Characterization of surface decorations in Prehispanic archaeological ceramics by Raman spectroscopy, FTIR, XRD and XRF

Autores
Centeno, Silvia A.; Williams, Veronica Isabel; Little, Nicole C.; Speakman, Robert J.
Año de publicación
2012
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
Non-invasive Raman microspectroscopy, FTIR, μXRD and XRF were used to identify the materials present in the black, red, and white surface decorations in selected pottery wares from two Prehispanic archaeological sites in Northwestern (NW) Argentina (AD 900?1530). The iron manganese spinel jacobsite, MnFe2O4, was found to be the main component of two of the fired black decorations analyzed, while hematite and amorphous silicates were found to be present in the red and white fired decorations, respectively. This is the first study, to our knowledge, that firmly identifies jacobsite in black decorations in Prehispanic archaeological ceramics. In fragments recovered from one site, a carbon-based black pigment was identified while gypsum was observed in the recessed areas of decorative surface incisions. Gypsum, potassium nitrate and halite, most likely deposited during burial, were observed on the surface of some of the fragments analyzed. The results are discussed in the context of the technological processes involved and are compared to compositions previously reported for decorations in ceramic objects from NW Argentina.
Fil: Centeno, Silvia A.. The Metropolitan Museum of Art; Estados Unidos
Fil: Williams, Veronica Isabel. Universidad de Buenos Aires. Facultad de Filosofía y Letras. Instituto de Arqueología; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina
Fil: Little, Nicole C.. Museum Conservation Institute; Estados Unidos
Fil: Speakman, Robert J.. Museum Conservation Institute; Estados Unidos
Materia
IRON MANGANESE SPINEL
JACOBSITE
PREHISPANIC CERAMICS
RAMAN SPECTROSCOPY
XRD
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/194487

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spelling Characterization of surface decorations in Prehispanic archaeological ceramics by Raman spectroscopy, FTIR, XRD and XRFCenteno, Silvia A.Williams, Veronica IsabelLittle, Nicole C.Speakman, Robert J.IRON MANGANESE SPINELJACOBSITEPREHISPANIC CERAMICSRAMAN SPECTROSCOPYXRDhttps://purl.org/becyt/ford/1.4https://purl.org/becyt/ford/1Non-invasive Raman microspectroscopy, FTIR, μXRD and XRF were used to identify the materials present in the black, red, and white surface decorations in selected pottery wares from two Prehispanic archaeological sites in Northwestern (NW) Argentina (AD 900?1530). The iron manganese spinel jacobsite, MnFe2O4, was found to be the main component of two of the fired black decorations analyzed, while hematite and amorphous silicates were found to be present in the red and white fired decorations, respectively. This is the first study, to our knowledge, that firmly identifies jacobsite in black decorations in Prehispanic archaeological ceramics. In fragments recovered from one site, a carbon-based black pigment was identified while gypsum was observed in the recessed areas of decorative surface incisions. Gypsum, potassium nitrate and halite, most likely deposited during burial, were observed on the surface of some of the fragments analyzed. The results are discussed in the context of the technological processes involved and are compared to compositions previously reported for decorations in ceramic objects from NW Argentina.Fil: Centeno, Silvia A.. The Metropolitan Museum of Art; Estados UnidosFil: Williams, Veronica Isabel. Universidad de Buenos Aires. Facultad de Filosofía y Letras. Instituto de Arqueología; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas; ArgentinaFil: Little, Nicole C.. Museum Conservation Institute; Estados UnidosFil: Speakman, Robert J.. Museum Conservation Institute; Estados UnidosElsevier Science2012-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/194487Centeno, Silvia A.; Williams, Veronica Isabel; Little, Nicole C.; Speakman, Robert J.; Characterization of surface decorations in Prehispanic archaeological ceramics by Raman spectroscopy, FTIR, XRD and XRF; Elsevier Science; Vibrational Spectroscopy; 58; 1-2012; 119-1240924-2031CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/doi/10.1016/j.vibspec.2011.11.004info:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-sa/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-09-29T09:40:11Zoai:ri.conicet.gov.ar:11336/194487instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-09-29 09:40:12.042CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Characterization of surface decorations in Prehispanic archaeological ceramics by Raman spectroscopy, FTIR, XRD and XRF
title Characterization of surface decorations in Prehispanic archaeological ceramics by Raman spectroscopy, FTIR, XRD and XRF
spellingShingle Characterization of surface decorations in Prehispanic archaeological ceramics by Raman spectroscopy, FTIR, XRD and XRF
Centeno, Silvia A.
