Crystal structure of (2R,4S,5R)-2-(4-benzyloxy-5-benzyloxymethyltetrahydrofuranyl) triphenyIphosphoníum tetrafluoroborate tetrachloromethane solvate, C<sub>37</sub>H<sub>36</sub>PB...

Autores
Frey, W.; Lieberknecht, A.; Griesser, H.; Bravo, Rodolfo Daniel; Colinas, Pedro Alfonso; Grigera, José Raúl
Año de publicación
1998
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
Source of material: The title compound was prepared by reaction of methyl 3,5-di-0-benzyl-2,3-dideoxy-D-ribofuranoside with hydrogentriphenylphosphonium tetrafluoroborate in acetonitrile. The precipitated phosphonium salt was recrystallized from tetrachloromethane/dichloromethane. One tetrachloromethane solvent molecule per asymmetric unit was found. This solvent molecule was strongly disordered.
Centro de Estudios de Compuestos Orgánicos
Instituto de Física de Líquidos y Sistemas Biológicos
Materia
Química
Tetrafluoroborate
Molecule
Nivel de accesibilidad
acceso abierto
Condiciones de uso
http://creativecommons.org/licenses/by-nc-nd/4.0/
Repositorio
SEDICI (UNLP)
Institución
Universidad Nacional de La Plata
OAI Identificador
oai:sedici.unlp.edu.ar:10915/120072
Acceder
id SEDICI_1d24f3249dc73beadac3426ee9369e37
oai_identifier_str oai:sedici.unlp.edu.ar:10915/120072
network_acronym_str SEDICI
repository_id_str 1329
network_name_str SEDICI (UNLP)
spelling Crystal structure of (2R,4S,5R)-2-(4-benzyloxy-5-benzyloxymethyltetrahydrofuranyl) triphenyIphosphoníum tetrafluoroborate tetrachloromethane solvate, C<sub>37</sub>H<sub>36</sub>PBF<sub>4</sub>O</sub>3</sub> CCI<sub>4</sub>Frey, W.Lieberknecht, A.Griesser, H.Bravo, Rodolfo DanielColinas, Pedro AlfonsoGrigera, José RaúlQuímicaTetrafluoroborateMoleculeSource of material: The title compound was prepared by reaction of methyl 3,5-di-0-benzyl-2,3-dideoxy-D-ribofuranoside with hydrogentriphenylphosphonium tetrafluoroborate in acetonitrile. The precipitated phosphonium salt was recrystallized from tetrachloromethane/dichloromethane. One tetrachloromethane solvent molecule per asymmetric unit was found. This solvent molecule was strongly disordered.Centro de Estudios de Compuestos OrgánicosInstituto de Física de Líquidos y Sistemas Biológicos1998info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionArticulohttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdf365-366http://sedici.unlp.edu.ar/handle/10915/120072enginfo:eu-repo/semantics/altIdentifier/issn/2197-4578info:eu-repo/semantics/altIdentifier/doi/10.1524/ncrs.1998.213.14.379info:eu-repo/semantics/openAccesshttp://creativecommons.org/licenses/by-nc-nd/4.0/Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International (CC BY-NC-ND 4.0)reponame:SEDICI (UNLP)instname:Universidad Nacional de La Platainstacron:UNLP2026-02-26T11:15:29Zoai:sedici.unlp.edu.ar:10915/120072Institucionalhttp://sedici.unlp.edu.ar/Universidad públicaNo correspondehttp://sedici.unlp.edu.ar/oai/snrdalira@sedici.unlp.edu.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:13292026-02-26 11:15:29.569SEDICI (UNLP) - Universidad Nacional de La Platafalse
dc.title.none.fl_str_mv Crystal structure of (2R,4S,5R)-2-(4-benzyloxy-5-benzyloxymethyltetrahydrofuranyl) triphenyIphosphoníum tetrafluoroborate tetrachloromethane solvate, C<sub>37</sub>H<sub>36</sub>PBF<sub>4</sub>O</sub>3</sub> CCI<sub>4</sub>
title Crystal structure of (2R,4S,5R)-2-(4-benzyloxy-5-benzyloxymethyltetrahydrofuranyl) triphenyIphosphoníum tetrafluoroborate tetrachloromethane solvate, C<sub>37</sub>H<sub>36</sub>PBF<sub>4</sub>O</sub>3</sub> CCI<sub>4</sub>
spellingShingle Crystal structure of (2R,4S,5R)-2-(4-benzyloxy-5-benzyloxymethyltetrahydrofuranyl) triphenyIphosphoníum tetrafluoroborate tetrachloromethane solvate, C<sub>37</sub>H<sub>36</sub>PBF<sub>4</sub>O</sub>3</sub> CCI<sub>4</sub>
Frey, W.
