Characterization of crystallographic texture of Zirconium alloy components by neutron diffraction

Autores
Malamud, Florencia; Moya Riffo, Alvaro Esteban; Vicente Alvarez, Miguel Angel; Vizcaino, Pablo; Li, M.J.; Liu, X.; Vogel, S.C.; Law, M.; Sumin, V.V.; Luzin, V.; Vasin, R.N.; Santisteban, Javier Roberto
Año de publicación
2018
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
The reproducibility of the determination of crystallographic texture of Zr-based components by neutron diffraction has been studied through a small round-robin exercise, with the participation of texture and residual stress diffractometers from five international laboratories. Both constant-wavelength and polychromatic neutron beams have been used to define the texture of specimens from a warm-rolled and annealed Zircaloy-4 plate, and from a Zr-2.5%Nb pressure tube. Measurements were also compared to synchrotron high energy X-ray diffraction experiments, as a complementary volumetric technique with much shorter data collection times compared to neutrons. Results are qualitatively consistent and reproducible in terms of pole figures and orientation distribution function, underlining the suitability of neutrons for bulk texture measurements. Expected uncertainty of measurements has been quantified by global parameters such as texture indexes and Kearns factors, and local parameters associated to the main texture components (volume fraction, centroids, and widths of fiber components). The typical uncertainties found for these parameters are compared to spatial differences found in a small batch of cold-rolled Zr-2.5%Nb pressure tubes.
Fil: Malamud, Florencia. Comisión Nacional de Energía Atómica. Centro Atómico Bariloche; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Patagonia Norte; Argentina
Fil: Moya Riffo, Alvaro Esteban. Comisión Nacional de Energía Atómica. Centro Atómico Bariloche; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Patagonia Norte; Argentina
Fil: Vicente Alvarez, Miguel Angel. Comisión Nacional de Energía Atómica. Centro Atómico Bariloche; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Patagonia Norte; Argentina
Fil: Vizcaino, Pablo. Comisión Nacional de Energía Atómica. Centro Atómico Ezeiza; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina
Fil: Li, M.J.. No especifíca;
Fil: Liu, X.. No especifíca;
Fil: Vogel, S.C.. No especifíca;
Fil: Law, M.. Australian Nuclear Science And Technology Organisation; Australia
Fil: Sumin, V.V.. Joint Institute For Nuclear Research; Rusia
Fil: Luzin, V.. Australian Nuclear Science And Technology Organisation; Australia
Fil: Vasin, R.N.. Joint Institute For Nuclear Research; Rusia
Fil: Santisteban, Javier Roberto. Comisión Nacional de Energía Atómica. Centro Atómico Bariloche; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Patagonia Norte; Argentina
Materia
CRYSTALLOGRAPHIC TEXTURE
ZIRCONIUM ALLOYS
NEUTRON DIFFRACTION
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/112312
Acceder
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oai_identifier_str oai:ri.conicet.gov.ar:11336/112312
network_acronym_str CONICETDig
repository_id_str 3498
network_name_str CONICET Digital (CONICET)
spelling Characterization of crystallographic texture of Zirconium alloy components by neutron diffractionMalamud, FlorenciaMoya Riffo, Alvaro EstebanVicente Alvarez, Miguel AngelVizcaino, PabloLi, M.J.Liu, X.Vogel, S.C.Law, M.Sumin, V.V.Luzin, V.Vasin, R.N.Santisteban, Javier RobertoCRYSTALLOGRAPHIC TEXTUREZIRCONIUM ALLOYSNEUTRON DIFFRACTIONhttps://purl.org/becyt/ford/2.5https://purl.org/becyt/ford/2The reproducibility of the determination of crystallographic texture of Zr-based components by neutron diffraction has been studied through a small round-robin exercise, with the participation of texture and residual stress diffractometers from five international laboratories. Both constant-wavelength and polychromatic neutron beams have been used to define the texture of specimens from a warm-rolled and annealed Zircaloy-4 plate, and from a Zr-2.5%Nb pressure tube. Measurements were also compared to synchrotron high energy X-ray diffraction experiments, as a complementary volumetric technique with much shorter data collection times compared to neutrons. Results are qualitatively