Evaluation of the mechanical damage on wheat starch granules by SEM, ESEM, AFM and texture image analysis

Autores
Barrera, Gabriela; Calderón Domínguez, Georgina; Chanona Pérez, Jorge; Gutiérrez López, Gustavo F.; Leon, Alberto Edel; Ribotta, Pablo Daniel
Año de publicación
2013
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
The effect of mechanical damage on wheat starch granules surface, at a microstructural level, was investigated by scanning electron microscopy (SEM), environmental scanning electron microscopy (ESEM), atomic force microscopy (AFM), and image textural analysis. The SEM and ESEM images of the native sample showed that the starch granules had smooth, flat surfaces and smooth edges. The samples with higher damaged starch content exhibited granular distortion, irregularity and less uniformity. The fractal dimension of contour parameter increased with mechanical damage, indicating thatthe surface irregularities quantitatively increased due to the damage. The surfaces of damaged granules showed depressions of different shapes and sizes. The roughness parameters and fractal dimension of the surface increased as a result of the mechanical damage. The surface of damaged granules showed higher entropy and lower homogeneity values when damaged starch increased. The results indicated that the mechanical process caused structural modifications at nano level.
Fil: Barrera, Gabriela. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Instituto de Ciencia y Tecnología de Alimentos Córdoba. Universidad Nacional de Córdoba. Facultad de Ciencias Químicas. Instituto de Ciencia y Tecnología de Alimentos Córdoba; Argentina
Fil: Calderón Domínguez, Georgina. Instituto Politécnico Nacional. Escuela Nacional de Ciencias Biológicas; México
Fil: Chanona Pérez, Jorge. Instituto Politécnico Nacional. Escuela Nacional de Ciencias Biológicas; México
Fil: Gutiérrez López, Gustavo F.. Instituto Politécnico Nacional. Escuela Nacional de Ciencias Biológicas; México
Fil: Leon, Alberto Edel. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Instituto de Ciencia y Tecnología de Alimentos Córdoba. Universidad Nacional de Córdoba. Facultad de Ciencias Químicas. Instituto de Ciencia y Tecnología de Alimentos Córdoba; Argentina
Fil: Ribotta, Pablo Daniel. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Instituto de Ciencia y Tecnología de Alimentos Córdoba. Universidad Nacional de Córdoba. Facultad de Ciencias Químicas. Instituto de Ciencia y Tecnología de Alimentos Córdoba; Argentina. Universidad Nacional de Córdoba. Secretaría de Ciencia y Tecnología. Instituto Superior de Investigación, Desarrollo y Servicio de Alimentos; Argentina
Materia
Damaged Starch
Sem
Esem
Afm
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/25187
Acceder
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oai_identifier_str oai:ri.conicet.gov.ar:11336/25187
network_acronym_str CONICETDig
repository_id_str 3498
network_name_str CONICET Digital (CONICET)
spelling Evaluation of the mechanical damage on wheat starch granules by SEM, ESEM, AFM and texture image analysisBarrera, GabrielaCalderón Domínguez, GeorginaChanona Pérez, JorgeGutiérrez López, Gustavo F.Leon, Alberto EdelRibotta, Pablo DanielDamaged StarchSemEsemAfmhttps://purl.org/becyt/ford/2.11https://purl.org/becyt/ford/2The effect of mechanical damage on wheat starch granules surface, at a microstructural level, was investigated by scanning electron microscopy (SEM), environmental scanning electron microscopy (ESEM), atomic force microscopy (AFM), and image textural analysis. The SEM and ESEM images of the native sample showed that the starch granules had smooth, flat surfaces and smooth edges. The samples with higher damaged starch content exhibited granular distortion, irregularity and less uniformity. The fractal dimension of contour parameter increased with mechanical damage, indicating thatthe surface irregularities quantitatively increased due to the damage. The surfaces of damaged granules showed depressions of different shapes and sizes. The roughness parameters and fractal dimension of the surface increased as a result of the mechanical damage. The surface of damaged granules showed higher entropy and lower homogeneity values when damaged starch increased. The results indicated that the mechanical process caused structural modifications at nano level.Fil: Barrera, Gabriela. