Composite films based on chitosan and nanomagnetite

Autores
Kloster, Gianina Andrea; Marcovich, Norma Esther; Mosiewicki, Mirna Alejandra
Año de publicación
2015
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
Magnetic chitosan nanocomposite films were prepared by a simple one-step method based on the in situ co-precipitation of nanomagnetite. Both plasticized and no-plasticized films were obtained and characterized by means of X-ray diffraction (XRD), transmission electron microscopy(TEM), scanning electron microscopy (SEM), Fourier Transform infrared spectroscopy (FTIR), thermal gravimetric analysis (TGA) and mechanical (tensile) and dynamic mechanical characterization. Nanomagnetite particles formed inside chitosan films were spherical with diameters ranging from 5 to 13 nm. The film surface and morphology and mechanical behavior were greatly affected by nanoparticles concentration, leading to increasing roughness, stiffness and fragility as the iron oxide content increases. The nanoparticles interact strongly with thechitosan matrix, as was corroborated by TGA, FTIR and DRX. Even though, particles retain their magnetic characteristics and thus, composites containing more than 2 % wt. NMP exhibit magnetic behavior.
Fil: Kloster, Gianina Andrea. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Mar del Plata. Instituto de Investigación En Ciencia y Tecnología de Materiales (i); Argentina. Universidad Nacional de Mar del Plata. Facultad de Ingeniería; Argentina
Fil: Marcovich, Norma Esther. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Mar del Plata. Instituto de Investigación En Ciencia y Tecnología de Materiales (i); Argentina. Universidad Nacional de Mar del Plata. Facultad de Ingeniería; Argentina
Fil: Mosiewicki, Mirna Alejandra. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Mar del Plata. Instituto de Investigación En Ciencia y Tecnología de Materiales (i); Argentina. Universidad Nacional de Mar del Plata. Facultad de Ingeniería; Argentina
Materia
Chitosan
Magnetite
Films
Biocomposites
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/5863

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spelling Composite films based on chitosan and nanomagnetiteKloster, Gianina AndreaMarcovich, Norma EstherMosiewicki, Mirna AlejandraChitosanMagnetiteFilmsBiocompositeshttps://purl.org/becyt/ford/2.5https://purl.org/becyt/ford/2https://purl.org/becyt/ford/2.5https://purl.org/becyt/ford/2Magnetic chitosan nanocomposite films were prepared by a simple one-step method based on the in situ co-precipitation of nanomagnetite. Both plasticized and no-plasticized films were obtained and characterized by means of X-ray diffraction (XRD), transmission electron microscopy(TEM), scanning electron microscopy (SEM), Fourier Transform infrared spectroscopy (FTIR), thermal gravimetric analysis (TGA) and mechanical (tensile) and dynamic mechanical characterization. Nanomagnetite particles formed inside chitosan films were spherical with diameters ranging from 5 to 13 nm. The film surface and morphology and mechanical behavior were greatly affected by nanoparticles concentration, leading to increasing roughness, stiffness and fragility as the iron oxide content increases. The nanoparticles interact strongly with thechitosan matrix, as was corroborated by TGA, FTIR and DRX. Even though, particles retain their magnetic characteristics and thus, composites containing more than 2 % wt. NMP exhibit magnetic behavior.Fil: Kloster, Gianina Andrea. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Mar del Plata. Instituto de Investigación En Ciencia y Tecnología de Materiales (i); Argentina. Universidad Nacional de Mar del Plata. Facultad de Ingeniería; ArgentinaFil: Marcovich, Norma Esther. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Mar del Plata. Instituto de Investigación En Ciencia y Tecnología de Materiales (i); Argentina. Universidad Nacional de Mar del Plata. Facultad de Ingeniería; ArgentinaFil: Mosiewicki, Mirna Alejandra. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Mar del Plata. Instituto de Investigación En Ciencia y Tecnología de Materiales (i); Argentina. Universidad Nacional de Mar del Plata. Facultad de Ingeniería; ArgentinaElsevier2015-03-05info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfapplication/pdfapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/5863Kloster, Gianina Andrea; Marcovich, Norma Esther; Mosiewicki, Mirna Alejandra; Composite films based on chitosan and nanomagnetite; Elsevier; European Polymer Journal; 66; 5-3-2015; 386-3960014-3057enginfo:eu-repo/semantics/altIdentifier/url/http://www.sciencedirect.com/science/article/pii/S0014305715001172info:eu-repo/semantics/altIdentifier/doi/10.1016/j.eurpolymj.2015.02.042info:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-nd/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-09-03T09:57:11Zoai:ri.conicet.gov.ar:11336/5863instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-09-03 09:57:11.995CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Composite films based on chitosan and nanomagnetite
