Surface modification of titanium by anodic oxidation in phosphoric acid at low potentials. Part 1. Structure, electronic properties and thickness of the anodic films

Autores
Gomez Sanchez, Andrea Valeria; Schreiner, Wido H.; Duffó, Gustavo Sergio; Ceré, Silvia
Año de publicación
2013
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
Titanium surface characteristics determine the degree of success of permanent implants. The topography, morphology of the surface in micro and nano scales, the impurities present and other characteristics are a main concern, and therefore a multi-technique approach is required in order to evaluate modification process effects on the surface. Surface modification of titanium in the nanometrical range was performed by means of anodisation in phosphoric with the aim of improving both the biocompatibility and the corrosion resistance in the biological media. Biocompatible characteristics of the modified titanium surface, as the presence of anatase in the oxide film and the incorporation of phosphate to the surface, were determined. Moreover, the electronic properties of the surface oxide presented a carrier number adequate for biomedical applications. The increase in the film thickness from 3 to 42 nm was estimated from EIS results when anodising potentials from 0 to 30 V were applied, whereas a bi-layer structure of the protective oxides formed was determined.
Fil: Gomez Sanchez, Andrea Valeria. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Fil: Schreiner, Wido H.. Universidade Federal do Paraná; Brasil
Fil: Duffó, Gustavo Sergio. Comisión Nacional de Energía Atómica. Gerencia del Área de Energía Nuclear. Unidad de Actividad de Materiales (CAC); Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina. Universidad Nacional de San Martín; Argentina
Fil: Ceré, Silvia. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Materia
Titanium
Anodic Oxide
Biomaterials
Surface Modification
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/24589

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spelling Surface modification of titanium by anodic oxidation in phosphoric acid at low potentials. Part 1. Structure, electronic properties and thickness of the anodic filmsGomez Sanchez, Andrea ValeriaSchreiner, Wido H.Duffó, Gustavo SergioCeré, SilviaTitaniumAnodic OxideBiomaterialsSurface Modificationhttps://purl.org/becyt/ford/2.5https://purl.org/becyt/ford/2Titanium surface characteristics determine the degree of success of permanent implants. The topography, morphology of the surface in micro and nano scales, the impurities present and other characteristics are a main concern, and therefore a multi-technique approach is required in order to evaluate modification process effects on the surface. Surface modification of titanium in the nanometrical range was performed by means of anodisation in phosphoric with the aim of improving both the biocompatibility and the corrosion resistance in the biological media. Biocompatible characteristics of the modified titanium surface, as the presence of anatase in the oxide film and the incorporation of phosphate to the surface, were determined. Moreover, the electronic properties of the surface oxide presented a carrier number adequate for biomedical applications. The increase in the film thickness from 3 to 42 nm was estimated from EIS results when anodising potentials from 0 to 30 V were applied, whereas a bi-layer structure of the protective oxides formed was determined.Fil: Gomez Sanchez, Andrea Valeria. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; ArgentinaFil: Schreiner, Wido H.. Universidade Federal do Paraná; BrasilFil: Duffó, Gustavo Sergio. Comisión Nacional de Energía Atómica. Gerencia del Área de Energía Nuclear. Unidad de Actividad de Materiales (CAC); Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina. Universidad Nacional de San Martín; ArgentinaFil: Ceré, Silvia. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; ArgentinaWiley2013-06info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/24589Gomez Sanchez, Andrea Valeria; Schreiner, Wido H.; Duffó, Gustavo Sergio; Ceré, Silvia; Surface modification of titanium by anodic oxidation in phosphoric acid at low potentials. Part 1. Structure, electronic properties and thickness of the anodic films; Wiley; Surface and Interface Analysis; 45; 6; 6-2013; 1037-10460142-24211096-9918CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/url/http://onlinelibrary.wiley.com/doi/10.1002/sia.5210/abstractinfo:eu-repo/semantics/altIdentifier/doi/10.1002/sia.5210info:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-sa/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-09-29T09:35:17Zoai:ri.conicet.gov.ar:11336/24589instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-09-29 09:35:17.934CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Surface modification of titanium by anodic oxidation in phosphoric acid at low potentials. Part 1. Structure, electronic properties and thickness of the anodic films
title Surface modification of titanium by anodic oxidation in phosphoric acid at low potentials. Part 1. Structure, electronic properties and thickness of the anodic films
spellingShingle Surface modification of titanium by anodic oxidation in phosphoric acid at low potentials. Part 1. Structure, electronic properties and thickness of the anodic films
Gomez Sanchez, Andrea Valeria
Titanium
Anodic Oxide
Biomaterials
Surface Modification
title_short Surface modification of titanium by anodic oxidation in phosphoric acid at low potentials. Part 1. Structure, electronic properties and thickness of the anodic films
title_full Surface modification of titanium by anodic oxidation in phosphoric acid at low potentials. Part 1. Structure, electronic properties and thickness of the anodic films
title_fullStr Surface modification of titanium by anodic oxidation in phosphoric acid at low potentials. Part 1. Structure, electronic properties and thickness of the anodic films
title_full_unstemmed Surface modification of titanium by anodic oxidation in phosphoric acid at low potentials. Part 1. Structure, electronic properties and thickness of the anodic films
title_sort Surface modification of titanium by anodic oxidation in phosphoric acid at low potentials. Part 1. Structure, electronic properties and thickness of the anodic films
dc.creator.none.fl_str_mv Gomez Sanchez, Andrea Valeria
Schreiner, Wido H.
