Phase stability of 3Y-TSZ ceramics after different surface treatments

Autores
Calambas Pulgarin, Heydy Lorena; Albano, Maria Patricia; Garrido, Liliana Beatriz
Año de publicación
2015
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
The ability of zirconia ceramics to develop a bioactive surface is of great importance for biomedical applications. For that, it is also required to control phase stability (i.e. to avoid the tetragonal to monoclinic phase transformation) of zirconia surfaces in order to impart a high mechanical resistance. In this work, the phase stability of dense 3 mol% yttria stabilized-zirconia (3Y-TSZ) ceramics after acid and hydrothermal treatments was examined. Ceramic discs were prepared by slip casting from well dispersed 52 vol% suspensions, and subsequently sintered to 1300-1500 °C. The effect of various synthesis parameters and 0.25 wt% alumina doping on the phase transformation after acid and hydrothermal treatments was semi-quantitatively evaluated by XRD. The 3Y-TSZ sintered to 1500°C exhibited higher t→m transformation than samples sintered at lower temperatures. The phase transformation up to10h of hydrothermal treatment occurred by nucleation and growth mechanisms in which the nucleation process predominated. The presence of 0.25 wt% alumina in 3Y-TSZ sintered at 1500°C slightly enhanced the resistance to acid treatment.
Fil: Calambas Pulgarin, Heydy Lorena. Provincia de Buenos Aires. Gobernación. Comisión de Investigaciones Científicas. Centro de Tecnología de Recursos Minerales y Cerámica. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Centro de Tecnología de Recursos Minerales y Cerámica; Argentina
Fil: Albano, Maria Patricia. Provincia de Buenos Aires. Gobernación. Comisión de Investigaciones Científicas. Centro de Tecnología de Recursos Minerales y Cerámica. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Centro de Tecnología de Recursos Minerales y Cerámica; Argentina
Fil: Garrido, Liliana Beatriz. Provincia de Buenos Aires. Gobernación. Comisión de Investigaciones Científicas. Centro de Tecnología de Recursos Minerales y Cerámica. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Centro de Tecnología de Recursos Minerales y Cerámica; Argentina
Materia
3y-Tsz
Bioceramics
Phase Stability
Slip Casting
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/50935
Acceder
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oai_identifier_str oai:ri.conicet.gov.ar:11336/50935
network_acronym_str CONICETDig
repository_id_str 3498
network_name_str CONICET Digital (CONICET)
spelling Phase stability of 3Y-TSZ ceramics after different surface treatmentsCalambas Pulgarin, Heydy LorenaAlbano, Maria PatriciaGarrido, Liliana Beatriz3y-TszBioceramicsPhase StabilitySlip Castinghttps://purl.org/becyt/ford/2.5https://purl.org/becyt/ford/2The ability of zirconia ceramics to develop a bioactive surface is of great importance for biomedical applications. For that, it is also required to control phase stability (i.e. to avoid the tetragonal to monoclinic phase transformation) of zirconia surfaces in order to impart a high mechanical resistance. In this work, the phase stability of dense 3 mol% yttria stabilized-zirconia (3Y-TSZ) ceramics after acid and hydrothermal treatments was examined. Ceramic discs were prepared by slip casting from well dispersed 52 vol% suspensions, and subsequently sintered to 1300-1500 °C. The effect of various synthesis parameters and 0.25 wt% alumina doping on the phase transformation after acid and hydrothermal treatments was semi-quantitatively evaluated by XRD. The 3Y-TSZ sintered to 1500°C exhibited higher t→m transformation than samples sintered at lower temperatures. The phase transformation up to10h of hydrothermal treatment occurred by nucleation and growth mechanisms in which the nucleation process predominated. The presence of 0.25 wt% alumina in 3Y-TSZ sintered at 1500°C slightly enhanced the resistance to acid treatment.Fil: Calambas Pulgarin, Heydy Lorena. Provincia de Buenos Aires. Gobernación. Comisión de Investigaciones Científicas. Centro de Tecnología de Recursos Minerales y Cerámica. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Centro de Tecnología de Recursos Minerales y Cerámica; ArgentinaFil: Albano, Maria Patricia. Provincia de Buenos Aires. Gobernación. Comisión de Investigaciones Científicas. Centro de Tecnología de Recursos Minerales y Cerámica. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Centro de Tecnología de Recursos Minerales y Cerámica; ArgentinaFil: Garrido, Liliana Beatriz. Provincia de Buenos Aires. Gobernación. Comisión de Investigaciones Científicas. Centro de Tecnología de Recursos Minerales y Cerámica. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Centro de Tecnología de Recursos Minerales y Cerámica; ArgentinaTrans Tech Publications2015-06info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/50935Calambas Pulgarin, Heydy Lorena; Albano, Maria Patricia; Garrido, Liliana Beatriz; Phase stability of 3Y-TSZ ceramics after different surface treatments; Trans Tech Publications; Materials Science Forum; 820; 6-2015; 330-3340255-5476CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/url/https://www.scientific.net/MSF.820.330info:eu-repo/semantics/altIdentifier/doi/10.4028/www.scientific.net/MSF.820.330info:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-sa/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-09-29T09:49:42Zoai:ri.conicet.gov.ar:11336/50935instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-09-29 09:49:43.211CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Phase stability of 3Y-TSZ ceramics after different surface treatments
