Synthesis of silica-based solids by sol-gel technique using lemon bio-waste: Juice, peels and ethanolic extract

Autores
Cordero Castaño, Andres Felipe; Igal, Katerine; Arreche, Romina; Vázquez, Patricia María Elena
Año de publicación
2022
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
After the consumption of the edible part, the citrus fruits are thrown into landfills generating serious pollution and disposal problems. Therefore, the use of citrus fruits for engineering applications has a dual purpose: to generate wealth from waste as an efficient reduction of solid waste. The main objective was to obtain silica-based materials from the precursor (TEOS), replacing acetic acid in acid hydrolysis with different parts of a lemon: peel, juice and peel ethanol extract. The solids obtained were characterized with different techniques such as TEM, SEM, FT-IR, potentiometric titration and XRD. TEM and SEM images were compared with the synthesized pure silica to contrast the morphology of the acidic hydrolysis with lemon. It can be concluded, in general terms, that the proposed objectives have been achieved, since materials were synthesized through a simple and fast method of obtaining, which allowed their inclusion in oxidic matrices. Until now, few attempts have been made to highlight the renewability of reagents used in the synthesis or to incorporate bio-based catalytic processes in larger scales. However, this research contributes to areas of environmentally friendly materials and synthesis, due to the synthesized solids could be used as a support in eco-catalysts.
Fil: Cordero Castaño, Andres Felipe. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Centro de Investigación y Desarrollo en Ciencias Aplicadas "Dr. Jorge J. Ronco". Universidad Nacional de la Plata. Facultad de Ciencias Exactas. Centro de Investigación y Desarrollo en Ciencias Aplicadas; Argentina. YPF - Tecnología; Argentina
Fil: Igal, Katerine. Provincia de Buenos Aires. Gobernación. Comisión de Investigaciones Científicas. Centro de Investigaciones en Tecnología de Pinturas. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Centro de Investigaciones en Tecnología de Pinturas; Argentina
Fil: Arreche, Romina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Centro de Investigación y Desarrollo en Ciencias Aplicadas "Dr. Jorge J. Ronco". Universidad Nacional de la Plata. Facultad de Ciencias Exactas. Centro de Investigación y Desarrollo en Ciencias Aplicadas; Argentina
Fil: Vázquez, Patricia María Elena. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Centro de Investigación y Desarrollo en Ciencias Aplicadas "Dr. Jorge J. Ronco". Universidad Nacional de la Plata. Facultad de Ciencias Exactas. Centro de Investigación y Desarrollo en Ciencias Aplicadas; Argentina
Materia
Bio-waste
Lemon
Sol-gelSilica
Circular economy
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/240985
Acceder
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repository_id_str 3498
network_name_str CONICET Digital (CONICET)
spelling Synthesis of silica-based solids by sol-gel technique using lemon bio-waste: Juice, peels and ethanolic extractCordero Castaño, Andres FelipeIgal, KaterineArreche, RominaVázquez, Patricia María ElenaBio-wasteLemonSol-gelSilicaCircular economyhttps://purl.org/becyt/ford/2.9https://purl.org/becyt/ford/2After the consumption of the edible part, the citrus fruits are thrown into landfills generating serious pollution and disposal problems. Therefore, the use of citrus fruits for engineering applications has a dual purpose: to generate wealth from waste as an efficient reduction of solid waste. The main objective was to obtain silica-based materials from the precursor (TEOS), replacing acetic acid in acid hydrolysis with different parts of a lemon: peel, juice and peel ethanol extract. The solids obtained were characterized with different techniques such as TEM, SEM, FT-IR, potentiometric titration and XRD. TEM and SEM images were compared with the synthesized pure silica to contrast the morphology of the acidic hydrolysis with lemon. It can be concluded, in general terms, that the proposed objectives have been achieved, since materials were synthesized through a simple and fast method of obtaining, which allowed their inclusion in oxidic matrices. Until now, few attempts have been made to highlight the renewability of reagents used in the synthesis or to incorporate bio-based catalytic processes in larger scales. However, this research contributes to areas of environmentally friendly materials and synthesis, due to the synthesized solids could be used as a support in eco-catalysts.Fil: Cordero Castaño, Andres Felipe. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Centro de Investigación y Desarrollo en Ciencias Aplicadas "Dr. Jorge J. Ronco". Universidad Nacional de la Plata. Facultad de Ciencias Exactas. Centro de Investigación y Desarrollo en Ciencias Aplicadas; Argentina. YPF - Tecnología; ArgentinaFil: Igal, Katerine. Provincia de Buenos Aires. Gobernación. Comisión de Investigaciones Científicas. Centro de Investigaciones en Tecnología de Pinturas. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Centro de Investigaciones en Tecnología de Pinturas; ArgentinaFil: Arreche, Romina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Centro de Investigación y Desarrollo en Ciencias Aplicadas "Dr. Jorge J. Ronco". Universidad Nacional de la Plata. Facultad de Ciencias Exactas. Centro de Investigación y Desarrollo en Ciencias Aplicadas; ArgentinaFil: Vázquez, Patricia María Elena. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Centro de Investigación y Desarrollo en Ciencias Aplicadas "Dr. Jorge J. Ronco". Universidad Nacional de la Plata. Facultad de Ciencias Exactas. Centro de Investigación y Desarrollo en Ciencias Aplicadas; ArgentinaElsevier2022-05info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/vnd.openxmlformats-officedocument.wordprocessingml.documentapplication/pdfhttp://hdl.handle.net/11336/240985Cordero Castaño, Andres Felipe; Igal, Katerine; Arreche, Romina; Vázquez, Patricia María Elena; Synthesis of silica-based solids by sol-gel technique using lemon bio-waste: Juice, peels and ethanolic extract; Elsevier; Current Research in Green and Sustainable Chemistry; 5; 100322; 5-2022; 1-112666-0865CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/url/https://www.sciencedirect.com/science/article/pii/S2666086522000649info:eu-repo/semantics/altIdentifier/doi/10.1016/j.crgsc.2022.100322info:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-nd/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-09-03T10:02:18Zoai:ri.conicet.gov.ar:11336/240985instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-09-03 10:02:18.411CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Synthesis of silica-based solids by sol-gel technique using lemon bio-waste: Juice, peels and ethanolic extract
title Synthesis of silica-based solids by sol-gel technique using lemon bio-waste: Juice, peels and ethanolic extract
spellingShingle Synthesis of silica-based solids by sol-gel technique using lemon bio-waste: Juice, peels and ethanolic extract
Cordero Castaño, Andres Felipe
Bio-waste
Lemon
Sol-gelSilica
Circular economy
title_short Synthesis of silica-based solids by sol-gel technique using lemon bio-waste: Juice, peels and ethanolic extract
title_full Synthesis of silica-based solids by sol-gel technique using lemon bio-waste: Juice, peels and ethanolic extract
title_fullStr Synthesis of silica-based solids by sol-gel technique using lemon bio-waste: Juice, peels and ethanolic extract
title_full_unstemmed Synthesis of silica-based solids by sol-gel technique using lemon bio-waste: Juice, peels and ethanolic extract
title_sort Synthesis of silica-based solids by sol-gel technique using lemon bio-waste: Juice, peels and ethanolic extract
dc.creator.none.fl_str_mv Cordero Castaño, Andres Felipe
Igal, Katerine
Arreche, Romina
Vázquez, Patricia María Elena
author Cordero Castaño, Andres Felipe
author_facet Cordero Castaño, Andres Felipe
Igal, Katerine
Arreche, Romina
Vázquez, Patricia María Elena
author_role author
author2 Igal, Katerine
Arreche, Romina
Vázquez, Patricia María Elena
author2_role author
author
author
dc.subject.none.fl_str_mv Bio-waste
Lemon
Sol-gelSilica
Circular economy
topic Bio-waste
Lemon
Sol-gelSilica
Circular economy
purl_subject.fl_str_mv https://purl.org/becyt/ford/2.9
https://purl.org/becyt/ford/2
dc.description.none.fl_txt_mv After the consumption of the edible part, the citrus fruits are thrown into landfills generating serious pollution and disposal problems. Therefore, the use of citrus fruits for engineering applications has a dual purpose: to generate wealth from waste as an efficient reduction of solid waste. The main objective was to obtain silica-based materials from the precursor (TEOS), replacing acetic acid in acid hydrolysis with different parts of a lemon: peel, juice and peel ethanol extract. The solids obtained were characterized with different techniques such as TEM, SEM, FT-IR, potentiometric titration and XRD. TEM and SEM images were compared with the synthesized pure silica to contrast the morphology of the acidic hydrolysis with lemon. It can be concluded, in general terms, that the proposed objectives have been achieved, since materials were synthesized through a simple and fast method of obtaining, which allowed their inclusion in oxidic matrices. Until now, few attempts have been made to highlight the renewability of reagents used in the synthesis or to incorporate bio-based catalytic processes in larger scales. However, this research contributes to areas of environmentally friendly materials and synthesis, due to the synthesized solids could be used as a support in eco-catalysts.