title Composite films based on chitosan and nanomagnetite
spellingShingle Composite films based on chitosan and nanomagnetite
Kloster, Gianina Andrea
Chitosan
Magnetite
Films
Biocomposites
title_short Composite films based on chitosan and nanomagnetite
title_full Composite films based on chitosan and nanomagnetite
title_fullStr Composite films based on chitosan and nanomagnetite
title_full_unstemmed Composite films based on chitosan and nanomagnetite
title_sort Composite films based on chitosan and nanomagnetite
dc.creator.none.fl_str_mv Kloster, Gianina Andrea
Marcovich, Norma Esther
Mosiewicki, Mirna Alejandra
author Kloster, Gianina Andrea
author_facet Kloster, Gianina Andrea
Marcovich, Norma Esther
Mosiewicki, Mirna Alejandra
author_role author
author2 Marcovich, Norma Esther
Mosiewicki, Mirna Alejandra
author2_role author
author
dc.subject.none.fl_str_mv Chitosan
Magnetite
Films
Biocomposites
topic Chitosan
Magnetite
Films
Biocomposites
purl_subject.fl_str_mv https://purl.org/becyt/ford/2.5
https://purl.org/becyt/ford/2
https://purl.org/becyt/ford/2.5
https://purl.org/becyt/ford/2
dc.description.none.fl_txt_mv Magnetic chitosan nanocomposite films were prepared by a simple one-step method based on the in situ co-precipitation of nanomagnetite. Both plasticized and no-plasticized films were obtained and characterized by means of X-ray diffraction (XRD), transmission electron microscopy(TEM), scanning electron microscopy (SEM), Fourier Transform infrared spectroscopy (FTIR), thermal gravimetric analysis (TGA) and mechanical (tensile) and dynamic mechanical characterization. Nanomagnetite particles formed inside chitosan films were spherical with diameters ranging from 5 to 13 nm. The film surface and morphology and mechanical behavior were greatly affected by nanoparticles concentration, leading to increasing roughness, stiffness and fragility as the iron oxide content increases. The nanoparticles interact strongly with thechitosan matrix, as was corroborated by TGA, FTIR and DRX. Even though, particles retain their magnetic characteristics and thus, composites containing more than 2 % wt. NMP exhibit magnetic behavior.
Fil: Kloster, Gianina Andrea. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Mar del Plata. Instituto de Investigación En Ciencia y Tecnología de Materiales (i); Argentina. Universidad Nacional de Mar del Plata. Facultad de Ingeniería; Argentina
Fil: Marcovich, Norma Esther. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Mar del Plata. Instituto de Investigación En Ciencia y Tecnología de Materiales (i); Argentina. Universidad Nacional de Mar del Plata. Facultad de Ingeniería; Argentina
Fil: Mosiewicki, Mirna Alejandra. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Mar del Plata. Instituto de Investigación En Ciencia y Tecnología de Materiales (i); Argentina. Universidad Nacional de Mar del Plata. Facultad de Ingeniería; Argentina
description Magnetic chitosan nanocomposite films were prepared by a simple one-step method based on the in situ co-precipitation of nanomagnetite. Both plasticized and no-plasticized films were obtained and characterized by means of X-ray diffraction (XRD), transmission electron microscopy(TEM), scanning electron microscopy (SEM), Fourier Transform infrared spectroscopy (FTIR), thermal gravimetric analysis (TGA) and mechanical (tensile) and dynamic mechanical characterization. Nanomagnetite particles formed inside chitosan films were spherical with diameters ranging from 5 to 13 nm. The film surface and morphology and mechanical behavior were greatly affected by nanoparticles concentration, leading to increasing roughness, stiffness and fragility as the iron oxide content increases. The nanoparticles interact strongly with thechitosan matrix, as was corroborated by TGA, FTIR and DRX. Even though, particles retain their magnetic characteristics and thus, composites containing more than 2 % wt. NMP exhibit magnetic behavior.
publishDate 2015
dc.date.none.fl_str_mv 2015-03-05
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/5863
Kloster, Gianina Andrea; Marcovich, Norma Esther; Mosiewicki, Mirna Alejandra; Composite films based on chitosan and nanomagnetite; Elsevier; European Polymer Journal; 66; 5-3-2015; 386-396
0014-3057
url http://hdl.handle.net/11336/5863
identifier_str_mv Kloster, Gianina Andrea; Marcovich, Norma Esther; Mosiewicki, Mirna Alejandra; Composite films based on chitosan and nanomagnetite; Elsevier; European Polymer Journal; 66; 5-3-2015; 386-396
0014-3057
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/url/http://www.sciencedirect.com/science/article/pii/S0014305715001172
info:eu-repo/semantics/altIdentifier/doi/10.1016/j.eurpolymj.2015.02.042
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
application/pdf
application/pdf
application/pdf
dc.publisher.none.fl_str_mv Elsevier
publisher.none.fl_str_mv Elsevier
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
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