Influence of the synthesis time in the textural and structural properties of Ni-Containing Mesoporous materials

Autores
Carraro, Paola María; Eimer, Griselda Alejandra; Oliva, Marcos Iván
Año de publicación
2015
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
MCM-41 materials have been synthesized by hydrothermal synthesis, and the influence of the synthesis time variation on the structural and textural properties of the final solids was studied. Nickel-modified samples were synthesized with a molar ratio Si/Ni of 60 and increased days of synthesis from 0 to 7 days. The structures obtained were characterized by X-ray diffraction (XRD) and UV-vis diffuse reflectance (UV–Vis DRS) spectroscopy. XRD patterns of samples are typical of MCM-41 structure, which improves with increasing the time of hydrothermal treatment. XRD and UV–vis studies revealed that the short synthesis times do not allow the proper incorporation of nickel in the structure. It was corroborated that, the synthesis time has an important influence on the properties of mesoporous material modified with Ni.
Fil: Carraro, Paola María. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Córdoba. Instituto de Física "enrique Gaviola"; Argentina. Consejo Nacional de Investigaciones Cientificas y Tecnicas. Centro Cientifico Tecnologico Cordoba. Centro de Investigacion y Tecnologia Quimica; Argentina
Fil: Eimer, Griselda Alejandra. Consejo Nacional de Investigaciones Cientificas y Tecnicas. Centro Cientifico Tecnologico Cordoba. Centro de Investigacion y Tecnologia Quimica; Argentina
Fil: Oliva, Marcos Iván. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Córdoba. Instituto de Física "enrique Gaviola"; Argentina. Universidad Nacional de Córdoba. Facultad de Matemática, Astronomía y Física; Argentina
Materia
MCM-41
Niquel
Synthesis time
Mesoporous materials
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/10958
Acceder
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oai_identifier_str oai:ri.conicet.gov.ar:11336/10958
network_acronym_str CONICETDig
repository_id_str 3498
network_name_str CONICET Digital (CONICET)
spelling Influence of the synthesis time in the textural and structural properties of Ni-Containing Mesoporous materialsCarraro, Paola MaríaEimer, Griselda AlejandraOliva, Marcos IvánMCM-41NiquelSynthesis timeMesoporous materialshttps://purl.org/becyt/ford/2.5https://purl.org/becyt/ford/2https://purl.org/becyt/ford/2.5https://purl.org/becyt/ford/2MCM-41 materials have been synthesized by hydrothermal synthesis, and the influence of the synthesis time variation on the structural and textural properties of the final solids was studied. Nickel-modified samples were synthesized with a molar ratio Si/Ni of 60 and increased days of synthesis from 0 to 7 days. The structures obtained were characterized by X-ray diffraction (XRD) and UV-vis diffuse reflectance (UV–Vis DRS) spectroscopy. XRD patterns of samples are typical of MCM-41 structure, which improves with increasing the time of hydrothermal treatment. XRD and UV–vis studies revealed that the short synthesis times do not allow the proper incorporation of nickel in the structure. It was corroborated that, the synthesis time has an important influence on the properties of mesoporous material modified with Ni.Fil: Carraro, Paola María. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Córdoba. Instituto de Física "enrique Gaviola"; Argentina. Consejo Nacional de Investigaciones Cientificas y Tecnicas. Centro Cientifico Tecnologico Cordoba. Centro de Investigacion y Tecnologia Quimica; ArgentinaFil: Eimer, Griselda Alejandra. Consejo Nacional de Investigaciones Cientificas y Tecnicas. Centro Cientifico Tecnologico Cordoba. Centro de Investigacion y Tecnologia Quimica; ArgentinaFil: Oliva, Marcos Iván. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Córdoba. Instituto de Física "enrique Gaviola"; Argentina. Universidad Nacional de Córdoba. Facultad de Matemática, Astronomía y Física; ArgentinaElsevier Science2015info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/10958Carraro, Paola María; Eimer, Griselda Alejandra; Oliva, Marcos Iván; Influence of the synthesis time in the textural and structural properties of Ni-Containing Mesoporous materials; Elsevier Science; Procedia Materials Science; 8; -1-2015; 561-5662211-8128enginfo:eu-repo/semantics/altIdentifier/doi/10.1016/j.mspro.2015.04.109info:eu-repo/semantics/altIdentifier/url/http://www.sciencedirect.com/science/article/pii/S2211812815001108info:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-nd/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-09-03T09:55:20Zoai:ri.conicet.gov.ar:11336/10958instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-09-03 09:55:20.975CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Influence of the synthesis time in the textural and structural properties of Ni-Containing Mesoporous materials
title Influence of the synthesis time in the textural and structural properties of Ni-Containing Mesoporous materials
