Purification and functionalization of carbon nanotubes by classical and advanced oxidation processes

Autores
Escobar, Mariano Martin; Goyanes, Silvia Nair; Corcuera, M. A.; Eceiza, A.; Mondragon, I.; Rubiolo, Gerardo Hector; Candal, Roberto Jorge
Año de publicación
2009
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
Advanced oxidation technologies (AOT) were applied for the production of accurately controlled oxidized multi-walled carbon nanotubes. Fenton process is effective to get carboxylic (-COO - or -COOH) and OH groups on the surface of carbon nanotubes while Photofenton and UV/H 2O 2 processes mostly produce OH groups on surface of multiwalled carbon nanotubes (MWCNT). All of them preserve the structure of MWCNT allowing to achieve accurately controlled oxidized MWCNT. Fourier transform infrared spectroscopy (FTIR) and thermogravimetical analysis (TGA) show that the acid treatment is the more efficient technique to generate COOH groups on MWCNT surface. However, this chemical technique generates strong damages on the MWCNT structure, as demonstrated by TGA, field emission scanning electron microscopy and transmission electron microscopy results. Copyright © 2009 American Scientific Publishers.
Fil: Escobar, Mariano Martin. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina. Universidad de Buenos Aires; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Ciudad Universitaria. Instituto de Física de Buenos Aires. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales. Instituto de Física de Buenos Aires; Argentina
Fil: Goyanes, Silvia Nair. Universidad de Buenos Aires; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Ciudad Universitaria. Instituto de Física de Buenos Aires. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales. Instituto de Física de Buenos Aires; Argentina
Fil: Corcuera, M. A.. Universidad del País Vasco; España
Fil: Eceiza, A.. Universidad del País Vasco; España
Fil: Mondragon, I.. Universidad del País Vasco; España
Fil: Rubiolo, Gerardo Hector. Comisión Nacional de Energía Atómica; Argentina. Universidad de Buenos Aires; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Ciudad Universitaria. Instituto de Física de Buenos Aires. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales. Instituto de Física de Buenos Aires; Argentina
Fil: Candal, Roberto Jorge. Universidad Nacional de San Martín; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina
Materia
Carbon Nanotubes
Controlled Oxidation
Fenton
Photo-Fenton
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/60413
Acceder
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network_name_str CONICET Digital (CONICET)
spelling Purification and functionalization of carbon nanotubes by classical and advanced oxidation processesEscobar, Mariano MartinGoyanes, Silvia NairCorcuera, M. A.Eceiza, A.Mondragon, I.Rubiolo, Gerardo HectorCandal, Roberto JorgeCarbon NanotubesControlled OxidationFentonPhoto-FentonAdvanced oxidation technologies (AOT) were applied for the production of accurately controlled oxidized multi-walled carbon nanotubes. Fenton process is effective to get carboxylic (-COO - or -COOH) and OH groups on the surface of carbon nanotubes while Photofenton and UV/H 2O 2 processes mostly produce OH groups on surface of multiwalled carbon nanotubes (MWCNT). All of them preserve the structure of MWCNT allowing to achieve accurately controlled oxidized MWCNT. Fourier transform infrared spectroscopy (FTIR) and thermogravimetical analysis (TGA) show that the acid treatment is the more efficient technique to generate COOH groups on MWCNT surface. However, this chemical technique generates strong damages on the MWCNT structure, as demonstrated by TGA, field emission scanning electron microscopy and transmission electron microscopy results. Copyright © 2009 American Scientific Publishers.Fil: Escobar, Mariano Martin. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina. Universidad de Buenos Aires; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Ciudad Universitaria. Instituto de Física de Buenos Aires. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales. Instituto de Física de Buenos Aires; ArgentinaFil: Goyanes, Silvia Nair. Universidad de Buenos Aires; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Ciudad Universitaria. Instituto de Física de Buenos Aires. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales. Instituto de Física de Buenos Aires; ArgentinaFil: Corcuera, M. A.. Universidad del País Vasco; EspañaFil: Eceiza, A.. Universidad del País Vasco; EspañaFil: Mondragon, I.. Universidad del País Vasco; EspañaFil: Rubiolo, Gerardo Hector. Comisión Nacional de Energía Atómica; Argentina. Universidad de Buenos Aires; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Ciudad Universitaria. Instituto de Física de Buenos Aires. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales. Instituto de Física de Buenos Aires; ArgentinaFil: Candal, Roberto Jorge. Universidad Nacional de San Martín; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas; ArgentinaAmerican Scientific Publishers2009-12info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfapplication/pdfapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/60413Escobar, Mariano Martin; Goyanes, Silvia Nair; Corcuera, M. A.; Eceiza, A.; Mondragon, I.; et al.; Purification and functionalization of carbon nanotubes by classical and advanced oxidation processes; American Scientific Publishers; Journal of Nanoscience and Nanotechnology; 9; 10; 12-2009; 6228-62331533-4880CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/doi/10.1166/jnn.2009.1563info:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-sa/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-10-22T12:09:54Zoai:ri.conicet.gov.ar:11336/60413instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-10-22 12:09:55.251CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Purification and functionalization of carbon nanotubes by classical and advanced oxidation processes
title Purification and functionalization of carbon nanotubes by classical and advanced oxidation processes
spellingShingle Purification and functionalization of carbon nanotubes by classical and advanced oxidation processes
Escobar, Mariano Martin
Carbon Nanotubes
Controlled Oxidation
Fenton
Photo-Fenton
title_short Purification and functionalization of carbon nanotubes by classical and advanced oxidation processes
title_full Purification and functionalization of carbon nanotubes by classical and advanced oxidation processes
title_fullStr Purification and functionalization of carbon nanotubes by classical and advanced oxidation processes
title_full_unstemmed Purification and functionalization of carbon nanotubes by classical and advanced oxidation processes
title_sort Purification and functionalization of carbon nanotubes by classical and advanced oxidation processes
dc.creator.none.fl_str_mv Escobar, Mariano Martin
Goyanes, Silvia Nair
Corcuera, M. A.
