Carbonitriding of ZrO2: relation between the weight loss and crystalline phase evolution during reaction

Autores
Tamborenea, Silvina Alejandra; Mazzoni, Alfredo Daniel; Aglietti, Esteban Fausto
Año de publicación
2005
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
Carbonitriding reactions of ZrO2 permit to obtain Zr(C,O,N) phases that belong to the pseudoternary “ZrO–ZrN–ZrC” system. The Zr(C,O,N) phase has cubic crystalline structure with a0 parameter depending on the C, O and N content. The formation reaction of the Zr(C,O,N) phases was followed using X-ray diffraction (XRD) and the weight loss (WL) data. The reaction was studied employing different carbon contents (15–31%) at temperatures from 1400 to 1650 ◦C. The -phase (Zr7O9.5N3.0) was the unique secondary product formed. The crystallite sizes of the zirconium phases were also determined by XRD. Some samples were analyzed using the Rietveld method with silicon as internal standard. Using the carbonitriding process a Zr(C,O,N) phase was obtained and the loss weight is a parameter permitting to control the reaction products. The oxidation resistance of the Zr(C,O,N) phase was studied employing differential thermal analysis (DTA)–thermogravimetric analysis (TG) techniques. Additionally, microstructure analysis of raw materials and reaction products were performed by scanning electronic microscopy (SEM). The reaction was studied employing different carbon contents (15¨C31%) at temperatures from 1400 to 1650 ¡ãC. The ¦Â¡å-phase (Zr7O9.5N3.0) was the unique secondary product formed. The crystallite sizes of the zirconium phases were also determined by XRD. Some samples were analyzed using the Rietveld method with silicon as internal standard. Using the carbonitriding process a Zr(C,O,N) phase was obtained and the loss weight is a parameter permitting to control the reaction products. The oxidation resistance of the Zr(C,O,N) phase was studied employing differential thermal analysis (DTA)¨Cthermogravimetric analysis (TG) techniques. Additionally, microstructure analysis of raw materials and reaction products were performed by scanning electronic microscopy (SEM).
Fil: Tamborenea, Silvina Alejandra. Provincia de Buenos Aires. Gobernación. Comisión de Investigaciones Científicas. Centro de Tecnología de Recursos Minerales y Cerámica. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Centro de Tecnología de Recursos Minerales y Cerámica; Argentina
Fil: Mazzoni, Alfredo Daniel. Provincia de Buenos Aires. Gobernación. Comisión de Investigaciones Científicas. Centro de Tecnología de Recursos Minerales y Cerámica. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Centro de Tecnología de Recursos Minerales y Cerámica; Argentina. Universidad Nacional de La Plata; Argentina
Fil: Aglietti, Esteban Fausto. Provincia de Buenos Aires. Gobernación. Comisión de Investigaciones Científicas. Centro de Tecnología de Recursos Minerales y Cerámica. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Centro de Tecnología de Recursos Minerales y Cerámica; Argentina. Universidad Nacional de La Plata; Argentina
Materia
Ceramics
Zirconia
Nitriding
Nivel de accesibilidad
acceso abierto
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CONICET Digital (CONICET)
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Consejo Nacional de Investigaciones Científicas y Técnicas
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network_name_str CONICET Digital (CONICET)
spelling Carbonitriding of ZrO2: relation between the weight loss and crystalline phase evolution during reactionTamborenea, Silvina AlejandraMazzoni, Alfredo DanielAglietti, Esteban FaustoCeramicsZirconiaNitridinghttps://purl.org/becyt/ford/2.5https://purl.org/becyt/ford/2Carbonitriding reactions of ZrO2 permit to obtain Zr(C,O,N) phases that belong to the pseudoternary “ZrO–ZrN–ZrC” system. The Zr(C,O,N) phase has cubic crystalline structure with a0 parameter depending on the C, O and N content. The formation reaction of the Zr(C,O,N) phases was followed using X-ray diffraction (XRD) and the weight loss (WL) data. The reaction was studied employing different carbon contents (15–31%) at temperatures from 1400 to 1650 ◦C. The -phase (Zr7O9.5N3.0) was the unique secondary product formed. The crystallite sizes of the zirconium phases were also determined by XRD. Some samples were analyzed using the Rietveld method with silicon as internal standard. Using the carbonitriding process a Zr(C,O,N) phase was obtained and the loss weight is a parameter permitting to control the reaction products. The oxidation resistance of the Zr(C,O,N) phase was studied employing differential thermal analysis (DTA)–thermogravimetric analysis (TG) techniques. Additionally, microstructure analysis of raw materials and reaction products were performed by scanning electronic microscopy (SEM). The reaction was studied employing different carbon contents (15¨C31%) at temperatures from 1400 to 1650 ¡ãC. The ¦Â¡å-phase (Zr7O9.5N3.0) was the unique secondary product formed. The crystallite sizes of the zirconium phases were also determined by XRD. Some samples were analyzed using the Rietveld method with silicon as internal standard. Using the carbonitriding process a Zr(C,O,N) phase was obtained and the loss weight is a parameter permitting to control the reaction products. The oxidation resistance of the Zr(C,O,N) phase was studied employing differential thermal analysis (DTA)¨Cthermogravimetric analysis (TG) techniques. Additionally, microstructure analysis of raw materials and reaction products were performed by scanning electronic microscopy (SEM).Fil: Tamborenea, Silvina Alejandra. Provincia de Buenos Aires. Gobernación. Comisión de Investigaciones Científicas. Centro de Tecnología de Recursos Minerales y Cerámica. