Review of the characterization of sodium alginate by intrinsic viscosity measurements: Comparative analysis between conventional and single point methods

Autores
Masuelli, Martin Alberto; Illanes, Cristian Omar
Año de publicación
2014
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
In the pharmaceutical and food industry, alginate is used in aqueous solutions and excipients as thickener, gelling agent, coagulant and encapsulant. This biopolymer is very important, with many key industrial applications, especially if the intrinsic viscosity [η] and the viscometric molecular weight (Mv) are known. Alginate is obtained from the cell walls of algae such as Macrocystis pyrifera, Laminaria hyperborea, Laminaria digitata, Laminaria japonica, Sargassum vulgare, etc.; bacteria such as Pseudomonas aeruginosa and Azotobacter vinelandii can also synthesize it. This work studied alginate in aqueous solution from 0.25 to 1% wt., measuring its intrinsic viscosity in order to obtain its Mv. The intrinsic viscosity is calculated by the classical methods of Huggins, Kremer, Schulz-Blashke and Martin. We compared several single point methods to determine which of them would be more appropriate for an alginate-water system. We also obtained Mark-Houwink parameters and the corresponding viscometric molecular weight.
Fil: Masuelli, Martin Alberto. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - San Luis. Instituto de Física Aplicada "Dr. Jorge Andrés Zgrablich". Universidad Nacional de San Luis. Facultad de Ciencias Físico Matemáticas y Naturales. Instituto de Física Aplicada "Dr. Jorge Andrés Zgrablich"; Argentina
Fil: Illanes, Cristian Omar. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - San Luis. Instituto de Física Aplicada "Dr. Jorge Andrés Zgrablich". Universidad Nacional de San Luis. Facultad de Ciencias Físico Matemáticas y Naturales. Instituto de Física Aplicada "Dr. Jorge Andrés Zgrablich"; Argentina
Materia
Alginate
Intrinsic Viscosity
Molecular weight
Single point methods
Hydrodynamic
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/69467
Acceder
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network_acronym_str CONICETDig
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network_name_str CONICET Digital (CONICET)
spelling Review of the characterization of sodium alginate by intrinsic viscosity measurements: Comparative analysis between conventional and single point methodsMasuelli, Martin AlbertoIllanes, Cristian OmarAlginateIntrinsic ViscosityMolecular weightSingle point methodsHydrodynamichttps://purl.org/becyt/ford/1.3https://purl.org/becyt/ford/1In the pharmaceutical and food industry, alginate is used in aqueous solutions and excipients as thickener, gelling agent, coagulant and encapsulant. This biopolymer is very important, with many key industrial applications, especially if the intrinsic viscosity [η] and the viscometric molecular weight (Mv) are known. Alginate is obtained from the cell walls of algae such as Macrocystis pyrifera, Laminaria hyperborea, Laminaria digitata, Laminaria japonica, Sargassum vulgare, etc.; bacteria such as Pseudomonas aeruginosa and Azotobacter vinelandii can also synthesize it. This work studied alginate in aqueous solution from 0.25 to 1% wt., measuring its intrinsic viscosity in order to obtain its Mv. The intrinsic viscosity is calculated by the classical methods of Huggins, Kremer, Schulz-Blashke and Martin. We compared several single point methods to determine which of them would be more appropriate for an alginate-water system. We also obtained Mark-Houwink parameters and the corresponding viscometric molecular weight.Fil: Masuelli, Martin Alberto. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - San Luis. Instituto de Física Aplicada "Dr. Jorge Andrés Zgrablich". Universidad Nacional de San Luis. Facultad de Ciencias Físico Matemáticas y Naturales. Instituto de Física Aplicada "Dr. Jorge Andrés Zgrablich"; ArgentinaFil: Illanes, Cristian Omar. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - San Luis. Instituto de Física Aplicada "Dr. Jorge Andrés Zgrablich". Universidad Nacional de San Luis. Facultad de Ciencias Físico Matemáticas y Naturales. Instituto de Física Aplicada "Dr. Jorge Andrés Zgrablich"; ArgentinaOpen Science Publishing2014-05info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/69467Masuelli, Martin Alberto; Illanes, Cristian Omar; Review of the characterization of sodium alginate by intrinsic viscosity measurements: Comparative analysis between conventional and single point methods; Open Science Publishing; International Journal of Biomaterials Science and Engineering; 1; 1; 5-2014; 1-112381-3806CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/url/http://www.openscienceonline.com/journal/archive2?journalId=732&paperId=533info:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-sa/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-09-29T10:13:51Zoai:ri.conicet.gov.ar:11336/69467instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-09-29 10:13:52.201CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Review of the characterization of sodium alginate by intrinsic viscosity measurements: Comparative analysis between conventional and single point methods
title Review of the characterization of sodium alginate by intrinsic viscosity measurements: Comparative analysis between conventional and single point methods
spellingShingle Review of the characterization of sodium alginate by intrinsic viscosity measurements: Comparative analysis between conventional and single point methods
