High-temperature mechanical behavior of partially sintered ceramics

Autores
Nečina, Vojtěch; Gass, Sebastian Emiliano; Uhlírová, Tereza; Talou, Mariano Hernán; Camerucci, Maria Andrea; Tomba Martinez, Analia Gladys
Año de publicación
2023
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
The high-temperature mechanical behavior (elastic properties, fracture strength, and degree of irreversible deformation) of partially sintered alumina and zirconia ceramics with different porosities and degrees of sintering was evaluated by (static) three-point bending tests at 1100 °C, from which load–deflection curves were obtained. Furthermore, the elastic modulus obtained from these curves was compared to Young’s modulus as measured via the impulse excitation technique. Bar-shaped specimens were prepared by uniaxial pressing and sintering at 1100, 1200, 1300 and 1400 °C for 2 h, and subsequently characterized via bulk density measurements, total porosity calculations and electron scanning microscopy analysis. The effects caused by progressive sintering and the occurrence of irreversible deformation due to the weak bonds (small sinter necks) between particles affected the values of the static elastic modulus, which resulted in values quite lower than those obtained by the impulse excitation technique. A very good correlation described with a power-law relationship was obtained between both type of modulus, dynamic and static one, in the whole range of sintering temperatures for the two evaluated porous ceramics. In particular, the very fine (nanocrystalline) grain size and the tendency to agglomerate of the zirconia powder facilitated the irreversible deformation by grain boundary sliding.
Fil: Nečina, Vojtěch. University Of Chemistry And Technology; República Checa
Fil: Gass, Sebastian Emiliano. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Fil: Uhlírová, Tereza. University Of Chemistry And Technology; República Checa
Fil: Talou, Mariano Hernán. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Fil: Camerucci, Maria Andrea. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Fil: Tomba Martinez, Analia Gladys. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Materia
ALUMINA
ZIRCONIA
PARTIAL SINTERING
HIGH-TEMPERATURE MECHANICAL PROPERTIES
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/251439
Acceder
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oai_identifier_str oai:ri.conicet.gov.ar:11336/251439
network_acronym_str CONICETDig
repository_id_str 3498
network_name_str CONICET Digital (CONICET)
spelling High-temperature mechanical behavior of partially sintered ceramicsNečina, VojtěchGass, Sebastian EmilianoUhlírová, TerezaTalou, Mariano HernánCamerucci, Maria AndreaTomba Martinez, Analia GladysALUMINAZIRCONIAPARTIAL SINTERINGHIGH-TEMPERATURE MECHANICAL PROPERTIEShttps://purl.org/becyt/ford/2.5https://purl.org/becyt/ford/2The high-temperature mechanical behavior (elastic properties, fracture strength, and degree of irreversible deformation) of partially sintered alumina and zirconia ceramics with different porosities and degrees of sintering was evaluated by (static) three-point bending tests at 1100 °C, from which load–deflection curves were obtained. Furthermore, the elastic modulus obtained from these curves was compared to Young’s modulus as measured via the impulse excitation technique. Bar-shaped specimens were prepared by uniaxial pressing and sintering at 1100, 1200, 1300 and 1400 °C for 2 h, and subsequently characterized via bulk density measurements, total porosity calculations and electron scanning microscopy analysis. The effects caused by progressive sintering and the occurrence of irreversible deformation due to the weak bonds (small sinter necks) between particles affected the values of the static elastic modulus, which resulted in values quite lower than those obtained by the impulse excitation technique. A very good correlation described with a power-law relationship was obtained between both type of modulus, dynamic and static one, in the whole range of sintering temperatures for the two evaluated porous ceramics. In particular, the very fine (nanocrystalline) grain size and the tendency to agglomerate of the zirconia powder facilitated the irreversible deformation by grain boundary sliding.Fil: Nečina, Vojtěch. University Of Chemistry And Technology; República ChecaFil: Gass, Sebastian Emiliano. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; ArgentinaFil: Uhlírová, Tereza. University Of Chemistry And Technology; República ChecaFil: Talou, Mariano Hernán. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; ArgentinaFil: Camerucci, Maria Andrea. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; ArgentinaFil: Tomba Martinez, Analia Gladys. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; ArgentinaSpringer2023-03info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/251439Nečina, Vojtěch; Gass, Sebastian Emiliano; Uhlírová, Tereza; Talou, Mariano Hernán; Camerucci, Maria Andrea; et al.; High-temperature mechanical behavior of partially sintered ceramics; Springer; Journal of Materials Science; 58; 12; 3-2023; 5208-52180022-2461CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/url/https://link.springer.com/10.1007/s10853-023-08382-xinfo:eu-repo/semantics/altIdentifier/doi/10.1007/s10853-023-08382-xinfo:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-sa/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-10-15T14:28:17Zoai:ri.conicet.gov.ar:11336/251439instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-10-15 14:28:17.523CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv High-temperature mechanical behavior of partially sintered ceramics
title High-temperature mechanical behavior of partially sintered ceramics
spellingShingle High-temperature mechanical behavior of partially sintered ceramics