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Centro de Tecnología de Recursos Minerales y Cerámica; ArgentinaFil: Mazzoni, Alfredo Daniel. Provincia de Buenos Aires. Gobernación. Comisión de Investigaciones Científicas. Centro de Tecnología de Recursos Minerales y Cerámica. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Centro de Tecnología de Recursos Minerales y Cerámica; Argentina. Universidad Nacional de La Plata; ArgentinaFil: Aglietti, Esteban Fausto. Provincia de Buenos Aires. Gobernación. Comisión de Investigaciones Científicas. Centro de Tecnología de Recursos Minerales y Cerámica. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Centro de Tecnología de Recursos Minerales y Cerámica; Argentina. Universidad Nacional de La Plata; ArgentinaElsevier Science SA2005-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/279339Tamborenea, Silvina Alejandra; Mazzoni, Alfredo Daniel; Aglietti, Esteban Fausto; Carbonitriding of ZrO2: relation between the weight loss and crystalline phase evolution during reaction; Elsevier Science SA; Materials Chemistry and Physics; 89; 1; 1-2005; 164-1690254-0584CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/url/https://www.sciencedirect.com/science/article/abs/pii/S0254058404004304info:eu-repo/semantics/altIdentifier/doi/10.1016/j.matchemphys.2004.09.001info:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-sa/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2026-02-26T10:20:37Zoai:ri.conicet.gov.ar:11336/279339instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982026-02-26 10:20:37.337CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Carbonitriding of ZrO2: relation between the weight loss and crystalline phase evolution during reaction
title Carbonitriding of ZrO2: relation between the weight loss and crystalline phase evolution during reaction
spellingShingle Carbonitriding of ZrO2: relation between the weight loss and crystalline phase evolution during reaction
Tamborenea, Silvina Alejandra
Ceramics
Zirconia
Nitriding
title_short Carbonitriding of ZrO2: relation between the weight loss and crystalline phase evolution during reaction
title_full Carbonitriding of ZrO2: relation between the weight loss and crystalline phase evolution during reaction
title_fullStr Carbonitriding of ZrO2: relation between the weight loss and crystalline phase evolution during reaction
title_full_unstemmed Carbonitriding of ZrO2: relation between the weight loss and crystalline phase evolution during reaction
title_sort Carbonitriding of ZrO2: relation between the weight loss and crystalline phase evolution during reaction
dc.creator.none.fl_str_mv Tamborenea, Silvina Alejandra
Mazzoni, Alfredo Daniel
Aglietti, Esteban Fausto
author Tamborenea, Silvina Alejandra
author_facet Tamborenea, Silvina Alejandra
Mazzoni, Alfredo Daniel
Aglietti, Esteban Fausto
author_role author
author2 Mazzoni, Alfredo Daniel
Aglietti, Esteban Fausto
author2_role author
author
dc.subject.none.fl_str_mv Ceramics
Zirconia
Nitriding
topic Ceramics
Zirconia
Nitriding
purl_subject.fl_str_mv https://purl.org/becyt/ford/2.5
https://purl.org/becyt/ford/2
dc.description.none.fl_txt_mv Carbonitriding reactions of ZrO2 permit to obtain Zr(C,O,N) phases that belong to the pseudoternary “ZrO–ZrN–ZrC” system. The Zr(C,O,N) phase has cubic crystalline structure with a0 parameter depending on the C, O and N content. The formation reaction of the Zr(C,O,N) phases was followed using X-ray diffraction (XRD) and the weight loss (WL) data. The reaction was studied employing different carbon contents (15–31%) at temperatures from 1400 to 1650 ◦C. The -phase (Zr7O9.5N3.0) was the unique secondary product formed. The crystallite sizes of the zirconium phases were also determined by XRD. Some samples were analyzed using the Rietveld method with silicon as internal standard. Using the carbonitriding process a Zr(C,O,N) phase was obtained and the loss weight is a parameter permitting to control the reaction products. The oxidation resistance of the Zr(C,O,N) phase was studied employing differential thermal analysis (DTA)–thermogravimetric analysis (TG) techniques. Additionally, microstructure analysis of raw materials and reaction products were performed by scanning electronic microscopy (SEM). The reaction was studied employing different carbon contents (15¨C31%) at temperatures from 1400 to 1650 ¡ãC. The ¦Â¡å-phase (Zr7O9.5N3.0) was the unique secondary product formed. The crystallite sizes of the zirconium phases were also determined by XRD. Some samples were analyzed using the Rietveld method with silicon as internal standard. Using the carbonitriding process a Zr(C,O,N) phase was obtained and the loss weight is a parameter permitting to control the reaction products. The oxidation resistance of the Zr(C,O,N) phase was studied employing differential thermal analysis (DTA)¨Cthermogravimetric analysis (TG) techniques. Additionally, microstructure analysis of raw materials and reaction products were performed by scanning electronic microscopy (SEM).
