Occluded cobalt species over ZSM-5 matrix: Design, preparation, characterization and magnetic behavior
- Autores
- Pierella, Liliana Beatriz; Saux, Clara; Bertorello, Hector Raul; Bercoff, Paula Gabriela; Botta, Pablo Martín; Rivas, Jose
- Año de publicación
- 2007
- Idioma
- inglés
- Tipo de recurso
- artículo
- Estado
- versión publicada
- Descripción
- Co-containing molecular sieves with MFI structure was synthesized by the hydrothermal crystallization method and cobalt was incorporated in it by wet impregnation at different percentages. Thermal post-treatments were applied to Co-ZSM-5: calcination and reduction. X ray diffraction (XRD) and FTIR studies confirmed crystallinity, structure and orthorhombic symmetry of the obtained samples (Co-ZSM-5 calcined and Co-ZSM-5 reduced). The XRD, Raman spectroscopy, SEM and TPR techniques for the calcined samples showed the presence of Co3O4 which diminished in the reduced samples and Co0 appeared. The magnetic behavior of the materials was evaluated by magnetization (M) variation with applied magnetic field (H) at different temperatures. Low magnetization is observed in the calcined samples while high values are ttained in the reduced samples, due to the presence of metallic Co.
Fil: Pierella, Liliana Beatriz. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Centro de Investigación y Tecnología Química. Universidad Tecnológica Nacional. Facultad Regional Córdoba. Centro de Investigación y Tecnología Química; Argentina
Fil: Saux, Clara. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Centro de Investigación y Tecnología Química. Universidad Tecnológica Nacional. Facultad Regional Córdoba. Centro de Investigación y Tecnología Química; Argentina
Fil: Bertorello, Hector Raul. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina. Universidad Nacional de Córdoba. Facultad de Matemática, Astronomía y Física; Argentina
Fil: Bercoff, Paula Gabriela. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina. Universidad Nacional de Córdoba. Facultad de Matemática, Astronomía y Física; Argentina
Fil: Botta, Pablo Martín. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina. Universidad de Santiago de Compostela; España
Fil: Rivas, Jose. Universidad de Santiago de Compostela; España - Materia
-
Microporous Materials
Magnetic Properties - Nivel de accesibilidad
- acceso abierto
- Condiciones de uso
- https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
- Repositorio
- Institución
- Consejo Nacional de Investigaciones Científicas y Técnicas
- OAI Identificador
- oai:ri.conicet.gov.ar:11336/40595
Ver los metadatos del registro completo
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Occluded cobalt species over ZSM-5 matrix: Design, preparation, characterization and magnetic behaviorPierella, Liliana BeatrizSaux, ClaraBertorello, Hector RaulBercoff, Paula GabrielaBotta, Pablo MartínRivas, JoseMicroporous MaterialsMagnetic Propertieshttps://purl.org/becyt/ford/2.5https://purl.org/becyt/ford/2Co-containing molecular sieves with MFI structure was synthesized by the hydrothermal crystallization method and cobalt was incorporated in it by wet impregnation at different percentages. Thermal post-treatments were applied to Co-ZSM-5: calcination and reduction. X ray diffraction (XRD) and FTIR studies confirmed crystallinity, structure and orthorhombic symmetry of the obtained samples (Co-ZSM-5 calcined and Co-ZSM-5 reduced). The XRD, Raman spectroscopy, SEM and TPR techniques for the calcined samples showed the presence of Co3O4 which diminished in the reduced samples and Co0 appeared. The magnetic behavior of the materials was evaluated by magnetization (M) variation with applied magnetic field (H) at different temperatures. Low magnetization is observed in the calcined samples while high values are ttained in the reduced samples, due to the presence of metallic Co.Fil: Pierella, Liliana Beatriz. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Centro de Investigación y Tecnología Química. Universidad Tecnológica Nacional. Facultad Regional Córdoba. Centro de Investigación y Tecnología Química; ArgentinaFil: Saux, Clara. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Centro de Investigación y Tecnología Química. Universidad Tecnológica Nacional. Facultad Regional Córdoba. Centro de Investigación y Tecnología Química; ArgentinaFil: Bertorello, Hector Raul. