A Validated Flowsheeting Tool for the Study of an Industrial Granulation Process

Autores
Cotabarren, Ivana María; Bertin, Diego Esteban; Bucala, Veronica; Piña, Juliana
Año de publicación
2013
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
This work evaluates the capabilities of a complete dynamic simulator developed for a urea granulation circuit (based on fluidized-bed technology) to analyze the process sensitivity against different disturbances and to study common operating problems. First, the circuit model is validated by comparing simulation results with plant data from a high capacity industry. Based on a sensitivity analysis of the process variables, diverse strategies are explored aiming to solve typical operational challenges (i.e., too high granulation temperatures, undesired dust formation, low fluidized-bed heights, etc.) by considering different control variables or alternative flowsheets configurations. It is demonstrated that an appropriate fluidization air distribution between the different granulator chambers allows to control, within certain limits, the often too high fluidized-bed temperatures. Furthermore, it is shown that by adjusting the total granulator pressure drop, the fluidized-bed levels can be kept within the desired ranges. Finally, the developed flowsheeting tool suggest that the partial bypass of the fines generated in the crusher can be an efficient strategy for improving product on specification, while the circuit variables remain within the desired operating range.
Fil: Cotabarren, Ivana María. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Bahía Blanca. Planta Piloto de Ingeniería Química (i); Argentina. Universidad Nacional del Sur. Departamento de Ingenieria Quimica; Argentina
Fil: Bertin, Diego Esteban. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Bahía Blanca. Planta Piloto de Ingeniería Química (i); Argentina. Universidad Nacional del Sur. Departamento de Ingenieria Quimica; Argentina
Fil: Bucala, Veronica. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Bahía Blanca. Planta Piloto de Ingeniería Química (i); Argentina. Universidad Nacional del Sur. Departamento de Ingenieria Quimica; Argentina
Fil: Piña, Juliana. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Bahía Blanca. Planta Piloto de Ingeniería Química (i); Argentina. Universidad Nacional del Sur. Departamento de Ingenieria Quimica; Argentina
Materia
Flowsheet Simulation
Granulation
Solids Processes
Urea
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/11923
Acceder
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repository_id_str 3498
network_name_str CONICET Digital (CONICET)
spelling A Validated Flowsheeting Tool for the Study of an Industrial Granulation ProcessCotabarren, Ivana MaríaBertin, Diego EstebanBucala, VeronicaPiña, JulianaFlowsheet SimulationGranulationSolids ProcessesUreahttps://purl.org/becyt/ford/2.4https://purl.org/becyt/ford/2This work evaluates the capabilities of a complete dynamic simulator developed for a urea granulation circuit (based on fluidized-bed technology) to analyze the process sensitivity against different disturbances and to study common operating problems. First, the circuit model is validated by comparing simulation results with plant data from a high capacity industry. Based on a sensitivity analysis of the process variables, diverse strategies are explored aiming to solve typical operational challenges (i.e., too high granulation temperatures, undesired dust formation, low fluidized-bed heights, etc.) by considering different control variables or alternative flowsheets configurations. It is demonstrated that an appropriate fluidization air distribution between the different granulator chambers allows to control, within certain limits, the often too high fluidized-bed temperatures. Furthermore, it is shown that by adjusting the total granulator pressure drop, the fluidized-bed levels can be kept within the desired ranges. Finally, the developed flowsheeting tool suggest that the partial bypass of the fines generated in the crusher can be an efficient strategy for improving product on specification, while the circuit variables remain within the desired operating range.Fil: Cotabarren, Ivana María. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Bahía Blanca. Planta Piloto de Ingeniería Química (i); Argentina. Universidad Nacional del Sur. Departamento de Ingenieria Quimica; ArgentinaFil: Bertin, Diego Esteban. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Bahía Blanca. Planta Piloto de Ingeniería Química (i); Argentina. Universidad Nacional del Sur. Departamento de Ingenieria Quimica; ArgentinaFil: Bucala, Veronica. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Bahía Blanca. Planta Piloto de Ingeniería Química (i); Argentina. Universidad Nacional del Sur. Departamento de Ingenieria Quimica; ArgentinaFil: Piña, Juliana. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Bahía Blanca. Planta Piloto de Ingeniería Química (i); Argentina. Universidad Nacional del Sur. Departamento de Ingenieria Quimica; ArgentinaAmerican Chemical Society2013-09info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfapplication/pdfapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/11923Cotabarren, Ivana María; Bertin, Diego Esteban; Bucala, Veronica; Piña, Juliana; A Validated Flowsheeting Tool for the Study of an Industrial Granulation Process; American Chemical Society; Industrial & Engineering Chemical Research; 52; 43; 9-2013; 15198-152100888-5885enginfo:eu-repo/semantics/altIdentifier/url/http://pubs.acs.org/doi/abs/10.1021/ie401650rinfo:eu-repo/semantics/altIdentifier/url/http://dx.doi.org/10.1021/ie401650rinfo:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-sa/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-10-22T11:22:30Zoai:ri.conicet.gov.ar:11336/11923instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-10-22 11:22:31.289CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv A Validated Flowsheeting Tool for the Study of an Industrial Granulation Process