Química
Tetrafluoroborate
Molecule
title_short Crystal structure of (2R,4S,5R)-2-(4-benzyloxy-5-benzyloxymethyltetrahydrofuranyl) triphenyIphosphoníum tetrafluoroborate tetrachloromethane solvate, C<sub>37</sub>H<sub>36</sub>PBF<sub>4</sub>O</sub>3</sub> CCI<sub>4</sub>
title_full Crystal structure of (2R,4S,5R)-2-(4-benzyloxy-5-benzyloxymethyltetrahydrofuranyl) triphenyIphosphoníum tetrafluoroborate tetrachloromethane solvate, C<sub>37</sub>H<sub>36</sub>PBF<sub>4</sub>O</sub>3</sub> CCI<sub>4</sub>
title_fullStr Crystal structure of (2R,4S,5R)-2-(4-benzyloxy-5-benzyloxymethyltetrahydrofuranyl) triphenyIphosphoníum tetrafluoroborate tetrachloromethane solvate, C<sub>37</sub>H<sub>36</sub>PBF<sub>4</sub>O</sub>3</sub> CCI<sub>4</sub>
title_full_unstemmed Crystal structure of (2R,4S,5R)-2-(4-benzyloxy-5-benzyloxymethyltetrahydrofuranyl) triphenyIphosphoníum tetrafluoroborate tetrachloromethane solvate, C<sub>37</sub>H<sub>36</sub>PBF<sub>4</sub>O</sub>3</sub> CCI<sub>4</sub>
title_sort Crystal structure of (2R,4S,5R)-2-(4-benzyloxy-5-benzyloxymethyltetrahydrofuranyl) triphenyIphosphoníum tetrafluoroborate tetrachloromethane solvate, C<sub>37</sub>H<sub>36</sub>PBF<sub>4</sub>O</sub>3</sub> CCI<sub>4</sub>
dc.creator.none.fl_str_mv Frey, W.
Lieberknecht, A.
Griesser, H.
Bravo, Rodolfo Daniel
Colinas, Pedro Alfonso
Grigera, José Raúl
author Frey, W.
author_facet Frey, W.
Lieberknecht, A.
Griesser, H.
Bravo, Rodolfo Daniel
Colinas, Pedro Alfonso
Grigera, José Raúl
author_role author
author2 Lieberknecht, A.
Griesser, H.
Bravo, Rodolfo Daniel
Colinas, Pedro Alfonso
Grigera, José Raúl
author2_role author
author
author
author
author
dc.subject.none.fl_str_mv Química
Tetrafluoroborate
Molecule
topic Química
Tetrafluoroborate
Molecule
dc.description.none.fl_txt_mv Source of material: The title compound was prepared by reaction of methyl 3,5-di-0-benzyl-2,3-dideoxy-D-ribofuranoside with hydrogentriphenylphosphonium tetrafluoroborate in acetonitrile. The precipitated phosphonium salt was recrystallized from tetrachloromethane/dichloromethane. One tetrachloromethane solvent molecule per asymmetric unit was found. This solvent molecule was strongly disordered.
Centro de Estudios de Compuestos Orgánicos
Instituto de Física de Líquidos y Sistemas Biológicos
description Source of material: The title compound was prepared by reaction of methyl 3,5-di-0-benzyl-2,3-dideoxy-D-ribofuranoside with hydrogentriphenylphosphonium tetrafluoroborate in acetonitrile. The precipitated phosphonium salt was recrystallized from tetrachloromethane/dichloromethane. One tetrachloromethane solvent molecule per asymmetric unit was found. This solvent molecule was strongly disordered.
publishDate 1998
dc.date.none.fl_str_mv 1998
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
Articulo
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://sedici.unlp.edu.ar/handle/10915/120072
url http://sedici.unlp.edu.ar/handle/10915/120072
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/issn/2197-4578
info:eu-repo/semantics/altIdentifier/doi/10.1524/ncrs.1998.213.14.379
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
http://creativecommons.org/licenses/by-nc-nd/4.0/
Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International (CC BY-NC-ND 4.0)
eu_rights_str_mv openAccess
rights_invalid_str_mv http://creativecommons.org/licenses/by-nc-nd/4.0/
Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International (CC BY-NC-ND 4.0)
dc.format.none.fl_str_mv application/pdf
365-366
dc.source.none.fl_str_mv reponame:SEDICI (UNLP)
instname:Universidad Nacional de La Plata
instacron:UNLP
reponame_str SEDICI (UNLP)
collection SEDICI (UNLP)
instname_str Universidad Nacional de La Plata
instacron_str UNLP
institution UNLP
repository.name.fl_str_mv SEDICI (UNLP) - Universidad Nacional de La Plata
repository.mail.fl_str_mv alira@sedici.unlp.edu.ar
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score 13.176822

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