Microstructure and corrosion behavior of AISI 316L duplex treated by means of ion nitriding and plasma based ion implantation and deposition

Autores
Escalada, Lisandro; Lutz, J.; Brühl, S.P.; Fazio, Mariana Andrea; Marquez, Adriana Beatriz; Mändl, S.; Manova, D.; Simison, Silvia Noemi
Año de publicación
2013
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
Austenitic stainless steels are the preferred materials for mechanical components in the food, oil and chemical industries due to their good corrosion resistance but they often suffer severe wear due to their poor tribological properties. Plasma surface engineering has been extended to stainless steel hardening, through the modification of the surface with ion nitriding or the application of hard coatings. In this work, AISI 316L samples were coated with titanium nitride by means of a cathodic arc (CA) and this technique was combined with plasma immersion ion implantation, in a process called plasma based ion implantation and deposition (PBII&D). The effect on corrosion resistance was analyzed, also considering ion nitriding as a pre-treatment. Microstructure and composition were analyzed by means of glancing angle XRD, SIMS, SEM, SEM-FIB and EDS. Localized corrosion resistance was analyzed in a cyclic potentiodynamic polarization experiment in 3.5% NaCl solution, and the corroded surface was analyzed with AFM, SEM and EDS as well. It was found that nitriding at 400 °C produces a thin nitrided layer with good corrosion resistance. A duplex TiN coating resulted in a further improvement of the corrosion resistance. Comparing cathodic arc and PBII&D coating techniques, the last one gives the thickest film and also the best corrosion behavior with good adhesion.
Fil: Escalada, Lisandro. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Mar del Plata. Instituto de Investigación En Ciencia y Tecnología de Materiales (i); Argentina. Universidad Nacional de Mar del Plata. Facultad de Ingeniería; Argentina
Fil: Lutz, J.. Leibniz Institute of Surface Modification; Alemania
Fil: Brühl, S.P.. Universidad Tecnologica Nacional. Facultad Regional Concepcion del Uruguay; Argentina
Fil: Fazio, Mariana Andrea. Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinacion Administrativa Ciudad Universitaria. Instituto de Física del Plasma; Argentina
Fil: Marquez, Adriana Beatriz. Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinacion Administrativa Ciudad Universitaria. Instituto de Física del Plasma; Argentina
Fil: Mändl, S.. Leibniz Institute of Surface Modification; Alemania
Fil: Manova, D.. Leibniz Institute of Surface Modification; Alemania
Fil: Simison, Silvia Noemi. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Mar del Plata. Instituto de Investigación En Ciencia y Tecnología de Materiales (i); Argentina. Universidad Nacional de Mar del Plata. Facultad de Ingeniería; Argentina
Materia
Plasma Nitriding
Tin Coating
Plasma Ion Implantation
Corrosion Resistance
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/4615
Acceder
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oai_identifier_str oai:ri.conicet.gov.ar:11336/4615
network_acronym_str CONICETDig
repository_id_str 3498
network_name_str CONICET Digital (CONICET)
spelling Microstructure and corrosion behavior of AISI 316L duplex treated by means of ion nitriding and plasma based ion implantation and depositionEscalada, LisandroLutz, J.Brühl, S.P.Fazio, Mariana AndreaMarquez, Adriana BeatrizMändl, S.Manova, D.Simison, Silvia NoemiPlasma NitridingTin CoatingPlasma Ion ImplantationCorrosion Resistancehttps://purl.org/becyt/ford/2.5https://purl.org/becyt/ford/2https://purl.org/becyt/ford/1.4https://purl.org/becyt/ford/1Austenitic stainless steels are the preferred materials for mechanical components in the food, oil and chemical industries due to their good corrosion resistance but they often suffer severe wear due to their poor tribological properties. Plasma surface engineering has been extended to stainless steel hardening, through the modification of the surface with ion nitriding or the application of hard coatings. In this work, AISI 316L samples were coated with titanium nitride by means of a cathodic arc (CA) and this technique was combined with plasma immersion ion implantation, in a process called plasma based ion implantation and deposition (PBII&D). The effect on corrosion resistance was analyzed, also considering ion nitriding as a pre-treatment. Microstructure and composition were analyzed by means of glancing angle XRD, SIMS, SEM, SEM-FIB and EDS. Localized corrosion resistance was analyzed in a cyclic potentiodynamic polarization experiment in 3.5% NaCl solution, and the corroded surface was analyzed with AFM, SEM and EDS as well. It was found that nitriding at 400 °C produces a thin nitrided layer with good corrosion resistance. A duplex TiN coating resulted in a further improvement of the corrosion resistance. Comparing cathodic arc and PBII&D coating techniques, the last one gives the thickest film and also the best corrosion behavior with good adhesion.Fil: Escalada, Lisandro. