Assessment of a Modified Hydrocyclone with Ultrasonic Assistance for Nickel Powder Electrochemical Production

Autores
González Pérez, Omar; Bisang, Jose Maria
Año de publicación
2022
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
An electrochemical reactor based on a modified hydrocyclone with ultrasonic assistance is examined with the purpose of analyzing the continuous production of nickel powder from dilute solutions simulating industrial wastewaters containing nickel. Under operating conditions, nickel deposition takes place under mass-transfer control and the helical flow inside the reactor generates a high mass-transfer coefficient, thus improving the removal of metal ions. The application of ultrasound is crucial for the detachment of the electrodeposited nickel, which allows its recovery as a metal powder. The best result was achieved at a current density of 5368 A m?2 and 60 °C yielding a nickel powder fraction obtained from the spigot of the device higher than 90%. The gravimetric current efficiency and the specific energy consumption were 33.4% and 23.8 kW h kg?1, respectively, for anexperiment lasting 13 min. The nickel particles are of high purity and dendritic nature with an average size of 22.9 μm.
Fil: González Pérez, Omar. Universidad Nacional del Litoral. Facultad de Ingeniería Química. Programa de Electroquímica Aplicada e Ingeniería Electroquímica; Argentina
Fil: Bisang, Jose Maria. Universidad Nacional del Litoral. Facultad de Ingeniería Química. Programa de Electroquímica Aplicada e Ingeniería Electroquímica; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Santa Fe; Argentina
Materia
NICKEL POWDER
ELECTROCHEMICAL REACTOR
HYDROCYCLONE
ULTRASOUND
EFFLUENT TREATMENT
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/221361

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network_name_str CONICET Digital (CONICET)
spelling Assessment of a Modified Hydrocyclone with Ultrasonic Assistance for Nickel Powder Electrochemical ProductionGonzález Pérez, OmarBisang, Jose MariaNICKEL POWDERELECTROCHEMICAL REACTORHYDROCYCLONEULTRASOUNDEFFLUENT TREATMENThttps://purl.org/becyt/ford/2.4https://purl.org/becyt/ford/2An electrochemical reactor based on a modified hydrocyclone with ultrasonic assistance is examined with the purpose of analyzing the continuous production of nickel powder from dilute solutions simulating industrial wastewaters containing nickel. Under operating conditions, nickel deposition takes place under mass-transfer control and the helical flow inside the reactor generates a high mass-transfer coefficient, thus improving the removal of metal ions. The application of ultrasound is crucial for the detachment of the electrodeposited nickel, which allows its recovery as a metal powder. The best result was achieved at a current density of 5368 A m?2 and 60 °C yielding a nickel powder fraction obtained from the spigot of the device higher than 90%. The gravimetric current efficiency and the specific energy consumption were 33.4% and 23.8 kW h kg?1, respectively, for anexperiment lasting 13 min. The nickel particles are of high purity and dendritic nature with an average size of 22.9 μm.Fil: González Pérez, Omar. Universidad Nacional del Litoral. Facultad de Ingeniería Química. Programa de Electroquímica Aplicada e Ingeniería Electroquímica; ArgentinaFil: Bisang, Jose Maria. Universidad Nacional del Litoral. Facultad de Ingeniería Química. Programa de Electroquímica Aplicada e Ingeniería Electroquímica; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Santa Fe; ArgentinaIOP Publishing2022-09info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/221361González Pérez, Omar; Bisang, Jose Maria; Assessment of a Modified Hydrocyclone with Ultrasonic Assistance for Nickel Powder Electrochemical Production; IOP Publishing; ECS Advances; 1; 3; 9-2022; 1-102754-2734CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/url/https://iopscience.iop.org/article/10.1149/2754-2734/ac914einfo:eu-repo/semantics/altIdentifier/doi/10.1149/2754-2734/ac914einfo:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-sa/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-10-15T14:58:25Zoai:ri.conicet.gov.ar:11336/221361instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-10-15 14:58:25.923CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Assessment of a Modified Hydrocyclone with Ultrasonic Assistance for Nickel Powder Electrochemical Production
title Assessment of a Modified Hydrocyclone with Ultrasonic Assistance for Nickel Powder Electrochemical Production
spellingShingle Assessment of a Modified Hydrocyclone with Ultrasonic Assistance for Nickel Powder Electrochemical Production
González Pérez, Omar