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Instituto de Ciencia y Tecnología de Alimentos Córdoba. Universidad Nacional de Córdoba. Facultad de Ciencias Químicas. Instituto de Ciencia y Tecnología de Alimentos Córdoba; ArgentinaFil: Calderón Domínguez, Georgina. Instituto Politécnico Nacional. Escuela Nacional de Ciencias Biológicas; MéxicoFil: Chanona Pérez, Jorge. Instituto Politécnico Nacional. Escuela Nacional de Ciencias Biológicas; MéxicoFil: Gutiérrez López, Gustavo F.. Instituto Politécnico Nacional. Escuela Nacional de Ciencias Biológicas; MéxicoFil: Leon, Alberto Edel. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Instituto de Ciencia y Tecnología de Alimentos Córdoba. Universidad Nacional de Córdoba. Facultad de Ciencias Químicas. Instituto de Ciencia y Tecnología de Alimentos Córdoba; ArgentinaFil: Ribotta, Pablo Daniel. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Instituto de Ciencia y Tecnología de Alimentos Córdoba. Universidad Nacional de Córdoba. Facultad de Ciencias Químicas. Instituto de Ciencia y Tecnología de Alimentos Córdoba; Argentina. Universidad Nacional de Córdoba. Secretaría de Ciencia y Tecnología. Instituto Superior de Investigación, Desarrollo y Servicio de Alimentos; ArgentinaElsevier2013-08info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfapplication/pdfapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/25187Barrera, Gabriela; Calderón Domínguez, Georgina; Chanona Pérez, Jorge; Gutiérrez López, Gustavo F.; Leon, Alberto Edel; et al.; Evaluation of the mechanical damage on wheat starch granules by SEM, ESEM, AFM and texture image analysis; Elsevier; Carbohydrate Polymers; 98; 2; 8-2013; 1449-14570144-8617CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/doi/10.1016/j.carbpol.2013.07.056info:eu-repo/semantics/altIdentifier/url/http://www.sciencedirect.com/science/article/pii/S014486171300742Xinfo:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-nd/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-09-29T09:42:47Zoai:ri.conicet.gov.ar:11336/25187instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-09-29 09:42:47.685CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Evaluation of the mechanical damage on wheat starch granules by SEM, ESEM, AFM and texture image analysis
title Evaluation of the mechanical damage on wheat starch granules by SEM, ESEM, AFM and texture image analysis
spellingShingle Evaluation of the mechanical damage on wheat starch granules by SEM, ESEM, AFM and texture image analysis
Barrera, Gabriela
Damaged Starch
Sem
Esem
Afm
title_short Evaluation of the mechanical damage on wheat starch granules by SEM, ESEM, AFM and texture image analysis
title_full Evaluation of the mechanical damage on wheat starch granules by SEM, ESEM, AFM and texture image analysis
title_fullStr Evaluation of the mechanical damage on wheat starch granules by SEM, ESEM, AFM and texture image analysis
title_full_unstemmed Evaluation of the mechanical damage on wheat starch granules by SEM, ESEM, AFM and texture image analysis
title_sort Evaluation of the mechanical damage on wheat starch granules by SEM, ESEM, AFM and texture image analysis
dc.creator.none.fl_str_mv Barrera, Gabriela
Calderón Domínguez, Georgina
Chanona Pérez, Jorge
Gutiérrez López, Gustavo F.
Leon, Alberto Edel
Ribotta, Pablo Daniel
author Barrera, Gabriela
author_facet Barrera, Gabriela
Calderón Domínguez, Georgina
Chanona Pérez, Jorge
Gutiérrez López, Gustavo F.
Leon, Alberto Edel
Ribotta, Pablo Daniel
author_role author
author2 Calderón Domínguez, Georgina
Chanona Pérez, Jorge
Gutiérrez López, Gustavo F.
