Structural and elemental X-ray microanalysis with synchrotron radiation in confocal geometry

Autores
Sosa, Carlos Manuel; Sanchez, Hector Jorge; Perez, Carlos A.; Perez, Roberto Daniel
Año de publicación
2014
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
A spectrometer for 3D structural and multielemental X-ray microanalysis with synchrotron radiation is presented in this work. It is based on the combination of the energy dispersive X-ray fluorescence and diffraction with polycapillary optics. The 3D spatial resolution was achieved by the superposition of the foci of two lenses arranged in confocal geometry. The parameters that affect the performance of the spectrometer were study in detail giving rise to a simplified calibration method for depth profile analysis. Two specific examples were included to illustrate the use of the spectrometer in order to identify their possible application fields.
Fil: Sosa, Carlos Manuel. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Instituto de Física Enrique Gaviola. Universidad Nacional de Córdoba. Instituto de Física Enrique Gaviola; Argentina
Fil: Sanchez, Hector Jorge. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Instituto de Física Enrique Gaviola. Universidad Nacional de Córdoba. Instituto de Física Enrique Gaviola; Argentina. Universidad Nacional de Córdoba. Facultad de Matemática, Astronomía y Física; Argentina
Fil: Perez, Carlos A.. Laboratório Nacional de Luz Síncrotron. Campinas; Brasil
Fil: Perez, Roberto Daniel. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Instituto de Física Enrique Gaviola. Universidad Nacional de Córdoba. Instituto de Física Enrique Gaviola; Argentina. Universidad Nacional de Córdoba. Facultad de Matemática, Astronomía y Física; Argentina
Materia
3d X-Ray Microanalysis
Polycapillary Optics
Edxrf
Edxrd
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/31832
Acceder
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repository_id_str 3498
network_name_str CONICET Digital (CONICET)
spelling Structural and elemental X-ray microanalysis with synchrotron radiation in confocal geometrySosa, Carlos ManuelSanchez, Hector JorgePerez, Carlos A.Perez, Roberto Daniel3d X-Ray MicroanalysisPolycapillary OpticsEdxrfEdxrdhttps://purl.org/becyt/ford/1.3https://purl.org/becyt/ford/1A spectrometer for 3D structural and multielemental X-ray microanalysis with synchrotron radiation is presented in this work. It is based on the combination of the energy dispersive X-ray fluorescence and diffraction with polycapillary optics. The 3D spatial resolution was achieved by the superposition of the foci of two lenses arranged in confocal geometry. The parameters that affect the performance of the spectrometer were study in detail giving rise to a simplified calibration method for depth profile analysis. Two specific examples were included to illustrate the use of the spectrometer in order to identify their possible application fields.Fil: Sosa, Carlos Manuel. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Instituto de Física Enrique Gaviola. Universidad Nacional de Córdoba. Instituto de Física Enrique Gaviola; ArgentinaFil: Sanchez, Hector Jorge. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Instituto de Física Enrique Gaviola. Universidad Nacional de Córdoba. Instituto de Física Enrique Gaviola; Argentina. Universidad Nacional de Córdoba. Facultad de Matemática, Astronomía y Física; ArgentinaFil: Perez, Carlos A.. Laboratório Nacional de Luz Síncrotron. Campinas; BrasilFil: Perez, Roberto Daniel. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Instituto de Física Enrique Gaviola. Universidad Nacional de Córdoba. Instituto de Física Enrique Gaviola; Argentina. Universidad Nacional de Córdoba. Facultad de Matemática, Astronomía y Física; ArgentinaElsevier Science2014-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/31832Perez, Roberto Daniel; Perez, Carlos A.; Sanchez, Hector Jorge; Sosa, Carlos Manuel; Structural and elemental X-ray microanalysis with synchrotron radiation in confocal geometry; Elsevier Science; Nuclear Instruments and Methods in Physics Research B: Beam Interactions with Materials and Atoms; 319; 1-2014; 171-1760168-583XCONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/url/http://www.sciencedirect.com/science/article/pii/S0168583X1301046Xinfo:eu-repo/semantics/altIdentifier/doi/10.1016/j.nimb.2013.10.021info:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-sa/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-09-29T09:56:43Zoai:ri.conicet.gov.ar:11336/31832instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-09-29 09:56:44.191CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Structural and elemental X-ray microanalysis with synchrotron radiation in confocal geometry
title Structural and elemental X-ray microanalysis with synchrotron radiation in confocal geometry
spellingShingle Structural and elemental X-ray microanalysis with synchrotron radiation in confocal geometry
Sosa, Carlos Manuel
3d X-Ray Microanalysis
Polycapillary Optics
Edxrf
Edxrd
title_short Structural and elemental X-ray microanalysis with synchrotron radiation in confocal geometry
title_full Structural and elemental X-ray microanalysis with synchrotron radiation in confocal geometry
title_fullStr Structural and elemental X-ray microanalysis with synchrotron radiation in confocal geometry
title_full_unstemmed Structural and elemental X-ray microanalysis with synchrotron radiation in confocal geometry
title_sort Structural and elemental X-ray microanalysis with synchrotron radiation in confocal geometry
dc.creator.none.fl_str_mv Sosa, Carlos Manuel
Sanchez, Hector Jorge
Perez, Carlos A.
