Volumetric Method for Free and Total Glycerin Determination in Biodiesel

Autores
Pisarello Milesi, Maria Laura; Dalla Costa, Bruno Oscar; Veizaga, Natalia Soledad; Querini, Carlos Alberto
Año de publicación
2010
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
In the last few years, biodiesel has gain considerable attention due to the increasing concern for the environmental problems associated with the use of fossil fuels. The quality control of this renewable fuel involves numerous analyses, several of them requiring the use of analytical instruments. According to ASTM and EN standards, the analyses of free and total glycerin which are of particular relevance to biodiesel quality must be carried out by GC analysis. This work presents an alternative volumetric method, which does not need expensive equipment, and is therefore particularly useful for quality control in small facilities. Another advantage of the proposed method is that it also overcomes the shortcomings of the GC procedure, such as detection limits and type of raw material used to produce biodiesel. While the GC analysis is restricted to biodiesel obtained from soybean, rapeseed or sunflower oil, the volumetric method has no limitations in this sense.
Fil: Pisarello Milesi, Maria Laura. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Santa Fe. Instituto de Investigaciones en Catálisis y Petroquímica "Ing. José Miguel Parera". Universidad Nacional del Litoral. Instituto de Investigaciones en Catálisis y Petroquímica "Ing. José Miguel Parera"; Argentina
Fil: Dalla Costa, Bruno Oscar. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Santa Fe. Instituto de Investigaciones en Catálisis y Petroquímica "Ing. José Miguel Parera". Universidad Nacional del Litoral. Instituto de Investigaciones en Catálisis y Petroquímica "Ing. José Miguel Parera"; Argentina
Fil: Veizaga, Natalia Soledad. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Santa Fe. Instituto de Investigaciones en Catálisis y Petroquímica "Ing. José Miguel Parera". Universidad Nacional del Litoral. Instituto de Investigaciones en Catálisis y Petroquímica "Ing. José Miguel Parera"; Argentina
Fil: Querini, Carlos Alberto. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Santa Fe. Instituto de Investigaciones en Catálisis y Petroquímica "Ing. José Miguel Parera". Universidad Nacional del Litoral. Instituto de Investigaciones en Catálisis y Petroquímica "Ing. José Miguel Parera"; Argentina
Materia
BIODIESEL ANALYSIS
VOLUMETRIC METHOD
TOTAL GLYCERIN
FREE GLYCERIN
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/278384
Acceder
id CONICETDig_ad47319d6767f6bbed42c567bc732203
oai_identifier_str oai:ri.conicet.gov.ar:11336/278384
network_acronym_str CONICETDig
repository_id_str 3498
network_name_str CONICET Digital (CONICET)
spelling Volumetric Method for Free and Total Glycerin Determination in BiodieselPisarello Milesi, Maria LauraDalla Costa, Bruno OscarVeizaga, Natalia SoledadQuerini, Carlos AlbertoBIODIESEL ANALYSISVOLUMETRIC METHODTOTAL GLYCERINFREE GLYCERINhttps://purl.org/becyt/ford/1.4https://purl.org/becyt/ford/1In the last few years, biodiesel has gain considerable attention due to the increasing concern for the environmental problems associated with the use of fossil fuels. The quality control of this renewable fuel involves numerous analyses, several of them requiring the use of analytical instruments. According to ASTM and EN standards, the analyses of free and total glycerin which are of particular relevance to biodiesel quality must be carried out by GC analysis. This work presents an alternative volumetric method, which does not need expensive equipment, and is therefore particularly useful for quality control in small facilities. Another advantage of the proposed method is that it also overcomes the shortcomings of the GC procedure, such as detection limits and type of raw material used to produce biodiesel. While the GC analysis is restricted to biodiesel obtained from soybean, rapeseed or sunflower oil, the volumetric method has no limitations in this sense.Fil: Pisarello Milesi, Maria Laura. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Santa Fe. Instituto de Investigaciones en Catálisis y Petroquímica "Ing. José Miguel Parera". Universidad Nacional del Litoral. Instituto de Investigaciones en Catálisis y Petroquímica "Ing. José Miguel Parera"; ArgentinaFil: Dalla Costa, Bruno Oscar. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Santa Fe. Instituto de Investigaciones en Catálisis y Petroquímica "Ing. José Miguel Parera". Universidad Nacional del Litoral. Instituto de Investigaciones en Catálisis y Petroquímica "Ing. José Miguel Parera"; ArgentinaFil: Veizaga, Natalia Soledad. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Santa Fe. Instituto de Investigaciones en Catálisis y Petroquímica "Ing. José Miguel Parera". Universidad Nacional del Litoral. Instituto de Investigaciones en Catálisis y Petroquímica "Ing. José Miguel Parera"; ArgentinaFil: Querini, Carlos Alberto. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Santa Fe. Instituto de Investigaciones en Catálisis y Petroquímica "Ing. José Miguel Parera". Universidad Nacional del Litoral. Instituto de Investigaciones en Catálisis y Petroquímica "Ing. José Miguel Parera"; ArgentinaAmerican Chemical Society2010-08info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfapplication/pdfapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/278384Pisarello Milesi, Maria Laura; Dalla Costa, Bruno Oscar; Veizaga, Natalia Soledad; Querini, Carlos Alberto; Volumetric Method for Free and Total Glycerin Determination in Biodiesel; American Chemical Society; Industrial & Engineering Chemical Research; 49; 19; 8-2010; 8935-89410888-5885CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/url/https://pubs.acs.org/doi/10.1021/ie100725finfo:eu-repo/semantics/altIdentifier/doi/10.1021/ie100725finfo:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-sa/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2026-01-08T12:50:49Zoai:ri.conicet.gov.ar:11336/278384instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982026-01-08 12:50:50.104CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Volumetric Method for Free and Total Glycerin Determination in Biodiesel
title Volumetric Method for Free and Total Glycerin Determination in Biodiesel
spellingShingle Volumetric Method for Free and Total Glycerin Determination in Biodiesel
Pisarello Milesi, Maria Laura
BIODIESEL ANALYSIS
VOLUMETRIC METHOD
TOTAL GLYCERIN
FREE GLYCERIN
title_short Volumetric Method for Free and Total Glycerin Determination in Biodiesel
title_full Volumetric Method for Free and Total Glycerin Determination in Biodiesel
title_fullStr Volumetric Method for Free and Total Glycerin Determination in Biodiesel
title_full_unstemmed Volumetric Method for Free and Total Glycerin Determination in Biodiesel
title_sort Volumetric Method for Free and Total Glycerin Determination in Biodiesel
dc.creator.none.fl_str_mv Pisarello Milesi, Maria Laura
Dalla Costa, Bruno Oscar
Veizaga, Natalia Soledad
Querini, Carlos Alberto
author Pisarello Milesi, Maria Laura
author_facet Pisarello Milesi, Maria Laura
Dalla Costa, Bruno Oscar
Veizaga, Natalia Soledad
Querini, Carlos Alberto
author_role author
author2 Dalla Costa, Bruno Oscar
Veizaga, Natalia Soledad
Querini, Carlos Alberto
author2_role author
author
author
dc.subject.none.fl_str_mv BIODIESEL ANALYSIS
VOLUMETRIC METHOD
TOTAL GLYCERIN
FREE GLYCERIN
topic BIODIESEL ANALYSIS
VOLUMETRIC METHOD
TOTAL GLYCERIN
FREE GLYCERIN
purl_subject.fl_str_mv https://purl.org/becyt/ford/1.4
https://purl.org/becyt/ford/1
dc.description.none.fl_txt_mv In the last few years, biodiesel has gain considerable attention due to the increasing concern for the environmental problems associated with the use of fossil fuels. The quality control of this renewable fuel involves numerous analyses, several of them requiring the use of analytical instruments. According to ASTM and EN standards, the analyses of free and total glycerin which are of particular relevance to biodiesel quality must be carried out by GC analysis. This work presents an alternative volumetric method, which does not need expensive equipment, and is therefore particularly useful for quality control in small facilities. Another advantage of the proposed method is that it also overcomes the shortcomings of the GC procedure, such as detection limits and type of raw material used to produce biodiesel. While the GC analysis is restricted to biodiesel obtained from soybean, rapeseed or sunflower oil, the volumetric method has no limitations in this sense.
