Optimization of antioxidant, mechanical and chemical physical properties of chitosan-sorbitol-gallic acid films by response surface methodology

Autores
Raspo, Matías Alejandro; Gomez, Cesar Gerardo; Andreatta, Alfonsina Ester
Año de publicación
2018
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
The interest in the development of biodegradable films is increasing, which is related to the wide availability of resources and methods of synthesis to generate them. For this reason, in this study, the preparation of films containing chitosan, sorbitol and gallic acid this study was proposed. The incorporation of natural antioxidants into films modifies their structure and provides new functionality to them. In order to determine the optimal content of sorbitol and gallic acid in the formulation of the chitosan films to obtain the highest antioxidant capacity and the best mechanical properties, an experimental design based on a two-factor Doehlert model was used. The optimum condition of film synthesis was obtained when a mixture of 1 wt chitosan, 3.62 wt% of sorbitol and 1 wt% of gallic acid was performed. The properties studied were experimentally evaluated at this optimal point and compared with the model predictions, showing good results. It proved to be a promising material to be successfully used as packaging material.
Fil: Raspo, Matías Alejandro. Universidad Tecnológica Nacional; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Bahía Blanca. Planta Piloto de Ingeniería Química (I). Grupo Vinculado al Plapiqui - Investigación y Desarrollo en Tecnología Química; Argentina
Fil: Gomez, Cesar Gerardo. Universidad Nacional de Córdoba. Facultad de Ciencias Químicas. Departamento de Química Orgánica; Argentina. Universidad Nacional de Córdoba. Instituto de Investigación y Desarrollo en Ingeniería de Procesos y Química Aplicada. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Instituto de Investigación y Desarrollo en Ingeniería de Procesos y Química Aplicada; Argentina
Fil: Andreatta, Alfonsina Ester. Universidad Tecnológica Nacional; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Bahía Blanca. Planta Piloto de Ingeniería Química (I). Grupo Vinculado al Plapiqui - Investigación y Desarrollo en Tecnología Química; Argentina
Materia
CHITOSAN
FILMS
GALLIC ACID
RESPONSE SURFACE METHODOLOGY
SORBITOL
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/92528
Acceder
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oai_identifier_str oai:ri.conicet.gov.ar:11336/92528
network_acronym_str CONICETDig
repository_id_str 3498
network_name_str CONICET Digital (CONICET)
spelling Optimization of antioxidant, mechanical and chemical physical properties of chitosan-sorbitol-gallic acid films by response surface methodologyRaspo, Matías AlejandroGomez, Cesar GerardoAndreatta, Alfonsina EsterCHITOSANFILMSGALLIC ACIDRESPONSE SURFACE METHODOLOGYSORBITOLhttps://purl.org/becyt/ford/2.4https://purl.org/becyt/ford/2The interest in the development of biodegradable films is increasing, which is related to the wide availability of resources and methods of synthesis to generate them. For this reason, in this study, the preparation of films containing chitosan, sorbitol and gallic acid this study was proposed. The incorporation of natural antioxidants into films modifies their structure and provides new functionality to them. In order to determine the optimal content of sorbitol and gallic acid in the formulation of the chitosan films to obtain the highest antioxidant capacity and the best mechanical properties, an experimental design based on a two-factor Doehlert model was used. The optimum condition of film synthesis was obtained when a mixture of 1 wt chitosan, 3.62 wt% of sorbitol and 1 wt% of gallic acid was performed. The properties studied were experimentally evaluated at this optimal point and compared with the model predictions, showing good results. It proved to be a promising material to be successfully used as packaging material.Fil: Raspo, Matías Alejandro. Universidad Tecnológica Nacional; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Bahía Blanca. Planta Piloto de Ingeniería Química (I). Grupo Vinculado al Plapiqui - Investigación y Desarrollo en Tecnología Química; ArgentinaFil: Gomez, Cesar Gerardo. Universidad Nacional de Córdoba. Facultad de Ciencias Químicas. Departamento de Química Orgánica; Argentina. Universidad Nacional de Córdoba. Instituto de Investigación y Desarrollo en Ingeniería de Procesos y Química Aplicada. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Instituto de Investigación y Desarrollo en Ingeniería de Procesos y Química Aplicada; ArgentinaFil: Andreatta, Alfonsina Ester. Universidad Tecnológica Nacional; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Bahía Blanca. Planta Piloto de Ingeniería Química (I). Grupo Vinculado al Plapiqui - Investigación y Desarrollo en Tecnología Química; ArgentinaElsevier2018-09info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/92528Raspo, Matías Alejandro; Gomez, Cesar Gerardo; Andreatta, Alfonsina Ester; Optimization of antioxidant, mechanical and chemical physical properties of chitosan-sorbitol-gallic acid films by response surface methodology; Elsevier; Polymer Testing; 70; 9-2018; 180-1870142-9418CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/url/https://linkinghub.elsevier.com/retrieve/pii/S014294181830583Xinfo:eu-repo/semantics/altIdentifier/doi/10.1016/j.polymertesting.2018.07.003info:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-nd/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-10-15T15:28:23Zoai:ri.conicet.gov.ar:11336/92528instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-10-15 15:28:23.271CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Optimization of antioxidant, mechanical and chemical physical properties of chitosan-sorbitol-gallic acid films by response surface methodology
title Optimization of antioxidant, mechanical and chemical physical properties of chitosan-sorbitol-gallic acid films by response surface methodology
