Simple synthesis of gold-decorated silica nanoparticles by in situ precipitation method with new plasmonic properties

Autores
Félix, Lizbet León; Martinez Porcel, Joaquin Emiliano; Herrera Aragón, Fermín Fidel; Pacheco Salazar, David Gregorio; Sousa, Marcelo Henrique
Año de publicación
2021
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
We describe a simple method for the preparation of gold-decorated silica (SiO2) nanoparticles (NPs) by the in situ precipitation method using simple BH4− ions reduction as a procedure, where BH4− ions are adsorbed onto PEI-functionalized SiO2 NPs for stabilizing and reducing gold ions onto PEI-SiO2 surface in water under ambient conditions. The result was 3-nm gold nanoshell NPs attached to SiO2 core (~ 75 nm) with a surface plasmon resonance (SPR) at ~ 680 nm. SPR band is associated with Au NP aggregates that arise from strong interparticle interaction. This is an alternative to the gold-seeding methods and the use of anionic gold species for the obtention of gold-decorated SiO2 NPs with an important red-shift in UV–Vis absorption and with potential applications in biosensors and photothermal therapy.
Fil: Félix, Lizbet León. Universidad Nacional de San Agustin de Arequipa; Perú
Fil: Martinez Porcel, Joaquin Emiliano. Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Ciudad Universitaria. Instituto de Química, Física de los Materiales, Medioambiente y Energía. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales. Instituto de Química, Física de los Materiales, Medioambiente y Energía; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Ciudad Universitaria. Instituto de Química, Física de los Materiales, Medioambiente y Energía. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales. Instituto de Química, Física de los Materiales, Medioambiente y Energía; Argentina
Fil: Herrera Aragón, Fermín Fidel. Universidad Nacional de San Agustin de Arequipa; Perú
Fil: Pacheco Salazar, David Gregorio. Universidad Nacional de San Agustin de Arequipa; Perú
Fil: Sousa, Marcelo Henrique. Universidade do Brasília; Brasil
Materia
DECORATED
GOLD
PEI-COATED SILICA
PLASMONIC
POLYETHYLENEIMINE
RED-SHIFT
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/176993
Acceder
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oai_identifier_str oai:ri.conicet.gov.ar:11336/176993
network_acronym_str CONICETDig
repository_id_str 3498
network_name_str CONICET Digital (CONICET)
spelling Simple synthesis of gold-decorated silica nanoparticles by in situ precipitation method with new plasmonic propertiesFélix, Lizbet LeónMartinez Porcel, Joaquin EmilianoHerrera Aragón, Fermín FidelPacheco Salazar, David GregorioSousa, Marcelo HenriqueDECORATEDGOLDPEI-COATED SILICAPLASMONICPOLYETHYLENEIMINERED-SHIFThttps://purl.org/becyt/ford/2.10https://purl.org/becyt/ford/2We describe a simple method for the preparation of gold-decorated silica (SiO2) nanoparticles (NPs) by the in situ precipitation method using simple BH4− ions reduction as a procedure, where BH4− ions are adsorbed onto PEI-functionalized SiO2 NPs for stabilizing and reducing gold ions onto PEI-SiO2 surface in water under ambient conditions. The result was 3-nm gold nanoshell NPs attached to SiO2 core (~ 75 nm) with a surface plasmon resonance (SPR) at ~ 680 nm. SPR band is associated with Au NP aggregates that arise from strong interparticle interaction. This is an alternative to the gold-seeding methods and the use of anionic gold species for the obtention of gold-decorated SiO2 NPs with an important red-shift in UV–Vis absorption and with potential applications in biosensors and photothermal therapy.Fil: Félix, Lizbet León. Universidad Nacional de San Agustin de Arequipa; PerúFil: Martinez Porcel, Joaquin Emiliano. Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Ciudad Universitaria. Instituto de Química, Física de los Materiales, Medioambiente y Energía. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales. Instituto de Química, Física de los Materiales, Medioambiente y Energía; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Ciudad Universitaria. Instituto de Química, Física de los Materiales, Medioambiente y Energía. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales. Instituto de Química, Física de los Materiales, Medioambiente y Energía; ArgentinaFil: Herrera Aragón, Fermín Fidel. Universidad Nacional de San Agustin de Arequipa; PerúFil: Pacheco Salazar, David Gregorio. Universidad Nacional de San Agustin de Arequipa; PerúFil: Sousa, Marcelo Henrique. Universidade do Brasília; BrasilSpringer2021-04info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/176993Félix, Lizbet León; Martinez Porcel, Joaquin Emiliano; Herrera Aragón, Fermín Fidel; Pacheco Salazar, David Gregorio; Sousa, Marcelo Henrique; Simple synthesis of gold-decorated silica nanoparticles by in situ precipitation method with new plasmonic properties; Springer; SN Applied Sciences; 3; 4; 4-2021; 1-102523-3971CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/doi/10.1007/s42452-021-04456-0info:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-sa/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-09-03T09:50:41Zoai:ri.conicet.gov.ar:11336/176993instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-09-03 09:50:41.611CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Simple synthesis of gold-decorated silica nanoparticles by in situ precipitation method with new plasmonic properties
title Simple synthesis of gold-decorated silica nanoparticles by in situ precipitation method with new plasmonic properties