consistent and reproducible in terms of pole figures and orientation distribution function, underlining the suitability of neutrons for bulk texture measurements. Expected uncertainty of measurements has been quantified by global parameters such as texture indexes and Kearns factors, and local parameters associated to the main texture components (volume fraction, centroids, and widths of fiber components). The typical uncertainties found for these parameters are compared to spatial differences found in a small batch of cold-rolled Zr-2.5%Nb pressure tubes.Fil: Malamud, Florencia. Comisión Nacional de Energía Atómica. Centro Atómico Bariloche; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Patagonia Norte; ArgentinaFil: Moya Riffo, Alvaro Esteban. Comisión Nacional de Energía Atómica. Centro Atómico Bariloche; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Patagonia Norte; ArgentinaFil: Vicente Alvarez, Miguel Angel. Comisión Nacional de Energía Atómica. Centro Atómico Bariloche; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Patagonia Norte; ArgentinaFil: Vizcaino, Pablo. Comisión Nacional de Energía Atómica. Centro Atómico Ezeiza; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas; ArgentinaFil: Li, M.J.. No especifíca;Fil: Liu, X.. No especifíca;Fil: Vogel, S.C.. No especifíca;Fil: Law, M.. Australian Nuclear Science And Technology Organisation; AustraliaFil: Sumin, V.V.. Joint Institute For Nuclear Research; RusiaFil: Luzin, V.. Australian Nuclear Science And Technology Organisation; AustraliaFil: Vasin, R.N.. Joint Institute For Nuclear Research; RusiaFil: Santisteban, Javier Roberto. Comisión Nacional de Energía Atómica. Centro Atómico Bariloche; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Patagonia Norte; ArgentinaElsevier Science2018-11info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfapplication/pdfapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/112312Malamud, Florencia; Moya Riffo, Alvaro Esteban; Vicente Alvarez, Miguel Angel; Vizcaino, Pablo; Li, M.J.; et al.; Characterization of crystallographic texture of Zirconium alloy components by neutron diffraction; Elsevier Science; Journal of Nuclear Materials; 510; 11-2018; 524-5380022-3115CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/url/https://linkinghub.elsevier.com/retrieve/pii/S0022311518308341info:eu-repo/semantics/altIdentifier/doi/10.1016/j.jnucmat.2018.08.003info:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-sa/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-09-29T09:52:43Zoai:ri.conicet.gov.ar:11336/112312instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-09-29 09:52:43.689CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Characterization of crystallographic texture of Zirconium alloy components by neutron diffraction
title Characterization of crystallographic texture of Zirconium alloy components by neutron diffraction
spellingShingle Characterization of crystallographic texture of Zirconium alloy components by neutron diffraction
Malamud, Florencia
CRYSTALLOGRAPHIC TEXTURE
ZIRCONIUM ALLOYS
NEUTRON DIFFRACTION
title_short Characterization of crystallographic texture of Zirconium alloy components by neutron diffraction
title_full Characterization of crystallographic texture of Zirconium alloy components by neutron diffraction
title_fullStr Characterization of crystallographic texture of Zirconium alloy components by neutron diffraction
title_full_unstemmed Characterization of crystallographic texture of Zirconium alloy components by neutron diffraction
title_sort Characterization of crystallographic texture of Zirconium alloy components by neutron diffraction
dc.creator.none.fl_str_mv Malamud, Florencia
Moya Riffo, Alvaro Esteban
Vicente Alvarez, Miguel Angel
Vizcaino, Pablo
Li, M.J.
Liu, X.
Vogel, S.C.
Law, M.
Sumin, V.V.
Luzin, V.
Vasin, R.N.
Santisteban, Javier Roberto
author Malamud, Florencia
author_facet Malamud, Florencia
Moya Riffo, Alvaro Esteban
Vicente Alvarez, Miguel Angel
Vizcaino, Pablo
Li, M.J.
Liu, X.
Vogel, S.C.
Law, M.
Sumin, V.V.
Luzin, V.
Vasin, R.N.
Santisteban, Javier Roberto
author_role author
author2 Moya Riffo, Alvaro Esteban
Vicente Alvarez, Miguel Angel
Vizcaino, Pablo
Li, M.J.
Liu, X.
Vogel, S.C.
Law, M.
Sumin, V.V.
Luzin, V.
Vasin, R.N.
