Easy synthesis of CaB<SUB>2</SUB>O<SUB>4</SUB> via pyrolysis of calcium fructoborate
- Autores
- Wagner, Claudia C.; Barán, Enrique José
- Año de publicación
- 2008
- Idioma
- inglés
- Tipo de recurso
- artículo
- Estado
- versión publicada
- Descripción
- The investigation of the thermal behavior of calcium fructoborate samples of composition Ca(C6H10O6BO)2.3.5H2O showed that CaB2O4 is generated as the final solid pyrolysis residue. On the basis of these observations a new, very easy, synthetic procedure for the preparation of high purity samples of this calcium borate is proposed. The material was characterized by X ray powder diffractometry and IR spectroscopy.
Facultad de Ingeniería - Materia
-
Ingeniería Química
Química
calcium borate
calcium fructoborate
IR spectra
high purity
new synthetic procedure
IR spectroscopy
pyrolysis residue
x ray analysis
synthetic procedures
thermal behaviors
X-ray powder diffractometry
pyrolysis - Nivel de accesibilidad
- acceso abierto
- Condiciones de uso
- http://creativecommons.org/licenses/by-nc-sa/3.0/
- Repositorio
.jpg)
- Institución
- Universidad Nacional de La Plata
- OAI Identificador
- oai:sedici.unlp.edu.ar:10915/38309
Ver los metadatos del registro completo
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Easy synthesis of CaB<SUB>2</SUB>O<SUB>4</SUB> via pyrolysis of calcium fructoborateWagner, Claudia C.Barán, Enrique JoséIngeniería QuímicaQuímicacalcium boratecalcium fructoborateIR spectrahigh puritynew synthetic procedureIR spectroscopypyrolysis residuex ray analysissynthetic proceduresthermal behaviorsX-ray powder diffractometrypyrolysisThe investigation of the thermal behavior of calcium fructoborate samples of composition Ca(C<SUB>6</SUB>H<SUB>10</SUB>O<SUB>6</SUB>BO)<SUB>2</SUB>.3.5H<SUB>2</SUB>O showed that CaB<SUB>2</SUB>O<SUB>4</SUB> is generated as the final solid pyrolysis residue. On the basis of these observations a new, very easy, synthetic procedure for the preparation of high purity samples of this calcium borate is proposed. The material was characterized by X ray powder diffractometry and IR spectroscopy.Facultad de Ingeniería2008info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionArticulohttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdf493-494http://sedici.unlp.edu.ar/handle/10915/38309enginfo:eu-repo/semantics/altIdentifier/url/http://www.scielo.br/pdf/mr/v11n4/20.pdfinfo:eu-repo/semantics/altIdentifier/issn/1516-1439info:eu-repo/semantics/openAccesshttp://creativecommons.org/licenses/by-nc-sa/3.0/Creative Commons Attribution-NonCommercial-ShareAlike 3.0 Unported (CC BY-NC-SA 3.0)reponame:SEDICI (UNLP)instname:Universidad Nacional de La Platainstacron:UNLP2025-10-15T10:49:41Zoai:sedici.unlp.edu.ar:10915/38309Institucionalhttp://sedici.unlp.edu.ar/Universidad públicaNo correspondehttp://sedici.unlp.edu.ar/oai/snrdalira@sedici.unlp.edu.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:13292025-10-15 10:49:41.41SEDICI (UNLP) - Universidad Nacional de La Platafalse |
| dc.title.none.fl_str_mv |
Easy synthesis of CaB<SUB>2</SUB>O<SUB>4</SUB> via pyrolysis of calcium fructoborate |
| title |
Easy synthesis of CaB<SUB>2</SUB>O<SUB>4</SUB> via pyrolysis of calcium fructoborate |
| spellingShingle |
Easy synthesis of CaB<SUB>2</SUB>O<SUB>4</SUB> via pyrolysis of calcium fructoborate Wagner, Claudia C. Ingeniería Química Química calcium borate calcium fructoborate IR spectra high purity new synthetic procedure IR spectroscopy pyrolysis residue x ray analysis synthetic procedures thermal behaviors X-ray powder diffractometry pyrolysis |