spellingShingle Influence of the synthesis time in the textural and structural properties of Ni-Containing Mesoporous materials
Carraro, Paola María
MCM-41
Niquel
Synthesis time
Mesoporous materials
title_short Influence of the synthesis time in the textural and structural properties of Ni-Containing Mesoporous materials
title_full Influence of the synthesis time in the textural and structural properties of Ni-Containing Mesoporous materials
title_fullStr Influence of the synthesis time in the textural and structural properties of Ni-Containing Mesoporous materials
title_full_unstemmed Influence of the synthesis time in the textural and structural properties of Ni-Containing Mesoporous materials
title_sort Influence of the synthesis time in the textural and structural properties of Ni-Containing Mesoporous materials
dc.creator.none.fl_str_mv Carraro, Paola María
Eimer, Griselda Alejandra
Oliva, Marcos Iván
author Carraro, Paola María
author_facet Carraro, Paola María
Eimer, Griselda Alejandra
Oliva, Marcos Iván
author_role author
author2 Eimer, Griselda Alejandra
Oliva, Marcos Iván
author2_role author
author
dc.subject.none.fl_str_mv MCM-41
Niquel
Synthesis time
Mesoporous materials
topic MCM-41
Niquel
Synthesis time
Mesoporous materials
purl_subject.fl_str_mv https://purl.org/becyt/ford/2.5
https://purl.org/becyt/ford/2
https://purl.org/becyt/ford/2.5
https://purl.org/becyt/ford/2
dc.description.none.fl_txt_mv MCM-41 materials have been synthesized by hydrothermal synthesis, and the influence of the synthesis time variation on the structural and textural properties of the final solids was studied. Nickel-modified samples were synthesized with a molar ratio Si/Ni of 60 and increased days of synthesis from 0 to 7 days. The structures obtained were characterized by X-ray diffraction (XRD) and UV-vis diffuse reflectance (UV–Vis DRS) spectroscopy. XRD patterns of samples are typical of MCM-41 structure, which improves with increasing the time of hydrothermal treatment. XRD and UV–vis studies revealed that the short synthesis times do not allow the proper incorporation of nickel in the structure. It was corroborated that, the synthesis time has an important influence on the properties of mesoporous material modified with Ni.
Fil: Carraro, Paola María. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Córdoba. Instituto de Física "enrique Gaviola"; Argentina. Consejo Nacional de Investigaciones Cientificas y Tecnicas. Centro Cientifico Tecnologico Cordoba. Centro de Investigacion y Tecnologia Quimica; Argentina
Fil: Eimer, Griselda Alejandra. Consejo Nacional de Investigaciones Cientificas y Tecnicas. Centro Cientifico Tecnologico Cordoba. Centro de Investigacion y Tecnologia Quimica; Argentina
Fil: Oliva, Marcos Iván. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Córdoba. Instituto de Física "enrique Gaviola"; Argentina. Universidad Nacional de Córdoba. Facultad de Matemática, Astronomía y Física; Argentina
description MCM-41 materials have been synthesized by hydrothermal synthesis, and the influence of the synthesis time variation on the structural and textural properties of the final solids was studied. Nickel-modified samples were synthesized with a molar ratio Si/Ni of 60 and increased days of synthesis from 0 to 7 days. The structures obtained were characterized by X-ray diffraction (XRD) and UV-vis diffuse reflectance (UV–Vis DRS) spectroscopy. XRD patterns of samples are typical of MCM-41 structure, which improves with increasing the time of hydrothermal treatment. XRD and UV–vis studies revealed that the short synthesis times do not allow the proper incorporation of nickel in the structure. It was corroborated that, the synthesis time has an important influence on the properties of mesoporous material modified with Ni.
publishDate 2015
dc.date.none.fl_str_mv 2015
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/10958
Carraro, Paola María; Eimer, Griselda Alejandra; Oliva, Marcos Iván; Influence of the synthesis time in the textural and structural properties of Ni-Containing Mesoporous materials; Elsevier Science; Procedia Materials Science; 8; -1-2015; 561-566
2211-8128
url http://hdl.handle.net/11336/10958
identifier_str_mv Carraro, Paola María; Eimer, Griselda Alejandra; Oliva, Marcos Iván; Influence of the synthesis time in the textural and structural properties of Ni-Containing Mesoporous materials; Elsevier Science; Procedia Materials Science; 8; -1-2015; 561-566
2211-8128
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/doi/10.1016/j.mspro.2015.04.109
info:eu-repo/semantics/altIdentifier/url/http://www.sciencedirect.com/science/article/pii/S2211812815001108
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
application/pdf
application/pdf
dc.publisher.none.fl_str_mv Elsevier Science
publisher.none.fl_str_mv Elsevier Science
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
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score 13.13397

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