“In-situ” antimony film electrode for the determination of tetracyclines in Argentinean honey samples

Autores
Krepper, Gabriela; Pierini, Gastón Dario; Pistonesi, Marcelo Fabian; Di Nezio, Maria Susana
Año de publicación
2017
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
The main goal of this work is the application of an antimony film electrode (SbFE) prepared for the first time “in-situ” to determine organic compound as tetracyclines commonly used in Argentine for hive treatment. The SbFE was prepared on a glassy carbon electrode (GCE) and square wave cathodic stripping voltammetry (SWCSV) technique was used. The SWCSV parameters were optimized based on a Draper Lin small composite design. The SWCSV response was linear in the TCs concentration range from 0.40 to 3.00 μM with a limit of detection (LOD) of 0.15 μM. The proposed method is a good and simple alternative to the determination of tetracyclines in Argentinean honeys samples. Recovery experiments were performed using spiked honey samples with standard deviation values from 0.75% and 9.69%.
Fil: Krepper, Gabriela. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Bahía Blanca. Instituto de Química del Sur. Universidad Nacional del Sur. Departamento de Química. Instituto de Química del Sur; Argentina
Fil: Pierini, Gastón Dario. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Bahía Blanca. Instituto de Química del Sur. Universidad Nacional del Sur. Departamento de Química. Instituto de Química del Sur; Argentina
Fil: Pistonesi, Marcelo Fabian. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Bahía Blanca. Instituto de Química del Sur. Universidad Nacional del Sur. Departamento de Química. Instituto de Química del Sur; Argentina
Fil: Di Nezio, Maria Susana. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Bahía Blanca. Instituto de Química del Sur. Universidad Nacional del Sur. Departamento de Química. Instituto de Química del Sur; Argentina
Materia
Honey
Square Wave Cathodic Stripping Voltammetry
Tetracyclines
"In Situ" Antimony Film Electrode
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/55290
Acceder
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network_name_str CONICET Digital (CONICET)
spelling “In-situ” antimony film electrode for the determination of tetracyclines in Argentinean honey samplesKrepper, GabrielaPierini, Gastón DarioPistonesi, Marcelo FabianDi Nezio, Maria SusanaHoneySquare Wave Cathodic Stripping VoltammetryTetracyclines"In Situ" Antimony Film Electrodehttps://purl.org/becyt/ford/1.4https://purl.org/becyt/ford/1The main goal of this work is the application of an antimony film electrode (SbFE) prepared for the first time “in-situ” to determine organic compound as tetracyclines commonly used in Argentine for hive treatment. The SbFE was prepared on a glassy carbon electrode (GCE) and square wave cathodic stripping voltammetry (SWCSV) technique was used. The SWCSV parameters were optimized based on a Draper Lin small composite design. The SWCSV response was linear in the TCs concentration range from 0.40 to 3.00 μM with a limit of detection (LOD) of 0.15 μM. The proposed method is a good and simple alternative to the determination of tetracyclines in Argentinean honeys samples. Recovery experiments were performed using spiked honey samples with standard deviation values from 0.75% and 9.69%.Fil: Krepper, Gabriela. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Bahía Blanca. Instituto de Química del Sur. Universidad Nacional del Sur. Departamento de Química. Instituto de Química del Sur; ArgentinaFil: Pierini, Gastón Dario. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Bahía Blanca. Instituto de Química del Sur. Universidad Nacional del Sur. Departamento de Química. Instituto de Química del Sur; ArgentinaFil: Pistonesi, Marcelo Fabian. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Bahía Blanca. Instituto de Química del Sur. Universidad Nacional del Sur. Departamento de Química. Instituto de Química del Sur; ArgentinaFil: Di Nezio, Maria Susana. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Bahía Blanca. Instituto de Química del Sur. Universidad Nacional del Sur. Departamento de Química. Instituto de Química del Sur; ArgentinaElsevier Science Sa2017-03-31info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/55290Krepper, Gabriela; Pierini, Gastón Dario; Pistonesi, Marcelo Fabian; Di Nezio, Maria Susana; “In-situ” antimony film electrode for the determination of tetracyclines in Argentinean honey samples; Elsevier Science Sa; Sensors and Actuators B: Chemical; 241; 31-3-2017; 560-5660925-4005CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/url/https://www.sciencedirect.com/science/article/pii/S0925400516317579info:eu-repo/semantics/altIdentifier/doi/10.1016/j.snb.2016.10.125info:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-sa/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-09-29T09:54:37Zoai:ri.conicet.gov.ar:11336/55290instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-09-29 09:54:37.504CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv “In-situ” antimony film electrode for the determination of tetracyclines in Argentinean honey samples
title “In-situ” antimony film electrode for the determination of tetracyclines in Argentinean honey samples