title A Validated Flowsheeting Tool for the Study of an Industrial Granulation Process
spellingShingle A Validated Flowsheeting Tool for the Study of an Industrial Granulation Process
Cotabarren, Ivana María
Flowsheet Simulation
Granulation
Solids Processes
Urea
title_short A Validated Flowsheeting Tool for the Study of an Industrial Granulation Process
title_full A Validated Flowsheeting Tool for the Study of an Industrial Granulation Process
title_fullStr A Validated Flowsheeting Tool for the Study of an Industrial Granulation Process
title_full_unstemmed A Validated Flowsheeting Tool for the Study of an Industrial Granulation Process
title_sort A Validated Flowsheeting Tool for the Study of an Industrial Granulation Process
dc.creator.none.fl_str_mv Cotabarren, Ivana María
Bertin, Diego Esteban
Bucala, Veronica
Piña, Juliana
author Cotabarren, Ivana María
author_facet Cotabarren, Ivana María
Bertin, Diego Esteban
Bucala, Veronica
Piña, Juliana
author_role author
author2 Bertin, Diego Esteban
Bucala, Veronica
Piña, Juliana
author2_role author
author
author
dc.subject.none.fl_str_mv Flowsheet Simulation
Granulation
Solids Processes
Urea
topic Flowsheet Simulation
Granulation
Solids Processes
Urea
purl_subject.fl_str_mv https://purl.org/becyt/ford/2.4
https://purl.org/becyt/ford/2
dc.description.none.fl_txt_mv This work evaluates the capabilities of a complete dynamic simulator developed for a urea granulation circuit (based on fluidized-bed technology) to analyze the process sensitivity against different disturbances and to study common operating problems. First, the circuit model is validated by comparing simulation results with plant data from a high capacity industry. Based on a sensitivity analysis of the process variables, diverse strategies are explored aiming to solve typical operational challenges (i.e., too high granulation temperatures, undesired dust formation, low fluidized-bed heights, etc.) by considering different control variables or alternative flowsheets configurations. It is demonstrated that an appropriate fluidization air distribution between the different granulator chambers allows to control, within certain limits, the often too high fluidized-bed temperatures. Furthermore, it is shown that by adjusting the total granulator pressure drop, the fluidized-bed levels can be kept within the desired ranges. Finally, the developed flowsheeting tool suggest that the partial bypass of the fines generated in the crusher can be an efficient strategy for improving product on specification, while the circuit variables remain within the desired operating range.
Fil: Cotabarren, Ivana María. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Bahía Blanca. Planta Piloto de Ingeniería Química (i); Argentina. Universidad Nacional del Sur. Departamento de Ingenieria Quimica; Argentina
Fil: Bertin, Diego Esteban. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Bahía Blanca. Planta Piloto de Ingeniería Química (i); Argentina. Universidad Nacional del Sur. Departamento de Ingenieria Quimica; Argentina
Fil: Bucala, Veronica. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Bahía Blanca. Planta Piloto de Ingeniería Química (i); Argentina. Universidad Nacional del Sur. Departamento de Ingenieria Quimica; Argentina
Fil: Piña, Juliana. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Bahía Blanca. Planta Piloto de Ingeniería Química (i); Argentina. Universidad Nacional del Sur. Departamento de Ingenieria Quimica; Argentina
description This work evaluates the capabilities of a complete dynamic simulator developed for a urea granulation circuit (based on fluidized-bed technology) to analyze the process sensitivity against different disturbances and to study common operating problems. First, the circuit model is validated by comparing simulation results with plant data from a high capacity industry. Based on a sensitivity analysis of the process variables, diverse strategies are explored aiming to solve typical operational challenges (i.e., too high granulation temperatures, undesired dust formation, low fluidized-bed heights, etc.) by considering different control variables or alternative flowsheets configurations. It is demonstrated that an appropriate fluidization air distribution between the different granulator chambers allows to control, within certain limits, the often too high fluidized-bed temperatures. Furthermore, it is shown that by adjusting the total granulator pressure drop, the fluidized-bed levels can be kept within the desired ranges. Finally, the developed flowsheeting tool suggest that the partial bypass of the fines generated in the crusher can be an efficient strategy for improving product on specification, while the circuit variables remain within the desired operating range.
publishDate 2013
dc.date.none.fl_str_mv 2013-09
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/11923
Cotabarren, Ivana María; Bertin, Diego Esteban; Bucala, Veronica; Piña, Juliana; A Validated Flowsheeting Tool for the Study of an Industrial Granulation Process; American Chemical Society; Industrial & Engineering Chemical Research; 52; 43; 9-2013; 15198-15210
0888-5885
url http://hdl.handle.net/11336/11923
identifier_str_mv Cotabarren, Ivana María; Bertin, Diego Esteban; Bucala, Veronica; Piña, Juliana; A Validated Flowsheeting Tool for the Study of an Industrial Granulation Process; American Chemical Society; Industrial & Engineering Chemical Research; 52; 43; 9-2013; 15198-15210
0888-5885
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/url/http://pubs.acs.org/doi/abs/10.1021/ie401650r
info:eu-repo/semantics/altIdentifier/url/http://dx.doi.org/10.1021/ie401650r
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
application/pdf
application/pdf
application/pdf
dc.publisher.none.fl_str_mv American Chemical Society
publisher.none.fl_str_mv American Chemical Society
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
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score 12.982451

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