Santisteban, Javier Roberto
author2_role author
author
author
author
author
author
author
author
author
author
author
dc.subject.none.fl_str_mv CRYSTALLOGRAPHIC TEXTURE
ZIRCONIUM ALLOYS
NEUTRON DIFFRACTION
topic CRYSTALLOGRAPHIC TEXTURE
ZIRCONIUM ALLOYS
NEUTRON DIFFRACTION
purl_subject.fl_str_mv https://purl.org/becyt/ford/2.5
https://purl.org/becyt/ford/2
dc.description.none.fl_txt_mv The reproducibility of the determination of crystallographic texture of Zr-based components by neutron diffraction has been studied through a small round-robin exercise, with the participation of texture and residual stress diffractometers from five international laboratories. Both constant-wavelength and polychromatic neutron beams have been used to define the texture of specimens from a warm-rolled and annealed Zircaloy-4 plate, and from a Zr-2.5%Nb pressure tube. Measurements were also compared to synchrotron high energy X-ray diffraction experiments, as a complementary volumetric technique with much shorter data collection times compared to neutrons. Results are qualitatively consistent and reproducible in terms of pole figures and orientation distribution function, underlining the suitability of neutrons for bulk texture measurements. Expected uncertainty of measurements has been quantified by global parameters such as texture indexes and Kearns factors, and local parameters associated to the main texture components (volume fraction, centroids, and widths of fiber components). The typical uncertainties found for these parameters are compared to spatial differences found in a small batch of cold-rolled Zr-2.5%Nb pressure tubes.
Fil: Malamud, Florencia. Comisión Nacional de Energía Atómica. Centro Atómico Bariloche; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Patagonia Norte; Argentina
Fil: Moya Riffo, Alvaro Esteban. Comisión Nacional de Energía Atómica. Centro Atómico Bariloche; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Patagonia Norte; Argentina
Fil: Vicente Alvarez, Miguel Angel. Comisión Nacional de Energía Atómica. Centro Atómico Bariloche; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Patagonia Norte; Argentina
Fil: Vizcaino, Pablo. Comisión Nacional de Energía Atómica. Centro Atómico Ezeiza; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina
Fil: Li, M.J.. No especifíca;
Fil: Liu, X.. No especifíca;
Fil: Vogel, S.C.. No especifíca;
Fil: Law, M.. Australian Nuclear Science And Technology Organisation; Australia
Fil: Sumin, V.V.. Joint Institute For Nuclear Research; Rusia
Fil: Luzin, V.. Australian Nuclear Science And Technology Organisation; Australia
Fil: Vasin, R.N.. Joint Institute For Nuclear Research; Rusia
Fil: Santisteban, Javier Roberto. Comisión Nacional de Energía Atómica. Centro Atómico Bariloche; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Patagonia Norte; Argentina
description The reproducibility of the determination of crystallographic texture of Zr-based components by neutron diffraction has been studied through a small round-robin exercise, with the participation of texture and residual stress diffractometers from five international laboratories. Both constant-wavelength and polychromatic neutron beams have been used to define the texture of specimens from a warm-rolled and annealed Zircaloy-4 plate, and from a Zr-2.5%Nb pressure tube. Measurements were also compared to synchrotron high energy X-ray diffraction experiments, as a complementary volumetric technique with much shorter data collection times compared to neutrons. Results are qualitatively consistent and reproducible in terms of pole figures and orientation distribution function, underlining the suitability of neutrons for bulk texture measurements. Expected uncertainty of measurements has been quantified by global parameters such as texture indexes and Kearns factors, and local parameters associated to the main texture components (volume fraction, centroids, and widths of fiber components). The typical uncertainties found for these parameters are compared to spatial differences found in a small batch of cold-rolled Zr-2.5%Nb pressure tubes.
publishDate 2018
dc.date.none.fl_str_mv 2018-11
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/112312
Malamud, Florencia; Moya Riffo, Alvaro Esteban; Vicente Alvarez, Miguel Angel; Vizcaino, Pablo; Li, M.J.; et al.; Characterization of crystallographic texture of Zirconium alloy components by neutron diffraction; Elsevier Science; Journal of Nuclear Materials; 510; 11-2018; 524-538
0022-3115
CONICET Digital
CONICET
url http://hdl.handle.net/11336/112312
identifier_str_mv Malamud, Florencia; Moya Riffo, Alvaro Esteban; Vicente Alvarez, Miguel Angel; Vizcaino, Pablo; Li, M.J.; et al.; Characterization of crystallographic texture of Zirconium alloy components by neutron diffraction; Elsevier Science; Journal of Nuclear Materials; 510; 11-2018; 524-538
0022-3115
CONICET Digital
CONICET
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/url/https://linkinghub.elsevier.com/retrieve/pii/S0022311518308341
info:eu-repo/semantics/altIdentifier/doi/10.1016/j.jnucmat.2018.08.003
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
application/pdf
application/pdf
application/pdf
dc.publisher.none.fl_str_mv Elsevier Science
publisher.none.fl_str_mv Elsevier Science
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
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score 13.070432

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