title Phase stability of 3Y-TSZ ceramics after different surface treatments
spellingShingle Phase stability of 3Y-TSZ ceramics after different surface treatments
Calambas Pulgarin, Heydy Lorena
3y-Tsz
Bioceramics
Phase Stability
Slip Casting
title_short Phase stability of 3Y-TSZ ceramics after different surface treatments
title_full Phase stability of 3Y-TSZ ceramics after different surface treatments
title_fullStr Phase stability of 3Y-TSZ ceramics after different surface treatments
title_full_unstemmed Phase stability of 3Y-TSZ ceramics after different surface treatments
title_sort Phase stability of 3Y-TSZ ceramics after different surface treatments
dc.creator.none.fl_str_mv Calambas Pulgarin, Heydy Lorena
Albano, Maria Patricia
Garrido, Liliana Beatriz
author Calambas Pulgarin, Heydy Lorena
author_facet Calambas Pulgarin, Heydy Lorena
Albano, Maria Patricia
Garrido, Liliana Beatriz
author_role author
author2 Albano, Maria Patricia
Garrido, Liliana Beatriz
author2_role author
author
dc.subject.none.fl_str_mv 3y-Tsz
Bioceramics
Phase Stability
Slip Casting
topic 3y-Tsz
Bioceramics
Phase Stability
Slip Casting
purl_subject.fl_str_mv https://purl.org/becyt/ford/2.5
https://purl.org/becyt/ford/2
dc.description.none.fl_txt_mv The ability of zirconia ceramics to develop a bioactive surface is of great importance for biomedical applications. For that, it is also required to control phase stability (i.e. to avoid the tetragonal to monoclinic phase transformation) of zirconia surfaces in order to impart a high mechanical resistance. In this work, the phase stability of dense 3 mol% yttria stabilized-zirconia (3Y-TSZ) ceramics after acid and hydrothermal treatments was examined. Ceramic discs were prepared by slip casting from well dispersed 52 vol% suspensions, and subsequently sintered to 1300-1500 °C. The effect of various synthesis parameters and 0.25 wt% alumina doping on the phase transformation after acid and hydrothermal treatments was semi-quantitatively evaluated by XRD. The 3Y-TSZ sintered to 1500°C exhibited higher t→m transformation than samples sintered at lower temperatures. The phase transformation up to10h of hydrothermal treatment occurred by nucleation and growth mechanisms in which the nucleation process predominated. The presence of 0.25 wt% alumina in 3Y-TSZ sintered at 1500°C slightly enhanced the resistance to acid treatment.
Fil: Calambas Pulgarin, Heydy Lorena. Provincia de Buenos Aires. Gobernación. Comisión de Investigaciones Científicas. Centro de Tecnología de Recursos Minerales y Cerámica. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Centro de Tecnología de Recursos Minerales y Cerámica; Argentina
Fil: Albano, Maria Patricia. Provincia de Buenos Aires. Gobernación. Comisión de Investigaciones Científicas. Centro de Tecnología de Recursos Minerales y Cerámica. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Centro de Tecnología de Recursos Minerales y Cerámica; Argentina
Fil: Garrido, Liliana Beatriz. Provincia de Buenos Aires. Gobernación. Comisión de Investigaciones Científicas. Centro de Tecnología de Recursos Minerales y Cerámica. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - La Plata. Centro de Tecnología de Recursos Minerales y Cerámica; Argentina
description The ability of zirconia ceramics to develop a bioactive surface is of great importance for biomedical applications. For that, it is also required to control phase stability (i.e. to avoid the tetragonal to monoclinic phase transformation) of zirconia surfaces in order to impart a high mechanical resistance. In this work, the phase stability of dense 3 mol% yttria stabilized-zirconia (3Y-TSZ) ceramics after acid and hydrothermal treatments was examined. Ceramic discs were prepared by slip casting from well dispersed 52 vol% suspensions, and subsequently sintered to 1300-1500 °C. The effect of various synthesis parameters and 0.25 wt% alumina doping on the phase transformation after acid and hydrothermal treatments was semi-quantitatively evaluated by XRD. The 3Y-TSZ sintered to 1500°C exhibited higher t→m transformation than samples sintered at lower temperatures. The phase transformation up to10h of hydrothermal treatment occurred by nucleation and growth mechanisms in which the nucleation process predominated. The presence of 0.25 wt% alumina in 3Y-TSZ sintered at 1500°C slightly enhanced the resistance to acid treatment.
publishDate 2015
dc.date.none.fl_str_mv 2015-06
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/50935
Calambas Pulgarin, Heydy Lorena; Albano, Maria Patricia; Garrido, Liliana Beatriz; Phase stability of 3Y-TSZ ceramics after different surface treatments; Trans Tech Publications; Materials Science Forum; 820; 6-2015; 330-334
0255-5476
CONICET Digital
CONICET
url http://hdl.handle.net/11336/50935
identifier_str_mv Calambas Pulgarin, Heydy Lorena; Albano, Maria Patricia; Garrido, Liliana Beatriz; Phase stability of 3Y-TSZ ceramics after different surface treatments; Trans Tech Publications; Materials Science Forum; 820; 6-2015; 330-334
0255-5476
CONICET Digital
CONICET
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/url/https://www.scientific.net/MSF.820.330
info:eu-repo/semantics/altIdentifier/doi/10.4028/www.scientific.net/MSF.820.330
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
application/pdf
dc.publisher.none.fl_str_mv Trans Tech Publications
publisher.none.fl_str_mv Trans Tech Publications
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
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score 13.070432

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