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Mar del Plata. Instituto de Investigación En Ciencia y Tecnología de Materiales (i); Argentina. Universidad Nacional de Mar del Plata. Facultad de Ingeniería; ArgentinaFil: Lutz, J.. Leibniz Institute of Surface Modification; AlemaniaFil: Brühl, S.P.. Universidad Tecnologica Nacional. Facultad Regional Concepcion del Uruguay; ArgentinaFil: Fazio, Mariana Andrea. Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinacion Administrativa Ciudad Universitaria. Instituto de Física del Plasma; ArgentinaFil: Marquez, Adriana Beatriz. Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinacion Administrativa Ciudad Universitaria. Instituto de Física del Plasma; ArgentinaFil: Mändl, S.. Leibniz Institute of Surface Modification; AlemaniaFil: Manova, D.. Leibniz Institute of Surface Modification; AlemaniaFil: Simison, Silvia Noemi. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Mar del Plata. Instituto de Investigación En Ciencia y Tecnología de Materiales (i); Argentina. Universidad Nacional de Mar del Plata. Facultad de Ingeniería; ArgentinaElsevier2013-03-05info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfapplication/pdfapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/4615Escalada, Lisandro; Lutz, J.; Brühl, S.P.; Fazio, Mariana Andrea; Marquez, Adriana Beatriz; et al.; Microstructure and corrosion behavior of AISI 316L duplex treated by means of ion nitriding and plasma based ion implantation and deposition; Elsevier; Surface and Coatings Technology; 223; 5-3-2013; 41-460257-8972enginfo:eu-repo/semantics/altIdentifier/doi/10.1016/j.surfcoat.2013.02.025info:eu-repo/semantics/altIdentifier/issn/0257-8972info:eu-repo/semantics/altIdentifier/url/http://www.sciencedirect.com/science/article/pii/S0257897213001801info:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-sa/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-09-29T09:55:38Zoai:ri.conicet.gov.ar:11336/4615instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-09-29 09:55:38.819CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Microstructure and corrosion behavior of AISI 316L duplex treated by means of ion nitriding and plasma based ion implantation and deposition
title Microstructure and corrosion behavior of AISI 316L duplex treated by means of ion nitriding and plasma based ion implantation and deposition
spellingShingle Microstructure and corrosion behavior of AISI 316L duplex treated by means of ion nitriding and plasma based ion implantation and deposition
Escalada, Lisandro
Plasma Nitriding
Tin Coating
Plasma Ion Implantation
Corrosion Resistance
title_short Microstructure and corrosion behavior of AISI 316L duplex treated by means of ion nitriding and plasma based ion implantation and deposition
title_full Microstructure and corrosion behavior of AISI 316L duplex treated by means of ion nitriding and plasma based ion implantation and deposition
title_fullStr Microstructure and corrosion behavior of AISI 316L duplex treated by means of ion nitriding and plasma based ion implantation and deposition
title_full_unstemmed Microstructure and corrosion behavior of AISI 316L duplex treated by means of ion nitriding and plasma based ion implantation and deposition
title_sort Microstructure and corrosion behavior of AISI 316L duplex treated by means of ion nitriding and plasma based ion implantation and deposition
dc.creator.none.fl_str_mv Escalada, Lisandro
Lutz, J.
Brühl, S.P.
Fazio, Mariana Andrea
Marquez, Adriana Beatriz
Mändl, S.
Manova, D.
Simison, Silvia Noemi
author Escalada, Lisandro
author_facet Escalada, Lisandro
Lutz, J.
Brühl, S.P.
Fazio, Mariana Andrea
Marquez, Adriana Beatriz
Mändl, S.
Manova, D.
Simison, Silvia Noemi
author_role author
author2 Lutz, J.
Brühl, S.P.
Fazio, Mariana Andrea
Marquez, Adriana Beatriz
Mändl, S.
Manova, D.
