Microstructural evolution during solution treatment of Co-Cr-Mo-C biocompatible alloys

Autores
Giacchi, Jessica Vanina; Fornaro, Osvaldo; Palacio, Hugo Anibal
Año de publicación
2012
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
Three different Co-Cr-Mo-C alloys conforming to ASTM F75 standard were poured inan industrial environment and subjected to a conventional solution treatment at1225 °C for several time intervals. The microstructural changes andtransformations were studied in each case in order to evaluate the way in whichtreatment time influences the secondary phase fraction and clarify themicrostructural changes that could occur. To assess how treatment time affectsmicrostructure, optical microscopy and image analyzer software, scanningelectron microscopy and energy dispersion spectrometry analysis were employed.The main phases detected in the as-cast state were: σ-phase, M6C, and M23C6carbides. The latter presented two different morphologies, blocky type andlamellar type. Despite being considered the most detrimental feature tomechanical properties, σ-phase and lamellar carbides dissolution took place inthe early stages of solution treatment. M23C6 carbides featured two differentbehaviors. In the alloy obtained by melting an appropriate quantity of alloyedcommercial materials, a decrease in size, spheroidization and transformationinto M6C carbides were simultaneously observed. In the commercial ASTM F75alloy, in turn, despite being the same phase, only a marked decrease inprecipitates size was noticed. These different behaviors could be ascribed tothe initial presence of other phases in the alloy obtained from alloyedmaterials, such as σ-phase and pearlitic carbides, or to the initialprecipitate size which was much larger in the first than in the commercial ASTMF75 alloy studied. M6C carbides dissolved directly in the matrix as they couldnot be detected in samples solution-treated for 15 min.
Fil: Giacchi, Jessica Vanina. Universidad Nacional del Centro de la Provincia de Buenos Aires. Facultad de Ciencias Exactas. Instituto de Física de Materiales; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Tandil; Argentina
Fil: Fornaro, Osvaldo. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Tandil; Argentina. Universidad Nacional del Centro de la Provincia de Buenos Aires. Facultad de Ciencias Exactas. Instituto de Física de Materiales; Argentina
Fil: Palacio, Hugo Anibal. Universidad Nacional del Centro de la Provincia de Buenos Aires. Facultad de Ciencias Exactas. Instituto de Física de Materiales; Argentina. Provincia de Buenos Aires. Gobernación. Comisión de Investigaciones Científicas; Argentina
Materia
CO-CR-MO
MICROSTRUCTURE
SOLIDIFICATION
SOLUTION TREATMENT
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/199313

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spelling Microstructural evolution during solution treatment of Co-Cr-Mo-C biocompatible alloysGiacchi, Jessica VaninaFornaro, OsvaldoPalacio, Hugo AnibalCO-CR-MOMICROSTRUCTURESOLIDIFICATIONSOLUTION TREATMENThttps://purl.org/becyt/ford/2.5https://purl.org/becyt/ford/2Three different Co-Cr-Mo-C alloys conforming to ASTM F75 standard were poured inan industrial environment and subjected to a conventional solution treatment at1225 °C for several time intervals. The microstructural changes andtransformations were studied in each case in order to evaluate the way in whichtreatment time influences the secondary phase fraction and clarify themicrostructural changes that could occur. To assess how treatment time affectsmicrostructure, optical microscopy and image analyzer software, scanningelectron microscopy and energy dispersion spectrometry analysis were employed.The main phases detected in the as-cast state were: σ-phase, M6C, and M23C6carbides. The latter presented two different morphologies, blocky type andlamellar type. Despite being considered the most detrimental feature tomechanical properties, σ-phase and lamellar carbides dissolution took place inthe early stages of solution treatment. M23C6 carbides featured two differentbehaviors. In the alloy obtained by melting an appropriate quantity of alloyedcommercial materials, a decrease in size, spheroidization and transformationinto M6C carbides were simultaneously observed. In the commercial ASTM F75alloy, in turn, despite being the same phase, only a marked decrease inprecipitates size was noticed. These different behaviors could be ascribed tothe initial presence of other phases in the alloy obtained from alloyedmaterials, such as σ-phase and pearlitic carbides, or to the initialprecipitate size which was much larger in the first than in the commercial ASTMF75 alloy studied. M6C carbides dissolved directly in the matrix as they couldnot be detected in samples solution-treated for 15 min.Fil: Giacchi, Jessica Vanina. Universidad Nacional del Centro de la Provincia de Buenos Aires. Facultad de Ciencias Exactas. Instituto de Física de Materiales; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Tandil; ArgentinaFil: Fornaro, Osvaldo. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Tandil; Argentina. Universidad Nacional del Centro de la Provincia de Buenos Aires. Facultad de Ciencias Exactas. Instituto de Física de Materiales; ArgentinaFil: Palacio, Hugo Anibal. Universidad Nacional del Centro de la Provincia de Buenos Aires. Facultad de Ciencias Exactas. Instituto de Física de Materiales; Argentina. Provincia de Buenos Aires. Gobernación. Comisión de Investigaciones Científicas; ArgentinaElsevier Science Inc.2012-06info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/199313Giacchi, Jessica Vanina; Fornaro, Osvaldo; Palacio, Hugo Anibal; Microstructural evolution during solution treatment of Co-Cr-Mo-C biocompatible alloys; Elsevier Science Inc.; Materials Characterization; 68; 6-2012; 49-571044-5803CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/url/https://www.sciencedirect.com/science/article/abs/pii/S1044580312000630?via%3Dihubinfo:eu-repo/semantics/altIdentifier/doi/10.1016/j.matchar.2012.03.006info:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-sa/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-09-29T09:40:59Zoai:ri.conicet.gov.ar:11336/199313instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-09-29 09:40:59.331CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Microstructural evolution during solution treatment of Co-Cr-Mo-C biocompatible alloys
title Microstructural evolution during solution treatment of Co-Cr-Mo-C biocompatible alloys
spellingShingle Microstructural evolution during solution treatment of Co-Cr-Mo-C biocompatible alloys
Giacchi, Jessica Vanina
CO-CR-MO
MICROSTRUCTURE
SOLIDIFICATION
SOLUTION TREATMENT
title_short Microstructural evolution during solution treatment of Co-Cr-Mo-C biocompatible alloys
title_full Microstructural evolution during solution treatment of Co-Cr-Mo-C biocompatible alloys
title_fullStr Microstructural evolution during solution treatment of Co-Cr-Mo-C biocompatible alloys
title_full_unstemmed Microstructural evolution during solution treatment of Co-Cr-Mo-C biocompatible alloys
title_sort Microstructural evolution during solution treatment of Co-Cr-Mo-C biocompatible alloys
dc.creator.none.fl_str_mv Giacchi, Jessica Vanina
Fornaro, Osvaldo
Palacio, Hugo Anibal
author Giacchi, Jessica Vanina
author_facet Giacchi, Jessica Vanina
Fornaro, Osvaldo
Palacio, Hugo Anibal
author_role author
author2 Fornaro, Osvaldo
Palacio, Hugo Anibal
author2_role author
author
dc.subject.none.fl_str_mv CO-CR-MO
MICROSTRUCTURE
SOLIDIFICATION
SOLUTION TREATMENT
topic CO-CR-MO
MICROSTRUCTURE
SOLIDIFICATION
SOLUTION TREATMENT
purl_subject.fl_str_mv https://purl.org/becyt/ford/2.5
https://purl.org/becyt/ford/2
dc.description.none.fl_txt_mv Three different Co-Cr-Mo-C alloys conforming to ASTM F75 standard were poured inan industrial environment and subjected to a conventional solution treatment at1225 °C for several time intervals. The microstructural changes andtransformations were studied in each case in order to evaluate the way in whichtreatment time influences the secondary phase fraction and clarify themicrostructural changes that could occur. To assess how treatment time affectsmicrostructure, optical microscopy and image analyzer software, scanningelectron microscopy and energy dispersion spectrometry analysis were employed.The main phases detected in the as-cast state were: σ-phase, M6C, and M23C6carbides. The latter presented two different morphologies, blocky type andlamellar type. Despite being considered the most detrimental feature tomechanical properties, σ-phase and lamellar carbides dissolution took place inthe early stages of solution treatment. M23C6 carbides featured two differentbehaviors. In the alloy obtained by melting an appropriate quantity of alloyedcommercial materials, a decrease in size, spheroidization and transformationinto M6C carbides were simultaneously observed. In the commercial ASTM F75alloy, in turn, despite being the same phase, only a marked decrease inprecipitates size was noticed. These different behaviors could be ascribed tothe initial presence of other phases in the alloy obtained from alloyedmaterials, such as σ-phase and pearlitic carbides, or to the initialprecipitate size which was much larger in the first than in the commercial ASTMF75 alloy studied. M6C carbides dissolved directly in the matrix as they couldnot be detected in samples solution-treated for 15 min.