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina. Universidad Nacional de Córdoba. Facultad de Matemática, Astronomía y Física; ArgentinaFil: Bercoff, Paula Gabriela. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina. Universidad Nacional de Córdoba. Facultad de Matemática, Astronomía y Física; ArgentinaFil: Botta, Pablo Martín. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina. Universidad de Santiago de Compostela; EspañaFil: Rivas, Jose. Universidad de Santiago de Compostela; EspañaPergamon-Elsevier Science Ltd2007-10-05info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfapplication/pdfapplication/pdfapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/40595Pierella, Liliana Beatriz; Saux, Clara; Bertorello, Hector Raul; Bercoff, Paula Gabriela; Botta, Pablo Martín; et al.; Occluded cobalt species over ZSM-5 matrix: Design, preparation, characterization and magnetic behavior; Pergamon-Elsevier Science Ltd; Materials Research Bulletin; 43; 8-9; 5-10-2007; 2026-20350025-5408CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/doi/10.1016/j.materresbull.2007.09.026info:eu-repo/semantics/altIdentifier/url/https://www.sciencedirect.com/science/article/pii/S002554080700428Xinfo:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-nd/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-09-03T09:45:06Zoai:ri.conicet.gov.ar:11336/40595instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-09-03 09:45:07.158CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse |
dc.title.none.fl_str_mv |
Occluded cobalt species over ZSM-5 matrix: Design, preparation, characterization and magnetic behavior |
title |
Occluded cobalt species over ZSM-5 matrix: Design, preparation, characterization and magnetic behavior |
spellingShingle |
Occluded cobalt species over ZSM-5 matrix: Design, preparation, characterization and magnetic behavior Pierella, Liliana Beatriz Microporous Materials Magnetic Properties |
title_short |
Occluded cobalt species over ZSM-5 matrix: Design, preparation, characterization and magnetic behavior |
title_full |
Occluded cobalt species over ZSM-5 matrix: Design, preparation, characterization and magnetic behavior |
title_fullStr |
Occluded cobalt species over ZSM-5 matrix: Design, preparation, characterization and magnetic behavior |
title_full_unstemmed |
Occluded cobalt species over ZSM-5 matrix: Design, preparation, characterization and magnetic behavior |
title_sort |
Occluded cobalt species over ZSM-5 matrix: Design, preparation, characterization and magnetic behavior |
dc.creator.none.fl_str_mv |
Pierella, Liliana Beatriz Saux, Clara Bertorello, Hector Raul Bercoff, Paula Gabriela Botta, Pablo Martín Rivas, Jose |
author |
Pierella, Liliana Beatriz |
author_facet |
Pierella, Liliana Beatriz Saux, Clara Bertorello, Hector Raul Bercoff, Paula Gabriela Botta, Pablo Martín Rivas, Jose |
author_role |
author |
author2 |
Saux, Clara Bertorello, Hector Raul Bercoff, Paula Gabriela Botta, Pablo Martín Rivas, Jose |
author2_role |
author author author author author |
dc.subject.none.fl_str_mv |
Microporous Materials Magnetic Properties |
topic |
Microporous Materials Magnetic Properties |
purl_subject.fl_str_mv |
https://purl.org/becyt/ford/2.5 https://purl.org/becyt/ford/2 |
dc.description.none.fl_txt_mv |
Co-containing molecular sieves with MFI structure was synthesized by the hydrothermal crystallization method and cobalt was incorporated in it by wet impregnation at different percentages. Thermal post-treatments were applied to Co-ZSM-5: calcination and reduction. X ray diffraction (XRD) and FTIR studies confirmed crystallinity, structure and orthorhombic symmetry of the obtained samples (Co-ZSM-5 calcined and Co-ZSM-5 reduced). The XRD, Raman spectroscopy, SEM and TPR techniques for the calcined samples showed the presence of Co3O4 which diminished in the reduced samples and Co0 appeared. The magnetic behavior of the materials was evaluated by magnetization (M) variation with applied magnetic field (H) at different temperatures. Low magnetization is observed in the calcined samples while high values are ttained in the reduced samples, due to the presence of metallic Co. Fil: Pierella, Liliana Beatriz. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Centro de Investigación y Tecnología Química. Universidad Tecnológica Nacional. Facultad Regional Córdoba. Centro de Investigación y Tecnología Química; Argentina Fil: Saux, Clara. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Centro de Investigación y Tecnología Química. Universidad Tecnológica Nacional. Facultad Regional Córdoba. Centro de Investigación y Tecnología Química; Argentina Fil: Bertorello, Hector Raul. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina. Universidad Nacional de Córdoba. Facultad de Matemática, Astronomía y Física; Argentina Fil: Bercoff, Paula Gabriela. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina. Universidad Nacional de Córdoba. Facultad de Matemática, Astronomía y Física; Argentina Fil: Botta, Pablo Martín. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina. Universidad de Santiago de Compostela; España Fil: Rivas, Jose. Universidad de Santiago de Compostela; España |
description |
Co-containing molecular sieves with MFI structure was synthesized by the hydrothermal crystallization method and cobalt was incorporated in it by wet impregnation at different percentages. Thermal post-treatments were applied to Co-ZSM-5: calcination and reduction. X ray diffraction (XRD) and FTIR studies confirmed crystallinity, structure and orthorhombic symmetry of the obtained samples (Co-ZSM-5 calcined and Co-ZSM-5 reduced). The XRD, Raman spectroscopy, SEM and TPR techniques for the calcined samples showed the presence of Co3O4 which diminished in the reduced samples and Co0 appeared. The magnetic behavior of the materials was evaluated by magnetization (M) variation with applied magnetic field (H) at different temperatures. Low magnetization is observed in the calcined samples while high values are ttained in the reduced samples, due to the presence of metallic Co. |
publishDate |
2007 |
dc.date.none.fl_str_mv |
2007-10-05 |
dc.type.none.fl_str_mv |
info:eu-repo/semantics/article info:eu-repo/semantics/publishedVersion http://purl.org/coar/resource_type/c_6501 info:ar-repo/semantics/articulo |
format |
article |
status_str |
publishedVersion |
dc.identifier.none.fl_str_mv |
http://hdl.handle.net/11336/40595 Pierella, Liliana Beatriz; Saux, Clara; Bertorello, Hector Raul; Bercoff, Paula Gabriela; Botta, Pablo Martín; et al.; Occluded cobalt species over ZSM-5 matrix: Design, preparation, characterization and magnetic behavior; Pergamon-Elsevier Science Ltd; Materials Research Bulletin; 43; 8-9; 5-10-2007; 2026-2035 0025-5408 CONICET Digital CONICET |
url |
http://hdl.handle.net/11336/40595 |
identifier_str_mv |
Pierella, Liliana Beatriz; Saux, Clara; Bertorello, Hector Raul; Bercoff, Paula Gabriela; Botta, Pablo Martín; et al.; Occluded cobalt species over ZSM-5 matrix: Design, preparation, characterization and magnetic behavior; Pergamon-Elsevier Science Ltd; Materials Research Bulletin; 43; 8-9; 5-10-2007; 2026-2035 0025-5408 CONICET Digital CONICET |
dc.language.none.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
info:eu-repo/semantics/altIdentifier/doi/10.1016/j.materresbull.2007.09.026 info:eu-repo/semantics/altIdentifier/url/https://www.sciencedirect.com/science/article/pii/S002554080700428X |
dc.rights.none.fl_str_mv |
info:eu-repo/semantics/openAccess https://creativecommons.org/licenses/by-nc-nd/2.5/ar/ |
eu_rights_str_mv |
openAccess |
rights_invalid_str_mv |
https://creativecommons.org/licenses/by-nc-nd/2.5/ar/ |
dc.format.none.fl_str_mv |
application/pdf application/pdf application/pdf application/pdf application/pdf application/pdf |
dc.publisher.none.fl_str_mv |
Pergamon-Elsevier Science Ltd |
publisher.none.fl_str_mv |
Pergamon-Elsevier Science Ltd |
dc.source.none.fl_str_mv |
reponame:CONICET Digital (CONICET) instname:Consejo Nacional de Investigaciones Científicas y Técnicas |
reponame_str |
CONICET Digital (CONICET) |
collection |
CONICET Digital (CONICET) |
instname_str |
Consejo Nacional de Investigaciones Científicas y Técnicas |
repository.name.fl_str_mv |
CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas |
repository.mail.fl_str_mv |
dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar |
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1842268710645006336 |
score |
13.13397 |