Fil: Tamborenea, Silvina Alejandra. Provincia de Buenos Aires. Gobernación. Comisión de Investigaciones Científicas. Centro de Tecnología de Recursos Minerales y Cerámica. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Centro de Tecnología de Recursos Minerales y Cerámica; Argentina
Fil: Mazzoni, Alfredo Daniel. Provincia de Buenos Aires. Gobernación. Comisión de Investigaciones Científicas. Centro de Tecnología de Recursos Minerales y Cerámica. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Centro de Tecnología de Recursos Minerales y Cerámica; Argentina. Universidad Nacional de La Plata; Argentina
Fil: Aglietti, Esteban Fausto. Provincia de Buenos Aires. Gobernación. Comisión de Investigaciones Científicas. Centro de Tecnología de Recursos Minerales y Cerámica. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Centro de Tecnología de Recursos Minerales y Cerámica; Argentina. Universidad Nacional de La Plata; Argentina
description Carbonitriding reactions of ZrO2 permit to obtain Zr(C,O,N) phases that belong to the pseudoternary “ZrO–ZrN–ZrC” system. The Zr(C,O,N) phase has cubic crystalline structure with a0 parameter depending on the C, O and N content. The formation reaction of the Zr(C,O,N) phases was followed using X-ray diffraction (XRD) and the weight loss (WL) data. The reaction was studied employing different carbon contents (15–31%) at temperatures from 1400 to 1650 ◦C. The -phase (Zr7O9.5N3.0) was the unique secondary product formed. The crystallite sizes of the zirconium phases were also determined by XRD. Some samples were analyzed using the Rietveld method with silicon as internal standard. Using the carbonitriding process a Zr(C,O,N) phase was obtained and the loss weight is a parameter permitting to control the reaction products. The oxidation resistance of the Zr(C,O,N) phase was studied employing differential thermal analysis (DTA)–thermogravimetric analysis (TG) techniques. Additionally, microstructure analysis of raw materials and reaction products were performed by scanning electronic microscopy (SEM). The reaction was studied employing different carbon contents (15¨C31%) at temperatures from 1400 to 1650 ¡ãC. The ¦Â¡å-phase (Zr7O9.5N3.0) was the unique secondary product formed. The crystallite sizes of the zirconium phases were also determined by XRD. Some samples were analyzed using the Rietveld method with silicon as internal standard. Using the carbonitriding process a Zr(C,O,N) phase was obtained and the loss weight is a parameter permitting to control the reaction products. The oxidation resistance of the Zr(C,O,N) phase was studied employing differential thermal analysis (DTA)¨Cthermogravimetric analysis (TG) techniques. Additionally, microstructure analysis of raw materials and reaction products were performed by scanning electronic microscopy (SEM).
publishDate 2005
dc.date.none.fl_str_mv 2005-01
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/279339
Tamborenea, Silvina Alejandra; Mazzoni, Alfredo Daniel; Aglietti, Esteban Fausto; Carbonitriding of ZrO2: relation between the weight loss and crystalline phase evolution during reaction; Elsevier Science SA; Materials Chemistry and Physics; 89; 1; 1-2005; 164-169
0254-0584
CONICET Digital
CONICET
url http://hdl.handle.net/11336/279339
identifier_str_mv Tamborenea, Silvina Alejandra; Mazzoni, Alfredo Daniel; Aglietti, Esteban Fausto; Carbonitriding of ZrO2: relation between the weight loss and crystalline phase evolution during reaction; Elsevier Science SA; Materials Chemistry and Physics; 89; 1; 1-2005; 164-169
0254-0584
CONICET Digital
CONICET
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/url/https://www.sciencedirect.com/science/article/abs/pii/S0254058404004304
info:eu-repo/semantics/altIdentifier/doi/10.1016/j.matchemphys.2004.09.001
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
application/pdf
dc.publisher.none.fl_str_mv Elsevier Science SA
publisher.none.fl_str_mv Elsevier Science SA
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
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