Fil: Giacchi, Jessica Vanina. Universidad Nacional del Centro de la Provincia de Buenos Aires. Facultad de Ciencias Exactas. Instituto de Física de Materiales; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Tandil; Argentina
Fil: Fornaro, Osvaldo. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Tandil; Argentina. Universidad Nacional del Centro de la Provincia de Buenos Aires. Facultad de Ciencias Exactas. Instituto de Física de Materiales; Argentina
Fil: Palacio, Hugo Anibal. Universidad Nacional del Centro de la Provincia de Buenos Aires. Facultad de Ciencias Exactas. Instituto de Física de Materiales; Argentina. Provincia de Buenos Aires. Gobernación. Comisión de Investigaciones Científicas; Argentina
description Three different Co-Cr-Mo-C alloys conforming to ASTM F75 standard were poured inan industrial environment and subjected to a conventional solution treatment at1225 °C for several time intervals. The microstructural changes andtransformations were studied in each case in order to evaluate the way in whichtreatment time influences the secondary phase fraction and clarify themicrostructural changes that could occur. To assess how treatment time affectsmicrostructure, optical microscopy and image analyzer software, scanningelectron microscopy and energy dispersion spectrometry analysis were employed.The main phases detected in the as-cast state were: σ-phase, M6C, and M23C6carbides. The latter presented two different morphologies, blocky type andlamellar type. Despite being considered the most detrimental feature tomechanical properties, σ-phase and lamellar carbides dissolution took place inthe early stages of solution treatment. M23C6 carbides featured two differentbehaviors. In the alloy obtained by melting an appropriate quantity of alloyedcommercial materials, a decrease in size, spheroidization and transformationinto M6C carbides were simultaneously observed. In the commercial ASTM F75alloy, in turn, despite being the same phase, only a marked decrease inprecipitates size was noticed. These different behaviors could be ascribed tothe initial presence of other phases in the alloy obtained from alloyedmaterials, such as σ-phase and pearlitic carbides, or to the initialprecipitate size which was much larger in the first than in the commercial ASTMF75 alloy studied. M6C carbides dissolved directly in the matrix as they couldnot be detected in samples solution-treated for 15 min.
publishDate 2012
dc.date.none.fl_str_mv 2012-06
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/199313
Giacchi, Jessica Vanina; Fornaro, Osvaldo; Palacio, Hugo Anibal; Microstructural evolution during solution treatment of Co-Cr-Mo-C biocompatible alloys; Elsevier Science Inc.; Materials Characterization; 68; 6-2012; 49-57
1044-5803
CONICET Digital
CONICET
url http://hdl.handle.net/11336/199313
identifier_str_mv Giacchi, Jessica Vanina; Fornaro, Osvaldo; Palacio, Hugo Anibal; Microstructural evolution during solution treatment of Co-Cr-Mo-C biocompatible alloys; Elsevier Science Inc.; Materials Characterization; 68; 6-2012; 49-57
1044-5803
CONICET Digital
CONICET
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/url/https://www.sciencedirect.com/science/article/abs/pii/S1044580312000630?via%3Dihub
info:eu-repo/semantics/altIdentifier/doi/10.1016/j.matchar.2012.03.006
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
dc.publisher.none.fl_str_mv Elsevier Science Inc.
publisher.none.fl_str_mv Elsevier Science Inc.
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
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instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
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repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
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