spellingShingle Optimization of antioxidant, mechanical and chemical physical properties of chitosan-sorbitol-gallic acid films by response surface methodology
Raspo, Matías Alejandro
CHITOSAN
FILMS
GALLIC ACID
RESPONSE SURFACE METHODOLOGY
SORBITOL
title_short Optimization of antioxidant, mechanical and chemical physical properties of chitosan-sorbitol-gallic acid films by response surface methodology
title_full Optimization of antioxidant, mechanical and chemical physical properties of chitosan-sorbitol-gallic acid films by response surface methodology
title_fullStr Optimization of antioxidant, mechanical and chemical physical properties of chitosan-sorbitol-gallic acid films by response surface methodology
title_full_unstemmed Optimization of antioxidant, mechanical and chemical physical properties of chitosan-sorbitol-gallic acid films by response surface methodology
title_sort Optimization of antioxidant, mechanical and chemical physical properties of chitosan-sorbitol-gallic acid films by response surface methodology
dc.creator.none.fl_str_mv Raspo, Matías Alejandro
Gomez, Cesar Gerardo
Andreatta, Alfonsina Ester
author Raspo, Matías Alejandro
author_facet Raspo, Matías Alejandro
Gomez, Cesar Gerardo
Andreatta, Alfonsina Ester
author_role author
author2 Gomez, Cesar Gerardo
Andreatta, Alfonsina Ester
author2_role author
author
dc.subject.none.fl_str_mv CHITOSAN
FILMS
GALLIC ACID
RESPONSE SURFACE METHODOLOGY
SORBITOL
topic CHITOSAN
FILMS
GALLIC ACID
RESPONSE SURFACE METHODOLOGY
SORBITOL
purl_subject.fl_str_mv https://purl.org/becyt/ford/2.4
https://purl.org/becyt/ford/2
dc.description.none.fl_txt_mv The interest in the development of biodegradable films is increasing, which is related to the wide availability of resources and methods of synthesis to generate them. For this reason, in this study, the preparation of films containing chitosan, sorbitol and gallic acid this study was proposed. The incorporation of natural antioxidants into films modifies their structure and provides new functionality to them. In order to determine the optimal content of sorbitol and gallic acid in the formulation of the chitosan films to obtain the highest antioxidant capacity and the best mechanical properties, an experimental design based on a two-factor Doehlert model was used. The optimum condition of film synthesis was obtained when a mixture of 1 wt chitosan, 3.62 wt% of sorbitol and 1 wt% of gallic acid was performed. The properties studied were experimentally evaluated at this optimal point and compared with the model predictions, showing good results. It proved to be a promising material to be successfully used as packaging material.
Fil: Raspo, Matías Alejandro. Universidad Tecnológica Nacional; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Bahía Blanca. Planta Piloto de Ingeniería Química (I). Grupo Vinculado al Plapiqui - Investigación y Desarrollo en Tecnología Química; Argentina
Fil: Gomez, Cesar Gerardo. Universidad Nacional de Córdoba. Facultad de Ciencias Químicas. Departamento de Química Orgánica; Argentina. Universidad Nacional de Córdoba. Instituto de Investigación y Desarrollo en Ingeniería de Procesos y Química Aplicada. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Instituto de Investigación y Desarrollo en Ingeniería de Procesos y Química Aplicada; Argentina
Fil: Andreatta, Alfonsina Ester. Universidad Tecnológica Nacional; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Bahía Blanca. Planta Piloto de Ingeniería Química (I). Grupo Vinculado al Plapiqui - Investigación y Desarrollo en Tecnología Química; Argentina
description The interest in the development of biodegradable films is increasing, which is related to the wide availability of resources and methods of synthesis to generate them. For this reason, in this study, the preparation of films containing chitosan, sorbitol and gallic acid this study was proposed. The incorporation of natural antioxidants into films modifies their structure and provides new functionality to them. In order to determine the optimal content of sorbitol and gallic acid in the formulation of the chitosan films to obtain the highest antioxidant capacity and the best mechanical properties, an experimental design based on a two-factor Doehlert model was used. The optimum condition of film synthesis was obtained when a mixture of 1 wt chitosan, 3.62 wt% of sorbitol and 1 wt% of gallic acid was performed. The properties studied were experimentally evaluated at this optimal point and compared with the model predictions, showing good results. It proved to be a promising material to be successfully used as packaging material.
publishDate 2018
dc.date.none.fl_str_mv 2018-09
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/92528
Raspo, Matías Alejandro; Gomez, Cesar Gerardo; Andreatta, Alfonsina Ester; Optimization of antioxidant, mechanical and chemical physical properties of chitosan-sorbitol-gallic acid films by response surface methodology; Elsevier; Polymer Testing; 70; 9-2018; 180-187
0142-9418
CONICET Digital
CONICET
url http://hdl.handle.net/11336/92528
identifier_str_mv Raspo, Matías Alejandro; Gomez, Cesar Gerardo; Andreatta, Alfonsina Ester; Optimization of antioxidant, mechanical and chemical physical properties of chitosan-sorbitol-gallic acid films by response surface methodology; Elsevier; Polymer Testing; 70; 9-2018; 180-187
0142-9418
CONICET Digital
CONICET
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/url/https://linkinghub.elsevier.com/retrieve/pii/S014294181830583X
info:eu-repo/semantics/altIdentifier/doi/10.1016/j.polymertesting.2018.07.003
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
application/pdf
application/pdf
dc.publisher.none.fl_str_mv Elsevier
publisher.none.fl_str_mv Elsevier
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
_version_ 1846083424093208576
score 13.221938

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