Turbidimetric and photometric determination of total tannins in tea using a micro-flow-batch analyzer
- Autores
- Lima, Marcelo B.; Andrade, Stéfani I. E.; Harding, David P.; Pistonesi, Marcelo Fabian; Fernández Band, Beatriz Susana; Araújo, Mário C.U.
- Año de publicación
- 2012
- Idioma
- inglés
- Tipo de recurso
- artículo
- Estado
- versión publicada
- Descripción
- Both turbidimetric and photometric determinations of total tannins in samples of green and black tea, using a micro-flow-batch analyzer (μFBA) were studied. The miniaturized system was formed using photocurable urethane-acrylate resin and ultraviolet lithography technique. The turbidimetric method was based on the precipitation reaction of Cu (II) with tannins in acetate medium at a pH of 4.5. The photometric method was based on the complexation reaction of tannins with ferrous tartrate. The turbidimetric μFBA was able to test 200 samples per hour. The photometric μFBA allowed 300 analyses per hour, generating 136 μL of residue per analysis. The paired t test, at a 95% confidence level, showed no statistically significant differences between results obtained by both methods and the reference method. The urethane-acrylate μFBA maintained satisfactory physical and chemical properties, and represents an improvement over conventional flow-batch analyzer.
Fil: Lima, Marcelo B.. Universidade Federal da Paraíba; Brasil
Fil: Andrade, Stéfani I. E.. Universidade Federal da Paraíba; Brasil
Fil: Harding, David P.. Universidade Federal da Paraíba; Brasil
Fil: Pistonesi, Marcelo Fabian. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Bahía Blanca. Instituto de Química del Sur. Universidad Nacional del Sur. Departamento de Química. Instituto de Química del Sur; Argentina
Fil: Fernández Band, Beatriz Susana. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Bahía Blanca. Instituto de Química del Sur. Universidad Nacional del Sur. Departamento de Química. Instituto de Química del Sur; Argentina
Fil: Araújo, Mário C.U.. Universidade Federal da Paraíba; Brasil - Materia
-
FLOW-BATCH SYSTEM
GREEN AND BLACK TEA
MICROFABRICATION
PHOTOMETRIC DETERMINATION
TANNINS
TURBIDIMETRIC DETERMINATION
URETHANE-ACRYLATE - Nivel de accesibilidad
- acceso abierto
- Condiciones de uso
- https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
- Repositorio
- Institución
- Consejo Nacional de Investigaciones Científicas y Técnicas
- OAI Identificador
- oai:ri.conicet.gov.ar:11336/58632
Ver los metadatos del registro completo
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Turbidimetric and photometric determination of total tannins in tea using a micro-flow-batch analyzerLima, Marcelo B.Andrade, Stéfani I. E.Harding, David P.Pistonesi, Marcelo FabianFernández Band, Beatriz SusanaAraújo, Mário C.U.FLOW-BATCH SYSTEMGREEN AND BLACK TEAMICROFABRICATIONPHOTOMETRIC DETERMINATIONTANNINSTURBIDIMETRIC DETERMINATIONURETHANE-ACRYLATEhttps://purl.org/becyt/ford/1.4https://purl.org/becyt/ford/1Both turbidimetric and photometric determinations of total tannins in samples of green and black tea, using a micro-flow-batch analyzer (μFBA) were studied. The miniaturized system was formed using photocurable urethane-acrylate resin and ultraviolet lithography technique. The turbidimetric method was based on the precipitation reaction of Cu (II) with tannins in acetate medium at a pH of 4.5. The photometric method was based on the complexation reaction of tannins with ferrous tartrate. The turbidimetric μFBA was able to test 200 samples per hour. The photometric μFBA allowed 300 analyses per hour, generating 136 μL of residue per analysis. The paired t test, at a 95% confidence level, showed no statistically significant differences between results obtained by both methods and the reference method. The urethane-acrylate μFBA maintained satisfactory physical and chemical properties, and represents an improvement over conventional flow-batch analyzer.Fil: Lima, Marcelo B.. Universidade Federal da Paraíba; BrasilFil: Andrade, Stéfani I. E.. Universidade Federal da Paraíba; BrasilFil: Harding, David P.. Universidade Federal da Paraíba; BrasilFil: Pistonesi, Marcelo Fabian. