Development and validation of a Capillary Zone Electrophoresis method for the determination of calcium in composite biomaterials
- Autores
- Cattalini, Juan Pablo; García, Javier; Mouriño, Viviana Silvia Lourdes; Lucangioli, Silvia Edith
- Año de publicación
- 2014
- Idioma
- inglés
- Tipo de recurso
- artículo
- Estado
- versión publicada
- Descripción
- This work presents the development and validation of a capillary zone electrophoresis method for calcium ions release quantitation from composite biomaterials with potential application in bone tissue engineering. Calcium ions quantitation was made using a fused silica capillary (40 cm, 75 µm ID) and background electrolyte containing 5 mM imidazole, 6 mM á-hydroxyisobutyric acid, 1 mM 1,4,7,10,13,16-hexaoxacyclo-octadecane and 20 % w/v methanol, at pH 4.5. Indirect UV-detection mode at 214 nm was performed. The separations were achieved using normal polarity at 6 kV, a cartridge temperature of 25 µC and 0.5 psi for 5 s for sample introduction. Parameters of validation such as specificity, linearity, limit of detection and quantitation, accuracy, precision and robustness were evaluated according to the International Conference on Harmonization guidelines. The new developed method resulted to be suitable for calcium determination from composite biomaterials for potential application in bone tissue engineering.
Fil: Cattalini, Juan Pablo. Universidad de Buenos Aires. Facultad de Farmacia y Bioquímica. Departamento de Tecnología Farmacéutica; Argentina; Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Houssay; Argentina;
Fil: García, Javier. Universidad de Buenos Aires. Facultad de Farmacia y Bioquímica. Departamento de Tecnología Farmacéutica; Argentina;
Fil: Mouriño, Viviana Silvia Lourdes. Universidad de Buenos Aires. Facultad de Farmacia y Bioquímica. Departamento de Tecnología Farmacéutica; Argentina; Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Houssay; Argentina;
Fil: Lucangioli, Silvia Edith. Universidad de Buenos Aires. Facultad de Farmacia y Bioquímica. Departamento de Tecnología Farmacéutica; Argentina; Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Houssay; Argentina; - Materia
-
CALCIUM QUANTITATION
CAPILLARY ZONE ELECTROPHORESIS
COMPOSITE MATERIALS
INDIRECT UV
IONS RELEASE
VALIDATION - Nivel de accesibilidad
- acceso embargado
- Condiciones de uso
- https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
- Repositorio
- Institución
- Consejo Nacional de Investigaciones Científicas y Técnicas
- OAI Identificador
- oai:ri.conicet.gov.ar:11336/1924
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CONICET Digital (CONICET) |
spelling |
Development and validation of a Capillary Zone Electrophoresis method for the determination of calcium in composite biomaterialsCattalini, Juan PabloGarcía, JavierMouriño, Viviana Silvia LourdesLucangioli, Silvia EdithCALCIUM QUANTITATIONCAPILLARY ZONE ELECTROPHORESISCOMPOSITE MATERIALSINDIRECT UVIONS RELEASEVALIDATIONhttps://purl.org/becyt/ford/3.4https://purl.org/becyt/ford/3This work presents the development and validation of a capillary zone electrophoresis method for calcium ions release quantitation from composite biomaterials with potential application in bone tissue engineering. Calcium ions quantitation was made using a fused silica capillary (40 cm, 75 µm ID) and background electrolyte containing 5 mM imidazole, 6 mM á-hydroxyisobutyric acid, 1 mM 1,4,7,10,13,16-hexaoxacyclo-octadecane and 20 % w/v methanol, at pH 4.5. Indirect UV-detection mode at 214 nm was performed. The separations were achieved using normal polarity at 6 kV, a cartridge temperature of 25 µC and 0.5 psi for 5 s for sample introduction. Parameters of validation such as specificity, linearity, limit of detection and quantitation, accuracy, precision and robustness were evaluated according to the International Conference on Harmonization guidelines. The new developed method resulted to be suitable for calcium determination from composite biomaterials for potential application in bone tissue engineering.Fil: Cattalini, Juan Pablo. Universidad de Buenos Aires. Facultad de Farmacia y Bioquímica. Departamento de Tecnología Farmacéutica; Argentina; Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Houssay; Argentina;Fil: García, Javier. Universidad de Buenos Aires. Facultad de Farmacia y Bioquímica. Departamento de Tecnología Farmacéutica; Argentina;Fil: Mouriño, Viviana Silvia Lourdes. Universidad de