Duffó, Gustavo Sergio
Ceré, Silvia
author Gomez Sanchez, Andrea Valeria
author_facet Gomez Sanchez, Andrea Valeria
Schreiner, Wido H.
Duffó, Gustavo Sergio
Ceré, Silvia
author_role author
author2 Schreiner, Wido H.
Duffó, Gustavo Sergio
Ceré, Silvia
author2_role author
author
author
dc.subject.none.fl_str_mv Titanium
Anodic Oxide
Biomaterials
Surface Modification
topic Titanium
Anodic Oxide
Biomaterials
Surface Modification
purl_subject.fl_str_mv https://purl.org/becyt/ford/2.5
https://purl.org/becyt/ford/2
dc.description.none.fl_txt_mv Titanium surface characteristics determine the degree of success of permanent implants. The topography, morphology of the surface in micro and nano scales, the impurities present and other characteristics are a main concern, and therefore a multi-technique approach is required in order to evaluate modification process effects on the surface. Surface modification of titanium in the nanometrical range was performed by means of anodisation in phosphoric with the aim of improving both the biocompatibility and the corrosion resistance in the biological media. Biocompatible characteristics of the modified titanium surface, as the presence of anatase in the oxide film and the incorporation of phosphate to the surface, were determined. Moreover, the electronic properties of the surface oxide presented a carrier number adequate for biomedical applications. The increase in the film thickness from 3 to 42 nm was estimated from EIS results when anodising potentials from 0 to 30 V were applied, whereas a bi-layer structure of the protective oxides formed was determined.
Fil: Gomez Sanchez, Andrea Valeria. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Fil: Schreiner, Wido H.. Universidade Federal do Paraná; Brasil
Fil: Duffó, Gustavo Sergio. Comisión Nacional de Energía Atómica. Gerencia del Área de Energía Nuclear. Unidad de Actividad de Materiales (CAC); Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina. Universidad Nacional de San Martín; Argentina
Fil: Ceré, Silvia. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
description Titanium surface characteristics determine the degree of success of permanent implants. The topography, morphology of the surface in micro and nano scales, the impurities present and other characteristics are a main concern, and therefore a multi-technique approach is required in order to evaluate modification process effects on the surface. Surface modification of titanium in the nanometrical range was performed by means of anodisation in phosphoric with the aim of improving both the biocompatibility and the corrosion resistance in the biological media. Biocompatible characteristics of the modified titanium surface, as the presence of anatase in the oxide film and the incorporation of phosphate to the surface, were determined. Moreover, the electronic properties of the surface oxide presented a carrier number adequate for biomedical applications. The increase in the film thickness from 3 to 42 nm was estimated from EIS results when anodising potentials from 0 to 30 V were applied, whereas a bi-layer structure of the protective oxides formed was determined.
publishDate 2013
dc.date.none.fl_str_mv 2013-06
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/24589
Gomez Sanchez, Andrea Valeria; Schreiner, Wido H.; Duffó, Gustavo Sergio; Ceré, Silvia; Surface modification of titanium by anodic oxidation in phosphoric acid at low potentials. Part 1. Structure, electronic properties and thickness of the anodic films; Wiley; Surface and Interface Analysis; 45; 6; 6-2013; 1037-1046
0142-2421
1096-9918
CONICET Digital
CONICET
url http://hdl.handle.net/11336/24589
identifier_str_mv Gomez Sanchez, Andrea Valeria; Schreiner, Wido H.; Duffó, Gustavo Sergio; Ceré, Silvia; Surface modification of titanium by anodic oxidation in phosphoric acid at low potentials. Part 1. Structure, electronic properties and thickness of the anodic films; Wiley; Surface and Interface Analysis; 45; 6; 6-2013; 1037-1046
0142-2421
1096-9918
CONICET Digital
CONICET
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language eng
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info:eu-repo/semantics/altIdentifier/doi/10.1002/sia.5210
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
dc.publisher.none.fl_str_mv Wiley
publisher.none.fl_str_mv Wiley
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