Perez, Roberto Daniel
author Sosa, Carlos Manuel
author_facet Sosa, Carlos Manuel
Sanchez, Hector Jorge
Perez, Carlos A.
Perez, Roberto Daniel
author_role author
author2 Sanchez, Hector Jorge
Perez, Carlos A.
Perez, Roberto Daniel
author2_role author
author
author
dc.subject.none.fl_str_mv 3d X-Ray Microanalysis
Polycapillary Optics
Edxrf
Edxrd
topic 3d X-Ray Microanalysis
Polycapillary Optics
Edxrf
Edxrd
purl_subject.fl_str_mv https://purl.org/becyt/ford/1.3
https://purl.org/becyt/ford/1
dc.description.none.fl_txt_mv A spectrometer for 3D structural and multielemental X-ray microanalysis with synchrotron radiation is presented in this work. It is based on the combination of the energy dispersive X-ray fluorescence and diffraction with polycapillary optics. The 3D spatial resolution was achieved by the superposition of the foci of two lenses arranged in confocal geometry. The parameters that affect the performance of the spectrometer were study in detail giving rise to a simplified calibration method for depth profile analysis. Two specific examples were included to illustrate the use of the spectrometer in order to identify their possible application fields.
Fil: Sosa, Carlos Manuel. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Instituto de Física Enrique Gaviola. Universidad Nacional de Córdoba. Instituto de Física Enrique Gaviola; Argentina
Fil: Sanchez, Hector Jorge. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Instituto de Física Enrique Gaviola. Universidad Nacional de Córdoba. Instituto de Física Enrique Gaviola; Argentina. Universidad Nacional de Córdoba. Facultad de Matemática, Astronomía y Física; Argentina
Fil: Perez, Carlos A.. Laboratório Nacional de Luz Síncrotron. Campinas; Brasil
Fil: Perez, Roberto Daniel. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Instituto de Física Enrique Gaviola. Universidad Nacional de Córdoba. Instituto de Física Enrique Gaviola; Argentina. Universidad Nacional de Córdoba. Facultad de Matemática, Astronomía y Física; Argentina
description A spectrometer for 3D structural and multielemental X-ray microanalysis with synchrotron radiation is presented in this work. It is based on the combination of the energy dispersive X-ray fluorescence and diffraction with polycapillary optics. The 3D spatial resolution was achieved by the superposition of the foci of two lenses arranged in confocal geometry. The parameters that affect the performance of the spectrometer were study in detail giving rise to a simplified calibration method for depth profile analysis. Two specific examples were included to illustrate the use of the spectrometer in order to identify their possible application fields.
publishDate 2014
dc.date.none.fl_str_mv 2014-01
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/31832
Perez, Roberto Daniel; Perez, Carlos A.; Sanchez, Hector Jorge; Sosa, Carlos Manuel; Structural and elemental X-ray microanalysis with synchrotron radiation in confocal geometry; Elsevier Science; Nuclear Instruments and Methods in Physics Research B: Beam Interactions with Materials and Atoms; 319; 1-2014; 171-176
0168-583X
CONICET Digital
CONICET
url http://hdl.handle.net/11336/31832
identifier_str_mv Perez, Roberto Daniel; Perez, Carlos A.; Sanchez, Hector Jorge; Sosa, Carlos Manuel; Structural and elemental X-ray microanalysis with synchrotron radiation in confocal geometry; Elsevier Science; Nuclear Instruments and Methods in Physics Research B: Beam Interactions with Materials and Atoms; 319; 1-2014; 171-176
0168-583X
CONICET Digital
CONICET
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/url/http://www.sciencedirect.com/science/article/pii/S0168583X1301046X
info:eu-repo/semantics/altIdentifier/doi/10.1016/j.nimb.2013.10.021
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
application/pdf
application/pdf
dc.publisher.none.fl_str_mv Elsevier Science
publisher.none.fl_str_mv Elsevier Science
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
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score 13.070432

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