Eceiza, A.
Mondragon, I.
Rubiolo, Gerardo Hector
Candal, Roberto Jorge
author Escobar, Mariano Martin
author_facet Escobar, Mariano Martin
Goyanes, Silvia Nair
Corcuera, M. A.
Eceiza, A.
Mondragon, I.
Rubiolo, Gerardo Hector
Candal, Roberto Jorge
author_role author
author2 Goyanes, Silvia Nair
Corcuera, M. A.
Eceiza, A.
Mondragon, I.
Rubiolo, Gerardo Hector
Candal, Roberto Jorge
author2_role author
author
author
author
author
author
dc.subject.none.fl_str_mv Carbon Nanotubes
Controlled Oxidation
Fenton
Photo-Fenton
topic Carbon Nanotubes
Controlled Oxidation
Fenton
Photo-Fenton
dc.description.none.fl_txt_mv Advanced oxidation technologies (AOT) were applied for the production of accurately controlled oxidized multi-walled carbon nanotubes. Fenton process is effective to get carboxylic (-COO - or -COOH) and OH groups on the surface of carbon nanotubes while Photofenton and UV/H 2O 2 processes mostly produce OH groups on surface of multiwalled carbon nanotubes (MWCNT). All of them preserve the structure of MWCNT allowing to achieve accurately controlled oxidized MWCNT. Fourier transform infrared spectroscopy (FTIR) and thermogravimetical analysis (TGA) show that the acid treatment is the more efficient technique to generate COOH groups on MWCNT surface. However, this chemical technique generates strong damages on the MWCNT structure, as demonstrated by TGA, field emission scanning electron microscopy and transmission electron microscopy results. Copyright © 2009 American Scientific Publishers.
Fil: Escobar, Mariano Martin. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina. Universidad de Buenos Aires; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Ciudad Universitaria. Instituto de Física de Buenos Aires. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales. Instituto de Física de Buenos Aires; Argentina
Fil: Goyanes, Silvia Nair. Universidad de Buenos Aires; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Ciudad Universitaria. Instituto de Física de Buenos Aires. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales. Instituto de Física de Buenos Aires; Argentina
Fil: Corcuera, M. A.. Universidad del País Vasco; España
Fil: Eceiza, A.. Universidad del País Vasco; España
Fil: Mondragon, I.. Universidad del País Vasco; España
Fil: Rubiolo, Gerardo Hector. Comisión Nacional de Energía Atómica; Argentina. Universidad de Buenos Aires; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Ciudad Universitaria. Instituto de Física de Buenos Aires. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales. Instituto de Física de Buenos Aires; Argentina
Fil: Candal, Roberto Jorge. Universidad Nacional de San Martín; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina
description Advanced oxidation technologies (AOT) were applied for the production of accurately controlled oxidized multi-walled carbon nanotubes. Fenton process is effective to get carboxylic (-COO - or -COOH) and OH groups on the surface of carbon nanotubes while Photofenton and UV/H 2O 2 processes mostly produce OH groups on surface of multiwalled carbon nanotubes (MWCNT). All of them preserve the structure of MWCNT allowing to achieve accurately controlled oxidized MWCNT. Fourier transform infrared spectroscopy (FTIR) and thermogravimetical analysis (TGA) show that the acid treatment is the more efficient technique to generate COOH groups on MWCNT surface. However, this chemical technique generates strong damages on the MWCNT structure, as demonstrated by TGA, field emission scanning electron microscopy and transmission electron microscopy results. Copyright © 2009 American Scientific Publishers.
publishDate 2009
dc.date.none.fl_str_mv 2009-12
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/60413
Escobar, Mariano Martin; Goyanes, Silvia Nair; Corcuera, M. A.; Eceiza, A.; Mondragon, I.; et al.; Purification and functionalization of carbon nanotubes by classical and advanced oxidation processes; American Scientific Publishers; Journal of Nanoscience and Nanotechnology; 9; 10; 12-2009; 6228-6233
1533-4880
CONICET Digital
CONICET
url http://hdl.handle.net/11336/60413
identifier_str_mv Escobar, Mariano Martin; Goyanes, Silvia Nair; Corcuera, M. A.; Eceiza, A.; Mondragon, I.; et al.; Purification and functionalization of carbon nanotubes by classical and advanced oxidation processes; American Scientific Publishers; Journal of Nanoscience and Nanotechnology; 9; 10; 12-2009; 6228-6233
1533-4880
CONICET Digital
CONICET
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/doi/10.1166/jnn.2009.1563
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
application/pdf
application/pdf
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dc.publisher.none.fl_str_mv American Scientific Publishers
publisher.none.fl_str_mv American Scientific Publishers
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
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instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
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