spellingShingle Simple synthesis of gold-decorated silica nanoparticles by in situ precipitation method with new plasmonic properties
Félix, Lizbet León
DECORATED
GOLD
PEI-COATED SILICA
PLASMONIC
POLYETHYLENEIMINE
RED-SHIFT
title_short Simple synthesis of gold-decorated silica nanoparticles by in situ precipitation method with new plasmonic properties
title_full Simple synthesis of gold-decorated silica nanoparticles by in situ precipitation method with new plasmonic properties
title_fullStr Simple synthesis of gold-decorated silica nanoparticles by in situ precipitation method with new plasmonic properties
title_full_unstemmed Simple synthesis of gold-decorated silica nanoparticles by in situ precipitation method with new plasmonic properties
title_sort Simple synthesis of gold-decorated silica nanoparticles by in situ precipitation method with new plasmonic properties
dc.creator.none.fl_str_mv Félix, Lizbet León
Martinez Porcel, Joaquin Emiliano
Herrera Aragón, Fermín Fidel
Pacheco Salazar, David Gregorio
Sousa, Marcelo Henrique
author Félix, Lizbet León
author_facet Félix, Lizbet León
Martinez Porcel, Joaquin Emiliano
Herrera Aragón, Fermín Fidel
Pacheco Salazar, David Gregorio
Sousa, Marcelo Henrique
author_role author
author2 Martinez Porcel, Joaquin Emiliano
Herrera Aragón, Fermín Fidel
Pacheco Salazar, David Gregorio
Sousa, Marcelo Henrique
author2_role author
author
author
author
dc.subject.none.fl_str_mv DECORATED
GOLD
PEI-COATED SILICA
PLASMONIC
POLYETHYLENEIMINE
RED-SHIFT
topic DECORATED
GOLD
PEI-COATED SILICA
PLASMONIC
POLYETHYLENEIMINE
RED-SHIFT
purl_subject.fl_str_mv https://purl.org/becyt/ford/2.10
https://purl.org/becyt/ford/2
dc.description.none.fl_txt_mv We describe a simple method for the preparation of gold-decorated silica (SiO2) nanoparticles (NPs) by the in situ precipitation method using simple BH4− ions reduction as a procedure, where BH4− ions are adsorbed onto PEI-functionalized SiO2 NPs for stabilizing and reducing gold ions onto PEI-SiO2 surface in water under ambient conditions. The result was 3-nm gold nanoshell NPs attached to SiO2 core (~ 75 nm) with a surface plasmon resonance (SPR) at ~ 680 nm. SPR band is associated with Au NP aggregates that arise from strong interparticle interaction. This is an alternative to the gold-seeding methods and the use of anionic gold species for the obtention of gold-decorated SiO2 NPs with an important red-shift in UV–Vis absorption and with potential applications in biosensors and photothermal therapy.
Fil: Félix, Lizbet León. Universidad Nacional de San Agustin de Arequipa; Perú
Fil: Martinez Porcel, Joaquin Emiliano. Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Ciudad Universitaria. Instituto de Química, Física de los Materiales, Medioambiente y Energía. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales. Instituto de Química, Física de los Materiales, Medioambiente y Energía; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Ciudad Universitaria. Instituto de Química, Física de los Materiales, Medioambiente y Energía. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales. Instituto de Química, Física de los Materiales, Medioambiente y Energía; Argentina
Fil: Herrera Aragón, Fermín Fidel. Universidad Nacional de San Agustin de Arequipa; Perú
Fil: Pacheco Salazar, David Gregorio. Universidad Nacional de San Agustin de Arequipa; Perú
Fil: Sousa, Marcelo Henrique. Universidade do Brasília; Brasil
description We describe a simple method for the preparation of gold-decorated silica (SiO2) nanoparticles (NPs) by the in situ precipitation method using simple BH4− ions reduction as a procedure, where BH4− ions are adsorbed onto PEI-functionalized SiO2 NPs for stabilizing and reducing gold ions onto PEI-SiO2 surface in water under ambient conditions. The result was 3-nm gold nanoshell NPs attached to SiO2 core (~ 75 nm) with a surface plasmon resonance (SPR) at ~ 680 nm. SPR band is associated with Au NP aggregates that arise from strong interparticle interaction. This is an alternative to the gold-seeding methods and the use of anionic gold species for the obtention of gold-decorated SiO2 NPs with an important red-shift in UV–Vis absorption and with potential applications in biosensors and photothermal therapy.
publishDate 2021
dc.date.none.fl_str_mv 2021-04
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/176993
Félix, Lizbet León; Martinez Porcel, Joaquin Emiliano; Herrera Aragón, Fermín Fidel; Pacheco Salazar, David Gregorio; Sousa, Marcelo Henrique; Simple synthesis of gold-decorated silica nanoparticles by in situ precipitation method with new plasmonic properties; Springer; SN Applied Sciences; 3; 4; 4-2021; 1-10
2523-3971
CONICET Digital
CONICET
url http://hdl.handle.net/11336/176993
identifier_str_mv Félix, Lizbet León; Martinez Porcel, Joaquin Emiliano; Herrera Aragón, Fermín Fidel; Pacheco Salazar, David Gregorio; Sousa, Marcelo Henrique; Simple synthesis of gold-decorated silica nanoparticles by in situ precipitation method with new plasmonic properties; Springer; SN Applied Sciences; 3; 4; 4-2021; 1-10
2523-3971
CONICET Digital
CONICET
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/doi/10.1007/s42452-021-04456-0
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
dc.publisher.none.fl_str_mv Springer
publisher.none.fl_str_mv Springer
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
_version_ 1842269047433986048
score 13.13397

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