Taguchi's Methodology for Determining Optimum Operating Conditions in Hydrothermal Pretreatments Applied to Canola Seeds

Autores
Fernández, María Belén; Burnet, Margarita A.; Perez, Ethel; Crapiste, Guillermo Hector; Nolasco, Susana Maria
Año de publicación
2014
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
The aim of the present work was to determine the operational optimum conditions in hydrothermal pretreatments applied to canola seeds. The effect of these pretreatments on the canola oil extraction yield and quality was evaluated. Sample was characterized by proximal analysis. As determinations of oil quality, acidity and peroxide value, tocopherol content and acidic composition were studied. Seeds were exposed to direct vapor in an autoclave. Pretreatments were carried out using different condition of temperature (100, 120 and 130°C), exposition time (5, 15 y 30 min) and seed granulometry (milled seeds, with a particle size in a range from 0.420 mm to 1.000 mm; broken seeds, with a particle size ranging from 1.000 mm to 1.410 mm and entire seeds). After each hydrothermal pretreatment, oil extraction yield was obtained with the Soxhlet method (hexane). The Taguchi methodology was followed in order to explore the operational optimum conditions selecting the most favorable levels of each variable, using an L9 experimental design. Initial oil content was 44.2 % dry basis (db). The best values of oil yield and quality were obtained when a temperature of 120°C, a time of 5 min and broken seeds were used. The optimum experiment generated an oil yield increment of 25% respect to the not hydrothermally-treated seed, meanwhile quality parameters remained within the commercialization values accepted.
Fil: Fernández, María Belén. Universidad Nacional del Centro de la Provincia de Buenos Aires. Facultad de Ingenieria Olavarria. Grupo Tecnologias de Semillas; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Tandil. Centro de Investigaciones en Física e Ingeniería del Centro de la Provincia de Buenos Aires; Argentina
Fil: Burnet, Margarita A.. Universidad Nacional del Centro de la Provincia de Buenos Aires. Facultad de Ingenieria Olavarria. Grupo Tecnologias de Semillas; Argentina
Fil: Perez, Ethel. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Bahía Blanca. Planta Piloto de Ingeniería Química (i); Argentina
Fil: Crapiste, Guillermo Hector. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Bahía Blanca. Planta Piloto de Ingeniería Química (i); Argentina
Fil: Nolasco, Susana Maria. Universidad Nacional del Centro de la Provincia de Buenos Aires. Facultad de Ingenieria Olavarria. Grupo Tecnologias de Semillas; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Tandil. Centro de Investigaciones en Física e Ingeniería del Centro de la Provincia de Buenos Aires; Argentina
Materia
Taguchi'S Methodology
Hydrothermal Pretreatment
Canola
Oil Yield And Quality
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/4677
Acceder
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oai_identifier_str oai:ri.conicet.gov.ar:11336/4677
network_acronym_str CONICETDig
repository_id_str 3498
network_name_str CONICET Digital (CONICET)
spelling Taguchi's Methodology for Determining Optimum Operating Conditions in Hydrothermal Pretreatments Applied to Canola SeedsFernández, María BelénBurnet, Margarita A.Perez, EthelCrapiste, Guillermo HectorNolasco, Susana MariaTaguchi'S MethodologyHydrothermal PretreatmentCanolaOil Yield And Qualityhttps://purl.org/becyt/ford/2.4https://purl.org/becyt/ford/2The aim of the present work was to determine the operational optimum conditions in hydrothermal pretreatments applied to canola seeds. The effect of these pretreatments on the canola oil extraction yield and quality was evaluated. Sample was characterized by proximal analysis. As determinations of oil quality, acidity and peroxide value, tocopherol content and acidic composition were studied. Seeds were exposed to direct vapor in an autoclave. Pretreatments were carried out using different condition of temperature (100, 120 and 130°C), exposition time (5, 15 y 30 min) and seed granulometry (milled seeds, with a particle size in a range from 0.420 mm to 1.000 mm; broken