Fil: Pisarello Milesi, Maria Laura. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Santa Fe. Instituto de Investigaciones en Catálisis y Petroquímica "Ing. José Miguel Parera". Universidad Nacional del Litoral. Instituto de Investigaciones en Catálisis y Petroquímica "Ing. José Miguel Parera"; Argentina
Fil: Dalla Costa, Bruno Oscar. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Santa Fe. Instituto de Investigaciones en Catálisis y Petroquímica "Ing. José Miguel Parera". Universidad Nacional del Litoral. Instituto de Investigaciones en Catálisis y Petroquímica "Ing. José Miguel Parera"; Argentina
Fil: Veizaga, Natalia Soledad. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Santa Fe. Instituto de Investigaciones en Catálisis y Petroquímica "Ing. José Miguel Parera". Universidad Nacional del Litoral. Instituto de Investigaciones en Catálisis y Petroquímica "Ing. José Miguel Parera"; Argentina
Fil: Querini, Carlos Alberto. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Santa Fe. Instituto de Investigaciones en Catálisis y Petroquímica "Ing. José Miguel Parera". Universidad Nacional del Litoral. Instituto de Investigaciones en Catálisis y Petroquímica "Ing. José Miguel Parera"; Argentina
description In the last few years, biodiesel has gain considerable attention due to the increasing concern for the environmental problems associated with the use of fossil fuels. The quality control of this renewable fuel involves numerous analyses, several of them requiring the use of analytical instruments. According to ASTM and EN standards, the analyses of free and total glycerin which are of particular relevance to biodiesel quality must be carried out by GC analysis. This work presents an alternative volumetric method, which does not need expensive equipment, and is therefore particularly useful for quality control in small facilities. Another advantage of the proposed method is that it also overcomes the shortcomings of the GC procedure, such as detection limits and type of raw material used to produce biodiesel. While the GC analysis is restricted to biodiesel obtained from soybean, rapeseed or sunflower oil, the volumetric method has no limitations in this sense.
publishDate 2010
dc.date.none.fl_str_mv 2010-08
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/278384
Pisarello Milesi, Maria Laura; Dalla Costa, Bruno Oscar; Veizaga, Natalia Soledad; Querini, Carlos Alberto; Volumetric Method for Free and Total Glycerin Determination in Biodiesel; American Chemical Society; Industrial & Engineering Chemical Research; 49; 19; 8-2010; 8935-8941
0888-5885
CONICET Digital
CONICET
url http://hdl.handle.net/11336/278384
identifier_str_mv Pisarello Milesi, Maria Laura; Dalla Costa, Bruno Oscar; Veizaga, Natalia Soledad; Querini, Carlos Alberto; Volumetric Method for Free and Total Glycerin Determination in Biodiesel; American Chemical Society; Industrial & Engineering Chemical Research; 49; 19; 8-2010; 8935-8941
0888-5885
CONICET Digital
CONICET
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/url/https://pubs.acs.org/doi/10.1021/ie100725f
info:eu-repo/semantics/altIdentifier/doi/10.1021/ie100725f
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
application/pdf
application/pdf
application/pdf
dc.publisher.none.fl_str_mv American Chemical Society
publisher.none.fl_str_mv American Chemical Society
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
_version_ 1853775182660894720
score 13.25844

Publicaciones similares