn packed with activated carbon Cerutti, Estela Soledad ACTIVATED CARBON BEE HONEY LEAD DETERMINATION ON-LINE PRECONCENTRATION |
title_short |
On-line preconcentration/determination of lead traces in bee honey by inductively coupled plasma optical emission spectrometry (ICP-OES) using a conical minicolumn packed with activated carbon |
title_full |
On-line preconcentration/determination of lead traces in bee honey by inductively coupled plasma optical emission spectrometry (ICP-OES) using a conical minicolumn packed with activated carbon |
title_fullStr |
On-line preconcentration/determination of lead traces in bee honey by inductively coupled plasma optical emission spectrometry (ICP-OES) using a conical minicolumn packed with activated carbon |
title_full_unstemmed |
On-line preconcentration/determination of lead traces in bee honey by inductively coupled plasma optical emission spectrometry (ICP-OES) using a conical minicolumn packed with activated carbon |
title_sort |
On-line preconcentration/determination of lead traces in bee honey by inductively coupled plasma optical emission spectrometry (ICP-OES) using a conical minicolumn packed with activated carbon |
dc.creator.none.fl_str_mv |
Cerutti, Estela Soledad Orsi, Ricardo Fernández Gásquez, José A. Olsina, Roberto Antonio Martinez, Luis Dante |
author |
Cerutti, Estela Soledad |
author_facet |
Cerutti, Estela Soledad Orsi, Ricardo Fernández Gásquez, José A. Olsina, Roberto Antonio Martinez, Luis Dante |
author_role |
author |
author2 |
Orsi, Ricardo Fernández Gásquez, José A. Olsina, Roberto Antonio Martinez, Luis Dante |
author2_role |
author author author author |
dc.subject.none.fl_str_mv |
ACTIVATED CARBON BEE HONEY LEAD DETERMINATION ON-LINE PRECONCENTRATION |
topic |
ACTIVATED CARBON BEE HONEY LEAD DETERMINATION ON-LINE PRECONCENTRATION |
purl_subject.fl_str_mv |
https://purl.org/becyt/ford/1.4 https://purl.org/becyt/ford/1 |
dc.description.none.fl_txt_mv |
In this study, the preconcentration of Pb2+ using a conical minicolumn packed with activated carbon (AC) was studied for preconcentration of Pb2+. The experiments showed that Pb2+ reacts with 8-hydroxyquinoline to form a complex at pH 10.0 and can be retained "on-line" on a conical minicolumn packed with activated carbon, then eluted with 20% (v/v) nitric acid. The conditions for the quantitative and reproducible preconcentration and subsequent ICP-OES determination with ultrasonic nebulization system (USN) were studied. A total enhancement factor (N) of 500 was obtained with respect to ICP-OES using pneumatic nebulization (10 for USN and 50 for enrichment factor) for a sample volume of 25 mL. The detection limit (DL) was 0.04 μg L-1. The relative standard deviation (RSD) were 3.0%. The optimized procedure was successfully applied to the determination of trace levels of Pb+2 in bee honey samples. Fil: Cerutti, Estela Soledad. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - San Luis. Instituto de Química de San Luis. Universidad Nacional de San Luis. Facultad de Química, Bioquímica y Farmacia. Instituto de Química de San Luis; Argentina Fil: Orsi, Ricardo Fernández. Universidad Nacional de San Luis. Facultad de Química, Bioquímica y Farmacia. Departamento de Química Analítica; Argentina Fil: Gásquez, José A.. Universidad Nacional de San Luis. Facultad de Química, Bioquímica y Farmacia. Departamento de Química Analítica; Argentina Fil: Olsina, Roberto Antonio. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - San Luis. Instituto de Química de San Luis. Universidad Nacional de San Luis. Facultad de Química, Bioquímica y Farmacia. Instituto de Química de San Luis; Argentina Fil: Martinez, Luis Dante. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - San Luis. Instituto de Química de San Luis. Universidad Nacional de San Luis. Facultad de Química, Bioquímica y Farmacia. Instituto de Química de San Luis; Argentina |
description |
In this study, the preconcentration of Pb2+ using a conical minicolumn packed with activated carbon (AC) was studied for preconcentration of Pb2+. The experiments showed that Pb2+ reacts with 8-hydroxyquinoline to form a complex at pH 10.0 and can be retained "on-line" on a conical minicolumn packed with activated carbon, then eluted with 20% (v/v) nitric acid. The conditions for the quantitative and reproducible preconcentration and subsequent ICP-OES determination with ultrasonic nebulization system (USN) were studied. A total enhancement factor (N) of 500 was obtained with respect to ICP-OES using pneumatic nebulization (10 for USN and 50 for enrichment factor) for a sample volume of 25 mL. The detection limit (DL) was 0.04 μg L-1. The relative standard deviation (RSD) were 3.0%. The optimized procedure was successfully applied to the determination of trace levels of Pb+2 in bee honey samples. |
publishDate |
2003 |
dc.date.none.fl_str_mv |
2003-08 |
dc.type.none.fl_str_mv |
info:eu-repo/semantics/article info:eu-repo/semantics/publishedVersion http://purl.org/coar/resource_type/c_6501 info:ar-repo/semantics/articulo |
format |
article |
status_str |
publishedVersion |
dc.identifier.none.fl_str_mv |
http://hdl.handle.net/11336/99337 Cerutti, Estela Soledad; Orsi, Ricardo Fernández; Gásquez, José A.; Olsina, Roberto Antonio; Martinez, Luis Dante; On-line preconcentration/determination of lead traces in bee honey by inductively coupled plasma optical emission spectrometry (ICP-OES) using a conical minicolumn packed with activated carbon; Taylor & Francis; Journal Of Trace And Microprobe Techniques; 21; 3; 8-2003; 421-432 0733-4680 CONICET Digital CONICET |
url |
http://hdl.handle.net/11336/99337 |
identifier_str_mv |
Cerutti, Estela Soledad; Orsi, Ricardo Fernández; Gásquez, José A.; Olsina, Roberto Antonio; Martinez, Luis Dante; On-line preconcentration/determination of lead traces in bee honey by inductively coupled plasma optical emission spectrometry (ICP-OES) using a conical minicolumn packed with activated carbon; Taylor & Francis; Journal Of Trace And Microprobe Techniques; 21; 3; 8-2003; 421-432 0733-4680 CONICET Digital CONICET |
dc.language.none.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
info:eu-repo/semantics/altIdentifier/url/https://www.tandfonline.com/doi/abs/10.1081/TMA-120023059 info:eu-repo/semantics/altIdentifier/doi/10.1081/TMA-120023059 |
dc.rights.none.fl_str_mv |
info:eu-repo/semantics/openAccess https://creativecommons.org/licenses/by-nc-sa/2.5/ar/ |
eu_rights_str_mv |
openAccess |
rights_invalid_str_mv |
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/ |
dc.format.none.fl_str_mv |
application/pdf application/pdf |
dc.publisher.none.fl_str_mv |
Taylor & Francis |
publisher.none.fl_str_mv |
Taylor & Francis |
dc.source.none.fl_str_mv |
reponame:CONICET Digital (CONICET) instname:Consejo Nacional de Investigaciones Científicas y Técnicas |
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CONICET Digital (CONICET) |
collection |
CONICET Digital (CONICET) |
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Consejo Nacional de Investigaciones Científicas y Técnicas |
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CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas |
repository.mail.fl_str_mv |
dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar |
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1842269919598608384 |
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13.13397 |