Simison, Silvia Noemi
author2_role author
author
author
author
author
author
author
dc.subject.none.fl_str_mv Plasma Nitriding
Tin Coating
Plasma Ion Implantation
Corrosion Resistance
topic Plasma Nitriding
Tin Coating
Plasma Ion Implantation
Corrosion Resistance
purl_subject.fl_str_mv https://purl.org/becyt/ford/2.5
https://purl.org/becyt/ford/2
https://purl.org/becyt/ford/1.4
https://purl.org/becyt/ford/1
dc.description.none.fl_txt_mv Austenitic stainless steels are the preferred materials for mechanical components in the food, oil and chemical industries due to their good corrosion resistance but they often suffer severe wear due to their poor tribological properties. Plasma surface engineering has been extended to stainless steel hardening, through the modification of the surface with ion nitriding or the application of hard coatings. In this work, AISI 316L samples were coated with titanium nitride by means of a cathodic arc (CA) and this technique was combined with plasma immersion ion implantation, in a process called plasma based ion implantation and deposition (PBII&D). The effect on corrosion resistance was analyzed, also considering ion nitriding as a pre-treatment. Microstructure and composition were analyzed by means of glancing angle XRD, SIMS, SEM, SEM-FIB and EDS. Localized corrosion resistance was analyzed in a cyclic potentiodynamic polarization experiment in 3.5% NaCl solution, and the corroded surface was analyzed with AFM, SEM and EDS as well. It was found that nitriding at 400 °C produces a thin nitrided layer with good corrosion resistance. A duplex TiN coating resulted in a further improvement of the corrosion resistance. Comparing cathodic arc and PBII&D coating techniques, the last one gives the thickest film and also the best corrosion behavior with good adhesion.
Fil: Escalada, Lisandro. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Mar del Plata. Instituto de Investigación En Ciencia y Tecnología de Materiales (i); Argentina. Universidad Nacional de Mar del Plata. Facultad de Ingeniería; Argentina
Fil: Lutz, J.. Leibniz Institute of Surface Modification; Alemania
Fil: Brühl, S.P.. Universidad Tecnologica Nacional. Facultad Regional Concepcion del Uruguay; Argentina
Fil: Fazio, Mariana Andrea. Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinacion Administrativa Ciudad Universitaria. Instituto de Física del Plasma; Argentina
Fil: Marquez, Adriana Beatriz. Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinacion Administrativa Ciudad Universitaria. Instituto de Física del Plasma; Argentina
Fil: Mändl, S.. Leibniz Institute of Surface Modification; Alemania
Fil: Manova, D.. Leibniz Institute of Surface Modification; Alemania
Fil: Simison, Silvia Noemi. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Mar del Plata. Instituto de Investigación En Ciencia y Tecnología de Materiales (i); Argentina. Universidad Nacional de Mar del Plata. Facultad de Ingeniería; Argentina
description Austenitic stainless steels are the preferred materials for mechanical components in the food, oil and chemical industries due to their good corrosion resistance but they often suffer severe wear due to their poor tribological properties. Plasma surface engineering has been extended to stainless steel hardening, through the modification of the surface with ion nitriding or the application of hard coatings. In this work, AISI 316L samples were coated with titanium nitride by means of a cathodic arc (CA) and this technique was combined with plasma immersion ion implantation, in a process called plasma based ion implantation and deposition (PBII&D). The effect on corrosion resistance was analyzed, also considering ion nitriding as a pre-treatment. Microstructure and composition were analyzed by means of glancing angle XRD, SIMS, SEM, SEM-FIB and EDS. Localized corrosion resistance was analyzed in a cyclic potentiodynamic polarization experiment in 3.5% NaCl solution, and the corroded surface was analyzed with AFM, SEM and EDS as well. It was found that nitriding at 400 °C produces a thin nitrided layer with good corrosion resistance. A duplex TiN coating resulted in a further improvement of the corrosion resistance. Comparing cathodic arc and PBII&D coating techniques, the last one gives the thickest film and also the best corrosion behavior with good adhesion.
publishDate 2013
dc.date.none.fl_str_mv 2013-03-05
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/4615
Escalada, Lisandro; Lutz, J.; Brühl, S.P.; Fazio, Mariana Andrea; Marquez, Adriana Beatriz; et al.; Microstructure and corrosion behavior of AISI 316L duplex treated by means of ion nitriding and plasma based ion implantation and deposition; Elsevier; Surface and Coatings Technology; 223; 5-3-2013; 41-46
0257-8972
url http://hdl.handle.net/11336/4615
identifier_str_mv Escalada, Lisandro; Lutz, J.; Brühl, S.P.; Fazio, Mariana Andrea; Marquez, Adriana Beatriz; et al.; Microstructure and corrosion behavior of AISI 316L duplex treated by means of ion nitriding and plasma based ion implantation and deposition; Elsevier; Surface and Coatings Technology; 223; 5-3-2013; 41-46
0257-8972
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/doi/10.1016/j.surfcoat.2013.02.025
info:eu-repo/semantics/altIdentifier/issn/0257-8972
info:eu-repo/semantics/altIdentifier/url/http://www.sciencedirect.com/science/article/pii/S0257897213001801
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
application/pdf
application/pdf
application/pdf
dc.publisher.none.fl_str_mv Elsevier
publisher.none.fl_str_mv Elsevier
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
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score 13.070432

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