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Bahía Blanca. Instituto de Química del Sur. Universidad Nacional del Sur. Departamento de Química. Instituto de Química del Sur; ArgentinaFil: Fernández Band, Beatriz Susana. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Bahía Blanca. Instituto de Química del Sur. Universidad Nacional del Sur. Departamento de Química. Instituto de Química del Sur; ArgentinaFil: Araújo, Mário C.U.. Universidade Federal da Paraíba; BrasilElsevier Science2012-01-15info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfapplication/pdfapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/58632Lima, Marcelo B.; Andrade, Stéfani I. E.; Harding, David P.; Pistonesi, Marcelo Fabian; Fernández Band, Beatriz Susana; et al.; Turbidimetric and photometric determination of total tannins in tea using a micro-flow-batch analyzer; Elsevier Science; Talanta; 88; 15-1-2012; 717-7230039-9140CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/url/http://www.sciencedirect.com/science/article/pii/S0039914011010587info:eu-repo/semantics/altIdentifier/doi/10.1016/j.talanta.2011.11.076info:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-nd/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-09-03T09:53:39Zoai:ri.conicet.gov.ar:11336/58632instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-09-03 09:53:39.769CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse |
dc.title.none.fl_str_mv |
Turbidimetric and photometric determination of total tannins in tea using a micro-flow-batch analyzer |
title |
Turbidimetric and photometric determination of total tannins in tea using a micro-flow-batch analyzer |
spellingShingle |
Turbidimetric and photometric determination of total tannins in tea using a micro-flow-batch analyzer Lima, Marcelo B. FLOW-BATCH SYSTEM GREEN AND BLACK TEA MICROFABRICATION PHOTOMETRIC DETERMINATION TANNINS TURBIDIMETRIC DETERMINATION URETHANE-ACRYLATE |
title_short |
Turbidimetric and photometric determination of total tannins in tea using a micro-flow-batch analyzer |
title_full |
Turbidimetric and photometric determination of total tannins in tea using a micro-flow-batch analyzer |
title_fullStr |
Turbidimetric and photometric determination of total tannins in tea using a micro-flow-batch analyzer |
title_full_unstemmed |
Turbidimetric and photometric determination of total tannins in tea using a micro-flow-batch analyzer |
title_sort |
Turbidimetric and photometric determination of total tannins in tea using a micro-flow-batch analyzer |
dc.creator.none.fl_str_mv |
Lima, Marcelo B. Andrade, Stéfani I. E. Harding, David P. Pistonesi, Marcelo Fabian Fernández Band, Beatriz Susana Araújo, Mário C.U. |
author |
Lima, Marcelo B. |
author_facet |
Lima, Marcelo B. Andrade, Stéfani I. E. Harding, David P. Pistonesi, Marcelo Fabian Fernández Band, Beatriz Susana Araújo, Mário C.U. |
author_role |
author |
author2 |
Andrade, Stéfani I. E. Harding, David P. Pistonesi, Marcelo Fabian Fernández Band, Beatriz Susana Araújo, Mário C.U. |
author2_role |
author author author author author |
dc.subject.none.fl_str_mv |
FLOW-BATCH SYSTEM GREEN AND BLACK TEA MICROFABRICATION PHOTOMETRIC DETERMINATION TANNINS TURBIDIMETRIC DETERMINATION URETHANE-ACRYLATE |
topic |
FLOW-BATCH SYSTEM GREEN AND BLACK TEA MICROFABRICATION PHOTOMETRIC DETERMINATION TANNINS TURBIDIMETRIC DETERMINATION URETHANE-ACRYLATE |
purl_subject.fl_str_mv |
https://purl.org/becyt/ford/1.4 https://purl.org/becyt/ford/1 |
dc.description.none.fl_txt_mv |
Both turbidimetric and photometric determinations of total tannins in samples of green and black tea, using a micro-flow-batch analyzer (μFBA) were studied. The miniaturized system was formed using photocurable urethane-acrylate resin and ultraviolet lithography technique. The turbidimetric method was based on the precipitation reaction of Cu (II) with tannins in acetate medium at a pH of 4.5. The photometric method was based on the complexation reaction of tannins with ferrous tartrate. The turbidimetric μFBA was able to test 200 samples per hour. The photometric μFBA allowed 300 analyses per hour, generating 136 μL of residue per analysis. The paired t test, at a 95% confidence level, showed no statistically significant differences between results obtained by both methods and the reference method. The urethane-acrylate μFBA maintained satisfactory physical and chemical properties, and represents an improvement over conventional flow-batch analyzer. Fil: Lima, Marcelo B.. Universidade Federal da Paraíba; Brasil Fil: Andrade, Stéfani I. E.. Universidade Federal da Paraíba; Brasil Fil: Harding, David P.. Universidade Federal da Paraíba; Brasil Fil: Pistonesi, Marcelo Fabian. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Bahía Blanca. Instituto de Química del Sur. Universidad Nacional del Sur. Departamento de Química. Instituto de Química del Sur; Argentina Fil: Fernández Band, Beatriz Susana. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Bahía Blanca. Instituto de Química del Sur. Universidad Nacional del Sur. Departamento de Química. Instituto de Química del Sur; Argentina Fil: Araújo, Mário C.U.. Universidade Federal da Paraíba; Brasil |
description |
Both turbidimetric and photometric determinations of total tannins in samples of green and black tea, using a micro-flow-batch analyzer (μFBA) were studied. The miniaturized system was formed using photocurable urethane-acrylate resin and ultraviolet lithography technique. The turbidimetric method was based on the precipitation reaction of Cu (II) with tannins in acetate medium at a pH of 4.5. The photometric method was based on the complexation reaction of tannins with ferrous tartrate. The turbidimetric μFBA was able to test 200 samples per hour. The photometric μFBA allowed 300 analyses per hour, generating 136 μL of residue per analysis. The paired t test, at a 95% confidence level, showed no statistically significant differences between results obtained by both methods and the reference method. The urethane-acrylate μFBA maintained satisfactory physical and chemical properties, and represents an improvement over conventional flow-batch analyzer. |
publishDate |
2012 |
dc.date.none.fl_str_mv |
2012-01-15 |
dc.type.none.fl_str_mv |
info:eu-repo/semantics/article info:eu-repo/semantics/publishedVersion http://purl.org/coar/resource_type/c_6501 info:ar-repo/semantics/articulo |
format |
article |
status_str |
publishedVersion |
dc.identifier.none.fl_str_mv |
http://hdl.handle.net/11336/58632 Lima, Marcelo B.; Andrade, Stéfani I. E.; Harding, David P.; Pistonesi, Marcelo Fabian; Fernández Band, Beatriz Susana; et al.; Turbidimetric and photometric determination of total tannins in tea using a micro-flow-batch analyzer; Elsevier Science; Talanta; 88; 15-1-2012; 717-723 0039-9140 CONICET Digital CONICET |
url |
http://hdl.handle.net/11336/58632 |
identifier_str_mv |
Lima, Marcelo B.; Andrade, Stéfani I. E.; Harding, David P.; Pistonesi, Marcelo Fabian; Fernández Band, Beatriz Susana; et al.; Turbidimetric and photometric determination of total tannins in tea using a micro-flow-batch analyzer; Elsevier Science; Talanta; 88; 15-1-2012; 717-723 0039-9140 CONICET Digital CONICET |
dc.language.none.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
info:eu-repo/semantics/altIdentifier/url/http://www.sciencedirect.com/science/article/pii/S0039914011010587 info:eu-repo/semantics/altIdentifier/doi/10.1016/j.talanta.2011.11.076 |
dc.rights.none.fl_str_mv |
info:eu-repo/semantics/openAccess https://creativecommons.org/licenses/by-nc-nd/2.5/ar/ |
eu_rights_str_mv |
openAccess |
rights_invalid_str_mv |
https://creativecommons.org/licenses/by-nc-nd/2.5/ar/ |
dc.format.none.fl_str_mv |
application/pdf application/pdf application/pdf application/pdf application/pdf |
dc.publisher.none.fl_str_mv |
Elsevier Science |
publisher.none.fl_str_mv |
Elsevier Science |
dc.source.none.fl_str_mv |
reponame:CONICET Digital (CONICET) instname:Consejo Nacional de Investigaciones Científicas y Técnicas |
reponame_str |
CONICET Digital (CONICET) |
collection |
CONICET Digital (CONICET) |
instname_str |
Consejo Nacional de Investigaciones Científicas y Técnicas |
repository.name.fl_str_mv |
CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas |
repository.mail.fl_str_mv |
dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar |
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1842269239771136000 |
score |
13.13397 |