IRON MANGANESE SPINEL
JACOBSITE
PREHISPANIC CERAMICS
RAMAN SPECTROSCOPY
XRD
title_short Characterization of surface decorations in Prehispanic archaeological ceramics by Raman spectroscopy, FTIR, XRD and XRF
title_full Characterization of surface decorations in Prehispanic archaeological ceramics by Raman spectroscopy, FTIR, XRD and XRF
title_fullStr Characterization of surface decorations in Prehispanic archaeological ceramics by Raman spectroscopy, FTIR, XRD and XRF
title_full_unstemmed Characterization of surface decorations in Prehispanic archaeological ceramics by Raman spectroscopy, FTIR, XRD and XRF
title_sort Characterization of surface decorations in Prehispanic archaeological ceramics by Raman spectroscopy, FTIR, XRD and XRF
dc.creator.none.fl_str_mv Centeno, Silvia A.
Williams, Veronica Isabel
Little, Nicole C.
Speakman, Robert J.
author Centeno, Silvia A.
author_facet Centeno, Silvia A.
Williams, Veronica Isabel
Little, Nicole C.
Speakman, Robert J.
author_role author
author2 Williams, Veronica Isabel
Little, Nicole C.
Speakman, Robert J.
author2_role author
author
author
dc.subject.none.fl_str_mv IRON MANGANESE SPINEL
JACOBSITE
PREHISPANIC CERAMICS
RAMAN SPECTROSCOPY
XRD
topic IRON MANGANESE SPINEL
JACOBSITE
PREHISPANIC CERAMICS
RAMAN SPECTROSCOPY
XRD
purl_subject.fl_str_mv https://purl.org/becyt/ford/1.4
https://purl.org/becyt/ford/1
dc.description.none.fl_txt_mv Non-invasive Raman microspectroscopy, FTIR, μXRD and XRF were used to identify the materials present in the black, red, and white surface decorations in selected pottery wares from two Prehispanic archaeological sites in Northwestern (NW) Argentina (AD 900?1530). The iron manganese spinel jacobsite, MnFe2O4, was found to be the main component of two of the fired black decorations analyzed, while hematite and amorphous silicates were found to be present in the red and white fired decorations, respectively. This is the first study, to our knowledge, that firmly identifies jacobsite in black decorations in Prehispanic archaeological ceramics. In fragments recovered from one site, a carbon-based black pigment was identified while gypsum was observed in the recessed areas of decorative surface incisions. Gypsum, potassium nitrate and halite, most likely deposited during burial, were observed on the surface of some of the fragments analyzed. The results are discussed in the context of the technological processes involved and are compared to compositions previously reported for decorations in ceramic objects from NW Argentina.
Fil: Centeno, Silvia A.. The Metropolitan Museum of Art; Estados Unidos
Fil: Williams, Veronica Isabel. Universidad de Buenos Aires. Facultad de Filosofía y Letras. Instituto de Arqueología; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina
Fil: Little, Nicole C.. Museum Conservation Institute; Estados Unidos
Fil: Speakman, Robert J.. Museum Conservation Institute; Estados Unidos
description Non-invasive Raman microspectroscopy, FTIR, μXRD and XRF were used to identify the materials present in the black, red, and white surface decorations in selected pottery wares from two Prehispanic archaeological sites in Northwestern (NW) Argentina (AD 900?1530). The iron manganese spinel jacobsite, MnFe2O4, was found to be the main component of two of the fired black decorations analyzed, while hematite and amorphous silicates were found to be present in the red and white fired decorations, respectively. This is the first study, to our knowledge, that firmly identifies jacobsite in black decorations in Prehispanic archaeological ceramics. In fragments recovered from one site, a carbon-based black pigment was identified while gypsum was observed in the recessed areas of decorative surface incisions. Gypsum, potassium nitrate and halite, most likely deposited during burial, were observed on the surface of some of the fragments analyzed. The results are discussed in the context of the technological processes involved and are compared to compositions previously reported for decorations in ceramic objects from NW Argentina.
publishDate 2012
dc.date.none.fl_str_mv 2012-01
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/194487
Centeno, Silvia A.; Williams, Veronica Isabel; Little, Nicole C.; Speakman, Robert J.; Characterization of surface decorations in Prehispanic archaeological ceramics by Raman spectroscopy, FTIR, XRD and XRF; Elsevier Science; Vibrational Spectroscopy; 58; 1-2012; 119-124
0924-2031
CONICET Digital
CONICET
url http://hdl.handle.net/11336/194487
identifier_str_mv Centeno, Silvia A.; Williams, Veronica Isabel; Little, Nicole C.; Speakman, Robert J.; Characterization of surface decorations in Prehispanic archaeological ceramics by Raman spectroscopy, FTIR, XRD and XRF; Elsevier Science; Vibrational Spectroscopy; 58; 1-2012; 119-124
0924-2031
CONICET Digital
CONICET
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/doi/10.1016/j.vibspec.2011.11.004
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
application/pdf
dc.publisher.none.fl_str_mv Elsevier Science
publisher.none.fl_str_mv Elsevier Science
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
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