NICKEL POWDER
ELECTROCHEMICAL REACTOR
HYDROCYCLONE
ULTRASOUND
EFFLUENT TREATMENT
title_short Assessment of a Modified Hydrocyclone with Ultrasonic Assistance for Nickel Powder Electrochemical Production
title_full Assessment of a Modified Hydrocyclone with Ultrasonic Assistance for Nickel Powder Electrochemical Production
title_fullStr Assessment of a Modified Hydrocyclone with Ultrasonic Assistance for Nickel Powder Electrochemical Production
title_full_unstemmed Assessment of a Modified Hydrocyclone with Ultrasonic Assistance for Nickel Powder Electrochemical Production
title_sort Assessment of a Modified Hydrocyclone with Ultrasonic Assistance for Nickel Powder Electrochemical Production
dc.creator.none.fl_str_mv González Pérez, Omar
Bisang, Jose Maria
author González Pérez, Omar
author_facet González Pérez, Omar
Bisang, Jose Maria
author_role author
author2 Bisang, Jose Maria
author2_role author
dc.subject.none.fl_str_mv NICKEL POWDER
ELECTROCHEMICAL REACTOR
HYDROCYCLONE
ULTRASOUND
EFFLUENT TREATMENT
topic NICKEL POWDER
ELECTROCHEMICAL REACTOR
HYDROCYCLONE
ULTRASOUND
EFFLUENT TREATMENT
purl_subject.fl_str_mv https://purl.org/becyt/ford/2.4
https://purl.org/becyt/ford/2
dc.description.none.fl_txt_mv An electrochemical reactor based on a modified hydrocyclone with ultrasonic assistance is examined with the purpose of analyzing the continuous production of nickel powder from dilute solutions simulating industrial wastewaters containing nickel. Under operating conditions, nickel deposition takes place under mass-transfer control and the helical flow inside the reactor generates a high mass-transfer coefficient, thus improving the removal of metal ions. The application of ultrasound is crucial for the detachment of the electrodeposited nickel, which allows its recovery as a metal powder. The best result was achieved at a current density of 5368 A m?2 and 60 °C yielding a nickel powder fraction obtained from the spigot of the device higher than 90%. The gravimetric current efficiency and the specific energy consumption were 33.4% and 23.8 kW h kg?1, respectively, for anexperiment lasting 13 min. The nickel particles are of high purity and dendritic nature with an average size of 22.9 μm.
Fil: González Pérez, Omar. Universidad Nacional del Litoral. Facultad de Ingeniería Química. Programa de Electroquímica Aplicada e Ingeniería Electroquímica; Argentina
Fil: Bisang, Jose Maria. Universidad Nacional del Litoral. Facultad de Ingeniería Química. Programa de Electroquímica Aplicada e Ingeniería Electroquímica; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Santa Fe; Argentina
description An electrochemical reactor based on a modified hydrocyclone with ultrasonic assistance is examined with the purpose of analyzing the continuous production of nickel powder from dilute solutions simulating industrial wastewaters containing nickel. Under operating conditions, nickel deposition takes place under mass-transfer control and the helical flow inside the reactor generates a high mass-transfer coefficient, thus improving the removal of metal ions. The application of ultrasound is crucial for the detachment of the electrodeposited nickel, which allows its recovery as a metal powder. The best result was achieved at a current density of 5368 A m?2 and 60 °C yielding a nickel powder fraction obtained from the spigot of the device higher than 90%. The gravimetric current efficiency and the specific energy consumption were 33.4% and 23.8 kW h kg?1, respectively, for anexperiment lasting 13 min. The nickel particles are of high purity and dendritic nature with an average size of 22.9 μm.
publishDate 2022
dc.date.none.fl_str_mv 2022-09
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/221361
González Pérez, Omar; Bisang, Jose Maria; Assessment of a Modified Hydrocyclone with Ultrasonic Assistance for Nickel Powder Electrochemical Production; IOP Publishing; ECS Advances; 1; 3; 9-2022; 1-10
2754-2734
CONICET Digital
CONICET
url http://hdl.handle.net/11336/221361
identifier_str_mv González Pérez, Omar; Bisang, Jose Maria; Assessment of a Modified Hydrocyclone with Ultrasonic Assistance for Nickel Powder Electrochemical Production; IOP Publishing; ECS Advances; 1; 3; 9-2022; 1-10
2754-2734
CONICET Digital
CONICET
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/url/https://iopscience.iop.org/article/10.1149/2754-2734/ac914e
info:eu-repo/semantics/altIdentifier/doi/10.1149/2754-2734/ac914e
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
application/pdf
dc.publisher.none.fl_str_mv IOP Publishing
publisher.none.fl_str_mv IOP Publishing
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
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