Fil: Cordero Castaño, Andres Felipe. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Centro de Investigación y Desarrollo en Ciencias Aplicadas "Dr. Jorge J. Ronco". Universidad Nacional de la Plata. Facultad de Ciencias Exactas. Centro de Investigación y Desarrollo en Ciencias Aplicadas; Argentina. YPF - Tecnología; Argentina
Fil: Igal, Katerine. Provincia de Buenos Aires. Gobernación. Comisión de Investigaciones Científicas. Centro de Investigaciones en Tecnología de Pinturas. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Centro de Investigaciones en Tecnología de Pinturas; Argentina
Fil: Arreche, Romina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Centro de Investigación y Desarrollo en Ciencias Aplicadas "Dr. Jorge J. Ronco". Universidad Nacional de la Plata. Facultad de Ciencias Exactas. Centro de Investigación y Desarrollo en Ciencias Aplicadas; Argentina
Fil: Vázquez, Patricia María Elena. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Centro de Investigación y Desarrollo en Ciencias Aplicadas "Dr. Jorge J. Ronco". Universidad Nacional de la Plata. Facultad de Ciencias Exactas. Centro de Investigación y Desarrollo en Ciencias Aplicadas; Argentina
description After the consumption of the edible part, the citrus fruits are thrown into landfills generating serious pollution and disposal problems. Therefore, the use of citrus fruits for engineering applications has a dual purpose: to generate wealth from waste as an efficient reduction of solid waste. The main objective was to obtain silica-based materials from the precursor (TEOS), replacing acetic acid in acid hydrolysis with different parts of a lemon: peel, juice and peel ethanol extract. The solids obtained were characterized with different techniques such as TEM, SEM, FT-IR, potentiometric titration and XRD. TEM and SEM images were compared with the synthesized pure silica to contrast the morphology of the acidic hydrolysis with lemon. It can be concluded, in general terms, that the proposed objectives have been achieved, since materials were synthesized through a simple and fast method of obtaining, which allowed their inclusion in oxidic matrices. Until now, few attempts have been made to highlight the renewability of reagents used in the synthesis or to incorporate bio-based catalytic processes in larger scales. However, this research contributes to areas of environmentally friendly materials and synthesis, due to the synthesized solids could be used as a support in eco-catalysts.
publishDate 2022
dc.date.none.fl_str_mv 2022-05
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/240985
Cordero Castaño, Andres Felipe; Igal, Katerine; Arreche, Romina; Vázquez, Patricia María Elena; Synthesis of silica-based solids by sol-gel technique using lemon bio-waste: Juice, peels and ethanolic extract; Elsevier; Current Research in Green and Sustainable Chemistry; 5; 100322; 5-2022; 1-11
2666-0865
CONICET Digital
CONICET
url http://hdl.handle.net/11336/240985
identifier_str_mv Cordero Castaño, Andres Felipe; Igal, Katerine; Arreche, Romina; Vázquez, Patricia María Elena; Synthesis of silica-based solids by sol-gel technique using lemon bio-waste: Juice, peels and ethanolic extract; Elsevier; Current Research in Green and Sustainable Chemistry; 5; 100322; 5-2022; 1-11
2666-0865
CONICET Digital
CONICET
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/url/https://www.sciencedirect.com/science/article/pii/S2666086522000649
info:eu-repo/semantics/altIdentifier/doi/10.1016/j.crgsc.2022.100322
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/vnd.openxmlformats-officedocument.wordprocessingml.document
application/pdf
dc.publisher.none.fl_str_mv Elsevier
publisher.none.fl_str_mv Elsevier
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
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score 13.13397

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