| title_short |
Easy synthesis of CaB<SUB>2</SUB>O<SUB>4</SUB> via pyrolysis of calcium fructoborate |
| title_full |
Easy synthesis of CaB<SUB>2</SUB>O<SUB>4</SUB> via pyrolysis of calcium fructoborate |
| title_fullStr |
Easy synthesis of CaB<SUB>2</SUB>O<SUB>4</SUB> via pyrolysis of calcium fructoborate |
| title_full_unstemmed |
Easy synthesis of CaB<SUB>2</SUB>O<SUB>4</SUB> via pyrolysis of calcium fructoborate |
| title_sort |
Easy synthesis of CaB<SUB>2</SUB>O<SUB>4</SUB> via pyrolysis of calcium fructoborate |
| dc.creator.none.fl_str_mv |
Wagner, Claudia C. Barán, Enrique José |
| author |
Wagner, Claudia C. |
| author_facet |
Wagner, Claudia C. Barán, Enrique José |
| author_role |
author |
| author2 |
Barán, Enrique José |
| author2_role |
author |
| dc.subject.none.fl_str_mv |
Ingeniería Química Química calcium borate calcium fructoborate IR spectra high purity new synthetic procedure IR spectroscopy pyrolysis residue x ray analysis synthetic procedures thermal behaviors X-ray powder diffractometry pyrolysis |
| topic |
Ingeniería Química Química calcium borate calcium fructoborate IR spectra high purity new synthetic procedure IR spectroscopy pyrolysis residue x ray analysis synthetic procedures thermal behaviors X-ray powder diffractometry pyrolysis |
| dc.description.none.fl_txt_mv |
The investigation of the thermal behavior of calcium fructoborate samples of composition Ca(C<SUB>6</SUB>H<SUB>10</SUB>O<SUB>6</SUB>BO)<SUB>2</SUB>.3.5H<SUB>2</SUB>O showed that CaB<SUB>2</SUB>O<SUB>4</SUB> is generated as the final solid pyrolysis residue. On the basis of these observations a new, very easy, synthetic procedure for the preparation of high purity samples of this calcium borate is proposed. The material was characterized by X ray powder diffractometry and IR spectroscopy. Facultad de Ingeniería |
| description |
The investigation of the thermal behavior of calcium fructoborate samples of composition Ca(C<SUB>6</SUB>H<SUB>10</SUB>O<SUB>6</SUB>BO)<SUB>2</SUB>.3.5H<SUB>2</SUB>O showed that CaB<SUB>2</SUB>O<SUB>4</SUB> is generated as the final solid pyrolysis residue. On the basis of these observations a new, very easy, synthetic procedure for the preparation of high purity samples of this calcium borate is proposed. The material was characterized by X ray powder diffractometry and IR spectroscopy. |
| publishDate |
2008 |
| dc.date.none.fl_str_mv |
2008 |
| dc.type.none.fl_str_mv |
info:eu-repo/semantics/article info:eu-repo/semantics/publishedVersion Articulo http://purl.org/coar/resource_type/c_6501 info:ar-repo/semantics/articulo |
| format |
article |
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publishedVersion |
| dc.identifier.none.fl_str_mv |
http://sedici.unlp.edu.ar/handle/10915/38309 |
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http://sedici.unlp.edu.ar/handle/10915/38309 |
| dc.language.none.fl_str_mv |
eng |
| language |
eng |
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info:eu-repo/semantics/altIdentifier/url/http://www.scielo.br/pdf/mr/v11n4/20.pdf info:eu-repo/semantics/altIdentifier/issn/1516-1439 |
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openAccess |
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http://creativecommons.org/licenses/by-nc-sa/3.0/ Creative Commons Attribution-NonCommercial-ShareAlike 3.0 Unported (CC BY-NC-SA 3.0) |
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application/pdf 493-494 |
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