spellingShingle “In-situ” antimony film electrode for the determination of tetracyclines in Argentinean honey samples
Krepper, Gabriela
Honey
Square Wave Cathodic Stripping Voltammetry
Tetracyclines
"In Situ" Antimony Film Electrode
title_short “In-situ” antimony film electrode for the determination of tetracyclines in Argentinean honey samples
title_full “In-situ” antimony film electrode for the determination of tetracyclines in Argentinean honey samples
title_fullStr “In-situ” antimony film electrode for the determination of tetracyclines in Argentinean honey samples
title_full_unstemmed “In-situ” antimony film electrode for the determination of tetracyclines in Argentinean honey samples
title_sort “In-situ” antimony film electrode for the determination of tetracyclines in Argentinean honey samples
dc.creator.none.fl_str_mv Krepper, Gabriela
Pierini, Gastón Dario
Pistonesi, Marcelo Fabian
Di Nezio, Maria Susana
author Krepper, Gabriela
author_facet Krepper, Gabriela
Pierini, Gastón Dario
Pistonesi, Marcelo Fabian
Di Nezio, Maria Susana
author_role author
author2 Pierini, Gastón Dario
Pistonesi, Marcelo Fabian
Di Nezio, Maria Susana
author2_role author
author
author
dc.subject.none.fl_str_mv Honey
Square Wave Cathodic Stripping Voltammetry
Tetracyclines
"In Situ" Antimony Film Electrode
topic Honey
Square Wave Cathodic Stripping Voltammetry
Tetracyclines
"In Situ" Antimony Film Electrode
purl_subject.fl_str_mv https://purl.org/becyt/ford/1.4
https://purl.org/becyt/ford/1
dc.description.none.fl_txt_mv The main goal of this work is the application of an antimony film electrode (SbFE) prepared for the first time “in-situ” to determine organic compound as tetracyclines commonly used in Argentine for hive treatment. The SbFE was prepared on a glassy carbon electrode (GCE) and square wave cathodic stripping voltammetry (SWCSV) technique was used. The SWCSV parameters were optimized based on a Draper Lin small composite design. The SWCSV response was linear in the TCs concentration range from 0.40 to 3.00 μM with a limit of detection (LOD) of 0.15 μM. The proposed method is a good and simple alternative to the determination of tetracyclines in Argentinean honeys samples. Recovery experiments were performed using spiked honey samples with standard deviation values from 0.75% and 9.69%.
Fil: Krepper, Gabriela. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Bahía Blanca. Instituto de Química del Sur. Universidad Nacional del Sur. Departamento de Química. Instituto de Química del Sur; Argentina
Fil: Pierini, Gastón Dario. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Bahía Blanca. Instituto de Química del Sur. Universidad Nacional del Sur. Departamento de Química. Instituto de Química del Sur; Argentina
Fil: Pistonesi, Marcelo Fabian. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Bahía Blanca. Instituto de Química del Sur. Universidad Nacional del Sur. Departamento de Química. Instituto de Química del Sur; Argentina
Fil: Di Nezio, Maria Susana. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Bahía Blanca. Instituto de Química del Sur. Universidad Nacional del Sur. Departamento de Química. Instituto de Química del Sur; Argentina
description The main goal of this work is the application of an antimony film electrode (SbFE) prepared for the first time “in-situ” to determine organic compound as tetracyclines commonly used in Argentine for hive treatment. The SbFE was prepared on a glassy carbon electrode (GCE) and square wave cathodic stripping voltammetry (SWCSV) technique was used. The SWCSV parameters were optimized based on a Draper Lin small composite design. The SWCSV response was linear in the TCs concentration range from 0.40 to 3.00 μM with a limit of detection (LOD) of 0.15 μM. The proposed method is a good and simple alternative to the determination of tetracyclines in Argentinean honeys samples. Recovery experiments were performed using spiked honey samples with standard deviation values from 0.75% and 9.69%.
publishDate 2017
dc.date.none.fl_str_mv 2017-03-31
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/55290
Krepper, Gabriela; Pierini, Gastón Dario; Pistonesi, Marcelo Fabian; Di Nezio, Maria Susana; “In-situ” antimony film electrode for the determination of tetracyclines in Argentinean honey samples; Elsevier Science Sa; Sensors and Actuators B: Chemical; 241; 31-3-2017; 560-566
0925-4005
CONICET Digital
CONICET
url http://hdl.handle.net/11336/55290
identifier_str_mv Krepper, Gabriela; Pierini, Gastón Dario; Pistonesi, Marcelo Fabian; Di Nezio, Maria Susana; “In-situ” antimony film electrode for the determination of tetracyclines in Argentinean honey samples; Elsevier Science Sa; Sensors and Actuators B: Chemical; 241; 31-3-2017; 560-566
0925-4005
CONICET Digital
CONICET
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/url/https://www.sciencedirect.com/science/article/pii/S0925400516317579
info:eu-repo/semantics/altIdentifier/doi/10.1016/j.snb.2016.10.125
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
dc.publisher.none.fl_str_mv Elsevier Science Sa
publisher.none.fl_str_mv Elsevier Science Sa
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
_version_ 1844613657898516480
score 13.070432

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