Nečina, Vojtěch
ALUMINA
ZIRCONIA
PARTIAL SINTERING
HIGH-TEMPERATURE MECHANICAL PROPERTIES
title_short High-temperature mechanical behavior of partially sintered ceramics
title_full High-temperature mechanical behavior of partially sintered ceramics
title_fullStr High-temperature mechanical behavior of partially sintered ceramics
title_full_unstemmed High-temperature mechanical behavior of partially sintered ceramics
title_sort High-temperature mechanical behavior of partially sintered ceramics
dc.creator.none.fl_str_mv Nečina, Vojtěch
Gass, Sebastian Emiliano
Uhlírová, Tereza
Talou, Mariano Hernán
Camerucci, Maria Andrea
Tomba Martinez, Analia Gladys
author Nečina, Vojtěch
author_facet Nečina, Vojtěch
Gass, Sebastian Emiliano
Uhlírová, Tereza
Talou, Mariano Hernán
Camerucci, Maria Andrea
Tomba Martinez, Analia Gladys
author_role author
author2 Gass, Sebastian Emiliano
Uhlírová, Tereza
Talou, Mariano Hernán
Camerucci, Maria Andrea
Tomba Martinez, Analia Gladys
author2_role author
author
author
author
author
dc.subject.none.fl_str_mv ALUMINA
ZIRCONIA
PARTIAL SINTERING
HIGH-TEMPERATURE MECHANICAL PROPERTIES
topic ALUMINA
ZIRCONIA
PARTIAL SINTERING
HIGH-TEMPERATURE MECHANICAL PROPERTIES
purl_subject.fl_str_mv https://purl.org/becyt/ford/2.5
https://purl.org/becyt/ford/2
dc.description.none.fl_txt_mv The high-temperature mechanical behavior (elastic properties, fracture strength, and degree of irreversible deformation) of partially sintered alumina and zirconia ceramics with different porosities and degrees of sintering was evaluated by (static) three-point bending tests at 1100 °C, from which load–deflection curves were obtained. Furthermore, the elastic modulus obtained from these curves was compared to Young’s modulus as measured via the impulse excitation technique. Bar-shaped specimens were prepared by uniaxial pressing and sintering at 1100, 1200, 1300 and 1400 °C for 2 h, and subsequently characterized via bulk density measurements, total porosity calculations and electron scanning microscopy analysis. The effects caused by progressive sintering and the occurrence of irreversible deformation due to the weak bonds (small sinter necks) between particles affected the values of the static elastic modulus, which resulted in values quite lower than those obtained by the impulse excitation technique. A very good correlation described with a power-law relationship was obtained between both type of modulus, dynamic and static one, in the whole range of sintering temperatures for the two evaluated porous ceramics. In particular, the very fine (nanocrystalline) grain size and the tendency to agglomerate of the zirconia powder facilitated the irreversible deformation by grain boundary sliding.
Fil: Nečina, Vojtěch. University Of Chemistry And Technology; República Checa
Fil: Gass, Sebastian Emiliano. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Fil: Uhlírová, Tereza. University Of Chemistry And Technology; República Checa
Fil: Talou, Mariano Hernán. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Fil: Camerucci, Maria Andrea. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Fil: Tomba Martinez, Analia Gladys. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
description The high-temperature mechanical behavior (elastic properties, fracture strength, and degree of irreversible deformation) of partially sintered alumina and zirconia ceramics with different porosities and degrees of sintering was evaluated by (static) three-point bending tests at 1100 °C, from which load–deflection curves were obtained. Furthermore, the elastic modulus obtained from these curves was compared to Young’s modulus as measured via the impulse excitation technique. Bar-shaped specimens were prepared by uniaxial pressing and sintering at 1100, 1200, 1300 and 1400 °C for 2 h, and subsequently characterized via bulk density measurements, total porosity calculations and electron scanning microscopy analysis. The effects caused by progressive sintering and the occurrence of irreversible deformation due to the weak bonds (small sinter necks) between particles affected the values of the static elastic modulus, which resulted in values quite lower than those obtained by the impulse excitation technique. A very good correlation described with a power-law relationship was obtained between both type of modulus, dynamic and static one, in the whole range of sintering temperatures for the two evaluated porous ceramics. In particular, the very fine (nanocrystalline) grain size and the tendency to agglomerate of the zirconia powder facilitated the irreversible deformation by grain boundary sliding.
publishDate 2023
dc.date.none.fl_str_mv 2023-03
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/251439
Nečina, Vojtěch; Gass, Sebastian Emiliano; Uhlírová, Tereza; Talou, Mariano Hernán; Camerucci, Maria Andrea; et al.; High-temperature mechanical behavior of partially sintered ceramics; Springer; Journal of Materials Science; 58; 12; 3-2023; 5208-5218
0022-2461
CONICET Digital
CONICET
url http://hdl.handle.net/11336/251439
identifier_str_mv Nečina, Vojtěch; Gass, Sebastian Emiliano; Uhlírová, Tereza; Talou, Mariano Hernán; Camerucci, Maria Andrea; et al.; High-temperature mechanical behavior of partially sintered ceramics; Springer; Journal of Materials Science; 58; 12; 3-2023; 5208-5218
0022-2461
CONICET Digital
CONICET
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/url/https://link.springer.com/10.1007/s10853-023-08382-x
info:eu-repo/semantics/altIdentifier/doi/10.1007/s10853-023-08382-x
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
dc.publisher.none.fl_str_mv Springer
publisher.none.fl_str_mv Springer
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
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score 13.22299

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