Masuelli, Martin Alberto
Alginate
Intrinsic Viscosity
Molecular weight
Single point methods
Hydrodynamic
title_short Review of the characterization of sodium alginate by intrinsic viscosity measurements: Comparative analysis between conventional and single point methods
title_full Review of the characterization of sodium alginate by intrinsic viscosity measurements: Comparative analysis between conventional and single point methods
title_fullStr Review of the characterization of sodium alginate by intrinsic viscosity measurements: Comparative analysis between conventional and single point methods
title_full_unstemmed Review of the characterization of sodium alginate by intrinsic viscosity measurements: Comparative analysis between conventional and single point methods
title_sort Review of the characterization of sodium alginate by intrinsic viscosity measurements: Comparative analysis between conventional and single point methods
dc.creator.none.fl_str_mv Masuelli, Martin Alberto
Illanes, Cristian Omar
author Masuelli, Martin Alberto
author_facet Masuelli, Martin Alberto
Illanes, Cristian Omar
author_role author
author2 Illanes, Cristian Omar
author2_role author
dc.subject.none.fl_str_mv Alginate
Intrinsic Viscosity
Molecular weight
Single point methods
Hydrodynamic
topic Alginate
Intrinsic Viscosity
Molecular weight
Single point methods
Hydrodynamic
purl_subject.fl_str_mv https://purl.org/becyt/ford/1.3
https://purl.org/becyt/ford/1
dc.description.none.fl_txt_mv In the pharmaceutical and food industry, alginate is used in aqueous solutions and excipients as thickener, gelling agent, coagulant and encapsulant. This biopolymer is very important, with many key industrial applications, especially if the intrinsic viscosity [η] and the viscometric molecular weight (Mv) are known. Alginate is obtained from the cell walls of algae such as Macrocystis pyrifera, Laminaria hyperborea, Laminaria digitata, Laminaria japonica, Sargassum vulgare, etc.; bacteria such as Pseudomonas aeruginosa and Azotobacter vinelandii can also synthesize it. This work studied alginate in aqueous solution from 0.25 to 1% wt., measuring its intrinsic viscosity in order to obtain its Mv. The intrinsic viscosity is calculated by the classical methods of Huggins, Kremer, Schulz-Blashke and Martin. We compared several single point methods to determine which of them would be more appropriate for an alginate-water system. We also obtained Mark-Houwink parameters and the corresponding viscometric molecular weight.
Fil: Masuelli, Martin Alberto. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - San Luis. Instituto de Física Aplicada "Dr. Jorge Andrés Zgrablich". Universidad Nacional de San Luis. Facultad de Ciencias Físico Matemáticas y Naturales. Instituto de Física Aplicada "Dr. Jorge Andrés Zgrablich"; Argentina
Fil: Illanes, Cristian Omar. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - San Luis. Instituto de Física Aplicada "Dr. Jorge Andrés Zgrablich". Universidad Nacional de San Luis. Facultad de Ciencias Físico Matemáticas y Naturales. Instituto de Física Aplicada "Dr. Jorge Andrés Zgrablich"; Argentina
description In the pharmaceutical and food industry, alginate is used in aqueous solutions and excipients as thickener, gelling agent, coagulant and encapsulant. This biopolymer is very important, with many key industrial applications, especially if the intrinsic viscosity [η] and the viscometric molecular weight (Mv) are known. Alginate is obtained from the cell walls of algae such as Macrocystis pyrifera, Laminaria hyperborea, Laminaria digitata, Laminaria japonica, Sargassum vulgare, etc.; bacteria such as Pseudomonas aeruginosa and Azotobacter vinelandii can also synthesize it. This work studied alginate in aqueous solution from 0.25 to 1% wt., measuring its intrinsic viscosity in order to obtain its Mv. The intrinsic viscosity is calculated by the classical methods of Huggins, Kremer, Schulz-Blashke and Martin. We compared several single point methods to determine which of them would be more appropriate for an alginate-water system. We also obtained Mark-Houwink parameters and the corresponding viscometric molecular weight.
publishDate 2014
dc.date.none.fl_str_mv 2014-05
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/69467
Masuelli, Martin Alberto; Illanes, Cristian Omar; Review of the characterization of sodium alginate by intrinsic viscosity measurements: Comparative analysis between conventional and single point methods; Open Science Publishing; International Journal of Biomaterials Science and Engineering; 1; 1; 5-2014; 1-11
2381-3806
CONICET Digital
CONICET
url http://hdl.handle.net/11336/69467
identifier_str_mv Masuelli, Martin Alberto; Illanes, Cristian Omar; Review of the characterization of sodium alginate by intrinsic viscosity measurements: Comparative analysis between conventional and single point methods; Open Science Publishing; International Journal of Biomaterials Science and Engineering; 1; 1; 5-2014; 1-11
2381-3806
CONICET Digital
CONICET
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/url/http://www.openscienceonline.com/journal/archive2?journalId=732&paperId=533
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
dc.publisher.none.fl_str_mv Open Science Publishing
publisher.none.fl_str_mv Open Science Publishing
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
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score 13.070432

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