seeds, with a particle size ranging from 1.000 mm to 1.410 mm and entire seeds). After each hydrothermal pretreatment, oil extraction yield was obtained with the Soxhlet method (hexane). The Taguchi methodology was followed in order to explore the operational optimum conditions selecting the most favorable levels of each variable, using an L9 experimental design. Initial oil content was 44.2 % dry basis (db). The best values of oil yield and quality were obtained when a temperature of 120°C, a time of 5 min and broken seeds were used. The optimum experiment generated an oil yield increment of 25% respect to the not hydrothermally-treated seed, meanwhile quality parameters remained within the commercialization values accepted.Fil: Fernández, María Belén. Universidad Nacional del Centro de la Provincia de Buenos Aires. Facultad de Ingenieria Olavarria. Grupo Tecnologias de Semillas; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Tandil. Centro de Investigaciones en Física e Ingeniería del Centro de la Provincia de Buenos Aires; ArgentinaFil: Burnet, Margarita A.. Universidad Nacional del Centro de la Provincia de Buenos Aires. Facultad de Ingenieria Olavarria. Grupo Tecnologias de Semillas; ArgentinaFil: Perez, Ethel. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Bahía Blanca. Planta Piloto de Ingeniería Química (i); ArgentinaFil: Crapiste, Guillermo Hector. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Bahía Blanca. Planta Piloto de Ingeniería Química (i); ArgentinaFil: Nolasco, Susana Maria. Universidad Nacional del Centro de la Provincia de Buenos Aires. Facultad de Ingenieria Olavarria. Grupo Tecnologias de Semillas; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Tandil. Centro de Investigaciones en Física e Ingeniería del Centro de la Provincia de Buenos Aires; ArgentinaWiley2014-03info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/4677Fernández, María Belén; Burnet, Margarita A.; Perez, Ethel; Crapiste, Guillermo Hector; Nolasco, Susana Maria; Taguchi's Methodology for Determining Optimum Operating Conditions in Hydrothermal Pretreatments Applied to Canola Seeds; Wiley; The Canadian Journal Of Chemical Engineering; 92; 7; 3-2014; 1239-12460008-4034enginfo:eu-repo/semantics/altIdentifier/url/http://onlinelibrary.wiley.com/doi/10.1002/cjce.21995/abstractinfo:eu-repo/semantics/altIdentifier/doi/10.1002/cjce.21995info:eu-repo/semantics/altIdentifier/issn/0008-4034info:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-sa/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-09-03T10:10:21Zoai:ri.conicet.gov.ar:11336/4677instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-09-03 10:10:21.802CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Taguchi's Methodology for Determining Optimum Operating Conditions in Hydrothermal Pretreatments Applied to Canola Seeds
title Taguchi's Methodology for Determining Optimum Operating Conditions in Hydrothermal Pretreatments Applied to Canola Seeds
spellingShingle Taguchi's Methodology for Determining Optimum Operating Conditions in Hydrothermal Pretreatments Applied to Canola Seeds
Fernández, María Belén
Taguchi'S Methodology
Hydrothermal Pretreatment
Canola
Oil Yield And Quality
title_short Taguchi's Methodology for Determining Optimum Operating Conditions in Hydrothermal Pretreatments Applied to Canola Seeds
title_full Taguchi's Methodology for Determining Optimum Operating Conditions in Hydrothermal Pretreatments Applied to Canola Seeds
title_fullStr Taguchi's Methodology for Determining Optimum Operating Conditions in Hydrothermal Pretreatments Applied to Canola Seeds
title_full_unstemmed Taguchi's Methodology for Determining Optimum Operating Conditions in Hydrothermal Pretreatments Applied to Canola Seeds
title_sort Taguchi's Methodology for Determining Optimum Operating Conditions in Hydrothermal Pretreatments Applied to Canola Seeds
dc.creator.none.fl_str_mv Fernández, María Belén
Burnet, Margarita A.
Perez, Ethel
Crapiste, Guillermo Hector
Nolasco, Susana Maria
author Fernández, María Belén
author_facet Fernández, María Belén
Burnet, Margarita A.
Perez, Ethel
Crapiste, Guillermo Hector
Nolasco, Susana Maria
author_role author
author2 Burnet, Margarita A.