Leon, Alberto Edel
Ribotta, Pablo Daniel
author2_role author
author
author
author
author
dc.subject.none.fl_str_mv Damaged Starch
Sem
Esem
Afm
topic Damaged Starch
Sem
Esem
Afm
purl_subject.fl_str_mv https://purl.org/becyt/ford/2.11
https://purl.org/becyt/ford/2
dc.description.none.fl_txt_mv The effect of mechanical damage on wheat starch granules surface, at a microstructural level, was investigated by scanning electron microscopy (SEM), environmental scanning electron microscopy (ESEM), atomic force microscopy (AFM), and image textural analysis. The SEM and ESEM images of the native sample showed that the starch granules had smooth, flat surfaces and smooth edges. The samples with higher damaged starch content exhibited granular distortion, irregularity and less uniformity. The fractal dimension of contour parameter increased with mechanical damage, indicating thatthe surface irregularities quantitatively increased due to the damage. The surfaces of damaged granules showed depressions of different shapes and sizes. The roughness parameters and fractal dimension of the surface increased as a result of the mechanical damage. The surface of damaged granules showed higher entropy and lower homogeneity values when damaged starch increased. The results indicated that the mechanical process caused structural modifications at nano level.
Fil: Barrera, Gabriela. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Instituto de Ciencia y Tecnología de Alimentos Córdoba. Universidad Nacional de Córdoba. Facultad de Ciencias Químicas. Instituto de Ciencia y Tecnología de Alimentos Córdoba; Argentina
Fil: Calderón Domínguez, Georgina. Instituto Politécnico Nacional. Escuela Nacional de Ciencias Biológicas; México
Fil: Chanona Pérez, Jorge. Instituto Politécnico Nacional. Escuela Nacional de Ciencias Biológicas; México
Fil: Gutiérrez López, Gustavo F.. Instituto Politécnico Nacional. Escuela Nacional de Ciencias Biológicas; México
Fil: Leon, Alberto Edel. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Instituto de Ciencia y Tecnología de Alimentos Córdoba. Universidad Nacional de Córdoba. Facultad de Ciencias Químicas. Instituto de Ciencia y Tecnología de Alimentos Córdoba; Argentina
Fil: Ribotta, Pablo Daniel. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Córdoba. Instituto de Ciencia y Tecnología de Alimentos Córdoba. Universidad Nacional de Córdoba. Facultad de Ciencias Químicas. Instituto de Ciencia y Tecnología de Alimentos Córdoba; Argentina. Universidad Nacional de Córdoba. Secretaría de Ciencia y Tecnología. Instituto Superior de Investigación, Desarrollo y Servicio de Alimentos; Argentina
description The effect of mechanical damage on wheat starch granules surface, at a microstructural level, was investigated by scanning electron microscopy (SEM), environmental scanning electron microscopy (ESEM), atomic force microscopy (AFM), and image textural analysis. The SEM and ESEM images of the native sample showed that the starch granules had smooth, flat surfaces and smooth edges. The samples with higher damaged starch content exhibited granular distortion, irregularity and less uniformity. The fractal dimension of contour parameter increased with mechanical damage, indicating thatthe surface irregularities quantitatively increased due to the damage. The surfaces of damaged granules showed depressions of different shapes and sizes. The roughness parameters and fractal dimension of the surface increased as a result of the mechanical damage. The surface of damaged granules showed higher entropy and lower homogeneity values when damaged starch increased. The results indicated that the mechanical process caused structural modifications at nano level.
publishDate 2013
dc.date.none.fl_str_mv 2013-08
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/25187
Barrera, Gabriela; Calderón Domínguez, Georgina; Chanona Pérez, Jorge; Gutiérrez López, Gustavo F.; Leon, Alberto Edel; et al.; Evaluation of the mechanical damage on wheat starch granules by SEM, ESEM, AFM and texture image analysis; Elsevier; Carbohydrate Polymers; 98; 2; 8-2013; 1449-1457
0144-8617
CONICET Digital
CONICET
url http://hdl.handle.net/11336/25187
identifier_str_mv Barrera, Gabriela; Calderón Domínguez, Georgina; Chanona Pérez, Jorge; Gutiérrez López, Gustavo F.; Leon, Alberto Edel; et al.; Evaluation of the mechanical damage on wheat starch granules by SEM, ESEM, AFM and texture image analysis; Elsevier; Carbohydrate Polymers; 98; 2; 8-2013; 1449-1457
0144-8617
CONICET Digital
CONICET
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/doi/10.1016/j.carbpol.2013.07.056
info:eu-repo/semantics/altIdentifier/url/http://www.sciencedirect.com/science/article/pii/S014486171300742X
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
application/pdf
application/pdf
application/pdf
dc.publisher.none.fl_str_mv Elsevier
publisher.none.fl_str_mv Elsevier
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
_version_ 1844613347492757504
score 13.070432

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