Buenos Aires. Facultad de Farmacia y Bioquímica. Departamento de Tecnología Farmacéutica; Argentina; Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Houssay; Argentina;Fil: Lucangioli, Silvia Edith. Universidad de Buenos Aires. Facultad de Farmacia y Bioquímica. Departamento de Tecnología Farmacéutica; Argentina; Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Houssay; Argentina;Bentham Science Publishers2014-10info:eu-repo/date/embargoEnd/2015-12-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/1924Cattalini, Juan Pablo; García, Javier; Mouriño, Viviana Silvia Lourdes; Lucangioli, Silvia Edith; Development and validation of a Capillary Zone Electrophoresis method for the determination of calcium in composite biomaterials; Bentham Science Publishers; Current Analytical Chemistry; 10; 4; 10-2014; 465-4721573-4110http://www.ingentaconnect.com/content/ben/cac/2014/00000010/00000004/art00004?crawler=true#expand/collapseenginfo:eu-repo/semantics/altIdentifier/doi/ 10.2174/15734110113099990038info:eu-repo/semantics/altIdentifier/url/http://benthamscience.com/journals/current-analytical-chemistry/volume/10/issue/4/page/465/info:eu-repo/semantics/embargoedAccesshttps://creativecommons.org/licenses/by-nc-sa/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-09-29T09:37:24Zoai:ri.conicet.gov.ar:11336/1924instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-09-29 09:37:24.885CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse |
dc.title.none.fl_str_mv |
Development and validation of a Capillary Zone Electrophoresis method for the determination of calcium in composite biomaterials |
title |
Development and validation of a Capillary Zone Electrophoresis method for the determination of calcium in composite biomaterials |
spellingShingle |
Development and validation of a Capillary Zone Electrophoresis method for the determination of calcium in composite biomaterials Cattalini, Juan Pablo CALCIUM QUANTITATION CAPILLARY ZONE ELECTROPHORESIS COMPOSITE MATERIALS INDIRECT UV IONS RELEASE VALIDATION |
title_short |
Development and validation of a Capillary Zone Electrophoresis method for the determination of calcium in composite biomaterials |
title_full |
Development and validation of a Capillary Zone Electrophoresis method for the determination of calcium in composite biomaterials |
title_fullStr |
Development and validation of a Capillary Zone Electrophoresis method for the determination of calcium in composite biomaterials |
title_full_unstemmed |
Development and validation of a Capillary Zone Electrophoresis method for the determination of calcium in composite biomaterials |
title_sort |
Development and validation of a Capillary Zone Electrophoresis method for the determination of calcium in composite biomaterials |
dc.creator.none.fl_str_mv |
Cattalini, Juan Pablo García, Javier Mouriño, Viviana Silvia Lourdes Lucangioli, Silvia Edith |
author |
Cattalini, Juan Pablo |
author_facet |
Cattalini, Juan Pablo García, Javier Mouriño, Viviana Silvia Lourdes Lucangioli, Silvia Edith |
author_role |
author |
author2 |
García, Javier Mouriño, Viviana Silvia Lourdes Lucangioli, Silvia Edith |
author2_role |
author author author |
dc.subject.none.fl_str_mv |
CALCIUM QUANTITATION CAPILLARY ZONE ELECTROPHORESIS COMPOSITE MATERIALS INDIRECT UV IONS RELEASE VALIDATION |
topic |
CALCIUM QUANTITATION CAPILLARY ZONE ELECTROPHORESIS COMPOSITE MATERIALS INDIRECT UV IONS RELEASE VALIDATION |
purl_subject.fl_str_mv |
https://purl.org/becyt/ford/3.4 https://purl.org/becyt/ford/3 |
dc.description.none.fl_txt_mv |
This work presents the development and validation of a capillary zone electrophoresis method for calcium ions release quantitation from composite biomaterials with potential application in bone tissue engineering. Calcium ions quantitation was made using a fused silica capillary (40 cm, 75 µm ID) and background electrolyte containing 5 mM imidazole, 6 mM á-hydroxyisobutyric acid, 1 mM 1,4,7,10,13,16-hexaoxacyclo-octadecane and 20 % w/v methanol, at pH 4.5. Indirect UV-detection mode at 214 nm was performed. The separations were achieved using normal polarity at 6 kV, a cartridge temperature of 25 µC and 0.5 psi for 5 s for sample introduction. Parameters of validation such as specificity, linearity, limit of detection and quantitation, accuracy, precision and robustness were evaluated according to the International Conference on Harmonization guidelines. The new developed method resulted to be