Perez, Ethel
Crapiste, Guillermo Hector
Nolasco, Susana Maria
author2_role author
author
author
author
dc.subject.none.fl_str_mv Taguchi'S Methodology
Hydrothermal Pretreatment
Canola
Oil Yield And Quality
topic Taguchi'S Methodology
Hydrothermal Pretreatment
Canola
Oil Yield And Quality
purl_subject.fl_str_mv https://purl.org/becyt/ford/2.4
https://purl.org/becyt/ford/2
dc.description.none.fl_txt_mv The aim of the present work was to determine the operational optimum conditions in hydrothermal pretreatments applied to canola seeds. The effect of these pretreatments on the canola oil extraction yield and quality was evaluated. Sample was characterized by proximal analysis. As determinations of oil quality, acidity and peroxide value, tocopherol content and acidic composition were studied. Seeds were exposed to direct vapor in an autoclave. Pretreatments were carried out using different condition of temperature (100, 120 and 130°C), exposition time (5, 15 y 30 min) and seed granulometry (milled seeds, with a particle size in a range from 0.420 mm to 1.000 mm; broken seeds, with a particle size ranging from 1.000 mm to 1.410 mm and entire seeds). After each hydrothermal pretreatment, oil extraction yield was obtained with the Soxhlet method (hexane). The Taguchi methodology was followed in order to explore the operational optimum conditions selecting the most favorable levels of each variable, using an L9 experimental design. Initial oil content was 44.2 % dry basis (db). The best values of oil yield and quality were obtained when a temperature of 120°C, a time of 5 min and broken seeds were used. The optimum experiment generated an oil yield increment of 25% respect to the not hydrothermally-treated seed, meanwhile quality parameters remained within the commercialization values accepted.
Fil: Fernández, María Belén. Universidad Nacional del Centro de la Provincia de Buenos Aires. Facultad de Ingenieria Olavarria. Grupo Tecnologias de Semillas; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Tandil. Centro de Investigaciones en Física e Ingeniería del Centro de la Provincia de Buenos Aires; Argentina
Fil: Burnet, Margarita A.. Universidad Nacional del Centro de la Provincia de Buenos Aires. Facultad de Ingenieria Olavarria. Grupo Tecnologias de Semillas; Argentina
Fil: Perez, Ethel. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Bahía Blanca. Planta Piloto de Ingeniería Química (i); Argentina
Fil: Crapiste, Guillermo Hector. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Bahía Blanca. Planta Piloto de Ingeniería Química (i); Argentina
Fil: Nolasco, Susana Maria. Universidad Nacional del Centro de la Provincia de Buenos Aires. Facultad de Ingenieria Olavarria. Grupo Tecnologias de Semillas; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Tandil. Centro de Investigaciones en Física e Ingeniería del Centro de la Provincia de Buenos Aires; Argentina
description The aim of the present work was to determine the operational optimum conditions in hydrothermal pretreatments applied to canola seeds. The effect of these pretreatments on the canola oil extraction yield and quality was evaluated. Sample was characterized by proximal analysis. As determinations of oil quality, acidity and peroxide value, tocopherol content and acidic composition were studied. Seeds were exposed to direct vapor in an autoclave. Pretreatments were carried out using different condition of temperature (100, 120 and 130°C), exposition time (5, 15 y 30 min) and seed granulometry (milled seeds, with a particle size in a range from 0.420 mm to 1.000 mm; broken seeds, with a particle size ranging from 1.000 mm to 1.410 mm and entire seeds). After each hydrothermal pretreatment, oil extraction yield was obtained with the Soxhlet method (hexane). The Taguchi methodology was followed in order to explore the operational optimum conditions selecting the most favorable levels of each variable, using an L9 experimental design. Initial oil content was 44.2 % dry basis (db). The best values of oil yield and quality were obtained when a temperature of 120°C, a time of 5 min and broken seeds were used. The optimum experiment generated an oil yield increment of 25% respect to the not hydrothermally-treated seed, meanwhile quality parameters remained within the commercialization values accepted.
publishDate 2014
dc.date.none.fl_str_mv 2014-03
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/4677
Fernández, María Belén; Burnet, Margarita A.; Perez, Ethel; Crapiste, Guillermo Hector; Nolasco, Susana Maria; Taguchi's Methodology for Determining Optimum Operating Conditions in Hydrothermal Pretreatments Applied to Canola Seeds; Wiley; The Canadian Journal Of Chemical Engineering; 92; 7; 3-2014; 1239-1246
0008-4034
url http://hdl.handle.net/11336/4677
identifier_str_mv Fernández, María Belén; Burnet, Margarita A.; Perez, Ethel; Crapiste, Guillermo Hector; Nolasco, Susana Maria; Taguchi's Methodology for Determining Optimum Operating Conditions in Hydrothermal Pretreatments Applied to Canola Seeds; Wiley; The Canadian Journal Of Chemical Engineering; 92; 7; 3-2014; 1239-1246
0008-4034
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/url/http://onlinelibrary.wiley.com/doi/10.1002/cjce.21995/abstract
info:eu-repo/semantics/altIdentifier/doi/10.1002/cjce.21995
info:eu-repo/semantics/altIdentifier/issn/0008-4034
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
application/pdf
application/pdf
dc.publisher.none.fl_str_mv Wiley
publisher.none.fl_str_mv Wiley
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
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