suitable for calcium determination from composite biomaterials for potential application in bone tissue engineering. Fil: Cattalini, Juan Pablo. Universidad de Buenos Aires. Facultad de Farmacia y Bioquímica. Departamento de Tecnología Farmacéutica; Argentina; Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Houssay; Argentina; Fil: García, Javier. Universidad de Buenos Aires. Facultad de Farmacia y Bioquímica. Departamento de Tecnología Farmacéutica; Argentina; Fil: Mouriño, Viviana Silvia Lourdes. Universidad de Buenos Aires. Facultad de Farmacia y Bioquímica. Departamento de Tecnología Farmacéutica; Argentina; Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Houssay; Argentina; Fil: Lucangioli, Silvia Edith. Universidad de Buenos Aires. Facultad de Farmacia y Bioquímica. Departamento de Tecnología Farmacéutica; Argentina; Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Houssay; Argentina; |
description |
This work presents the development and validation of a capillary zone electrophoresis method for calcium ions release quantitation from composite biomaterials with potential application in bone tissue engineering. Calcium ions quantitation was made using a fused silica capillary (40 cm, 75 µm ID) and background electrolyte containing 5 mM imidazole, 6 mM á-hydroxyisobutyric acid, 1 mM 1,4,7,10,13,16-hexaoxacyclo-octadecane and 20 % w/v methanol, at pH 4.5. Indirect UV-detection mode at 214 nm was performed. The separations were achieved using normal polarity at 6 kV, a cartridge temperature of 25 µC and 0.5 psi for 5 s for sample introduction. Parameters of validation such as specificity, linearity, limit of detection and quantitation, accuracy, precision and robustness were evaluated according to the International Conference on Harmonization guidelines. The new developed method resulted to be suitable for calcium determination from composite biomaterials for potential application in bone tissue engineering. |
publishDate |
2014 |
dc.date.none.fl_str_mv |
2014-10 info:eu-repo/date/embargoEnd/2015-12-01 |
dc.type.none.fl_str_mv |
info:eu-repo/semantics/article info:eu-repo/semantics/publishedVersion http://purl.org/coar/resource_type/c_6501 info:ar-repo/semantics/articulo |
format |
article |
status_str |
publishedVersion |
dc.identifier.none.fl_str_mv |
http://hdl.handle.net/11336/1924 Cattalini, Juan Pablo; García, Javier; Mouriño, Viviana Silvia Lourdes; Lucangioli, Silvia Edith; Development and validation of a Capillary Zone Electrophoresis method for the determination of calcium in composite biomaterials; Bentham Science Publishers; Current Analytical Chemistry; 10; 4; 10-2014; 465-472 1573-4110 http://www.ingentaconnect.com/content/ben/cac/2014/00000010/00000004/art00004?crawler=true#expand/collapse |
url |
http://hdl.handle.net/11336/1924 http://www.ingentaconnect.com/content/ben/cac/2014/00000010/00000004/art00004?crawler=true#expand/collapse |
identifier_str_mv |
Cattalini, Juan Pablo; García, Javier; Mouriño, Viviana Silvia Lourdes; Lucangioli, Silvia Edith; Development and validation of a Capillary Zone Electrophoresis method for the determination of calcium in composite biomaterials; Bentham Science Publishers; Current Analytical Chemistry; 10; 4; 10-2014; 465-472 1573-4110 |
dc.language.none.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
info:eu-repo/semantics/altIdentifier/doi/ 10.2174/15734110113099990038 info:eu-repo/semantics/altIdentifier/url/http://benthamscience.com/journals/current-analytical-chemistry/volume/10/issue/4/page/465/ |
dc.rights.none.fl_str_mv |
info:eu-repo/semantics/embargoedAccess https://creativecommons.org/licenses/by-nc-sa/2.5/ar/ |
eu_rights_str_mv |
embargoedAccess |
rights_invalid_str_mv |
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/ |
dc.format.none.fl_str_mv |
application/pdf application/pdf |
dc.publisher.none.fl_str_mv |
Bentham Science Publishers |
publisher.none.fl_str_mv |
Bentham Science Publishers |
dc.source.none.fl_str_mv |
reponame:CONICET Digital (CONICET) instname:Consejo Nacional de Investigaciones Científicas y Técnicas |
reponame_str |
CONICET Digital (CONICET) |
collection |
CONICET Digital (CONICET) |
instname_str |
Consejo Nacional de Investigaciones Científicas y Técnicas |
repository.name.fl_str_mv |
CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas |
repository.mail.fl_str_mv |
dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar |
_version_ |
1844613178164510720 |
score |
13.070432 |