Fast microwave synthesis of Pt-MFI zeolite coatings on silicon micromonoliths: Application to VOC catalytic combustion

Autores
Marin, Ingrid; Adrover, María Esperanza; Vega,Didac; Urbiztondo, Miguel; Pina, Maria Pilar; Mallada, Reyes; Santamaría, Jesús
Año de publicación
2012
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
This paper describes the preparation of a ZSM-5 zeolite layer onto conventional Si wafers and Si micromonoliths, by using microwave-assisted seeded hydrothermal synthesis. A homogeneous ZSM-5 zeolite layer up to 680 nm was obtained over the external surface of a Si micromonolith (surface to volume ratio >300,000 m-1) after only 4 min of hydrothermal synthesis at 453 K. As a proof of concept, the catalytic activity of the prepared ZSM-5 coated micromonoliths, after a conventional Pt ion-exchange process, was demonstrated in the combustion of traces of n-hexane (200 ppmV) in air.
Fil: Marin, Ingrid. Universidad de Zaragoza. Instituto de Nanociencia de Aragón; España
Fil: Adrover, María Esperanza. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Bahía Blanca. Planta Piloto de Ingeniería Química. Universidad Nacional del Sur. Planta Piloto de Ingeniería Química; Argentina
Fil: Vega,Didac. Universidad Politecnica de Catalunya; España
Fil: Urbiztondo, Miguel. Centro Universitario de la Defensa (cud); España
Fil: Pina, Maria Pilar. Universidad de Zaragoza. Instituto de Nanociencia de Aragón; España
Fil: Mallada, Reyes. Universidad de Zaragoza. Instituto de Nanociencia de Aragón; España
Fil: Santamaría, Jesús. Universidad de Zaragoza. Instituto de Nanociencia de Aragón; España
Materia
Mfi
Microreactor
Microwave Synthesis
Voc Combustion
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/53507
Acceder
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oai_identifier_str oai:ri.conicet.gov.ar:11336/53507
network_acronym_str CONICETDig
repository_id_str 3498
network_name_str CONICET Digital (CONICET)
spelling Fast microwave synthesis of Pt-MFI zeolite coatings on silicon micromonoliths: Application to VOC catalytic combustionMarin, IngridAdrover, María EsperanzaVega,DidacUrbiztondo, MiguelPina, Maria PilarMallada, ReyesSantamaría, JesúsMfiMicroreactorMicrowave SynthesisVoc Combustionhttps://purl.org/becyt/ford/2.4https://purl.org/becyt/ford/2This paper describes the preparation of a ZSM-5 zeolite layer onto conventional Si wafers and Si micromonoliths, by using microwave-assisted seeded hydrothermal synthesis. A homogeneous ZSM-5 zeolite layer up to 680 nm was obtained over the external surface of a Si micromonolith (surface to volume ratio >300,000 m-1) after only 4 min of hydrothermal synthesis at 453 K. As a proof of concept, the catalytic activity of the prepared ZSM-5 coated micromonoliths, after a conventional Pt ion-exchange process, was demonstrated in the combustion of traces of n-hexane (200 ppmV) in air.Fil: Marin, Ingrid. Universidad de Zaragoza. Instituto de Nanociencia de Aragón; EspañaFil: Adrover, María Esperanza. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Bahía Blanca. Planta Piloto de Ingeniería Química. Universidad Nacional del Sur. Planta Piloto de Ingeniería Química; ArgentinaFil: Vega,Didac. Universidad Politecnica de Catalunya; EspañaFil: Urbiztondo, Miguel. Centro Universitario de la Defensa (cud); EspañaFil: Pina, Maria Pilar. Universidad de Zaragoza. Instituto de Nanociencia de Aragón; EspañaFil: Mallada, Reyes. Universidad de Zaragoza. Instituto de Nanociencia de Aragón; EspañaFil: Santamaría, Jesús. Universidad de Zaragoza. Instituto de Nanociencia de Aragón; EspañaDe Gruyter2012-04info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/53507Marin, Ingrid; Adrover, María Esperanza; Vega,Didac; Urbiztondo, Miguel; Pina, Maria Pilar; et al.; Fast microwave synthesis of Pt-MFI zeolite coatings on silicon micromonoliths: Application to VOC catalytic combustion; De Gruyter; Green Processing and Synthesis; 1; 2; 4-2012; 169-1742191-95422191-9550CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/doi/10.1515/gps-2012-0006info:eu-repo/semantics/altIdentifier/url/https://www.degruyter.com/view/j/gps.2012.1.issue-2/gps-2012-0006/gps-2012-0006.xmlinfo:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-nd/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-11-12T09:49:46Zoai:ri.conicet.gov.ar:11336/53507instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-11-12 09:49:46.936CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv Fast microwave synthesis of Pt-MFI zeolite coatings on silicon micromonoliths: Application to VOC catalytic combustion
title Fast microwave synthesis of Pt-MFI zeolite coatings on silicon micromonoliths: Application to VOC catalytic combustion
spellingShingle Fast microwave synthesis of Pt-MFI zeolite coatings on silicon micromonoliths: Application to VOC catalytic combustion
Marin, Ingrid
Mfi
Microreactor
Microwave Synthesis
Voc Combustion
title_short Fast microwave synthesis of Pt-MFI zeolite coatings on silicon micromonoliths: Application to VOC catalytic combustion
title_full Fast microwave synthesis of Pt-MFI zeolite coatings on silicon micromonoliths: Application to VOC catalytic combustion
title_fullStr Fast microwave synthesis of Pt-MFI zeolite coatings on silicon micromonoliths: Application to VOC catalytic combustion
title_full_unstemmed Fast microwave synthesis of Pt-MFI zeolite coatings on silicon micromonoliths: Application to VOC catalytic combustion
title_sort Fast microwave synthesis of Pt-MFI zeolite coatings on silicon micromonoliths: Application to VOC catalytic combustion
dc.creator.none.fl_str_mv Marin, Ingrid
Adrover, María Esperanza
Vega,Didac
Urbiztondo, Miguel
Pina, Maria Pilar
Mallada, Reyes
Santamaría, Jesús
author Marin, Ingrid
author_facet Marin, Ingrid
Adrover, María Esperanza
Vega,Didac
Urbiztondo, Miguel
Pina, Maria Pilar
Mallada, Reyes
Santamaría, Jesús
author_role author
author2 Adrover, María Esperanza
Vega,Didac
Urbiztondo, Miguel
Pina, Maria Pilar
Mallada, Reyes
Santamaría, Jesús
author2_role author
author
author
author
author
author
dc.subject.none.fl_str_mv Mfi
Microreactor
Microwave Synthesis
Voc Combustion
topic Mfi
Microreactor
Microwave Synthesis
Voc Combustion
purl_subject.fl_str_mv https://purl.org/becyt/ford/2.4
https://purl.org/becyt/ford/2
dc.description.none.fl_txt_mv This paper describes the preparation of a ZSM-5 zeolite layer onto conventional Si wafers and Si micromonoliths, by using microwave-assisted seeded hydrothermal synthesis. A homogeneous ZSM-5 zeolite layer up to 680 nm was obtained over the external surface of a Si micromonolith (surface to volume ratio >300,000 m-1) after only 4 min of hydrothermal synthesis at 453 K. As a proof of concept, the catalytic activity of the prepared ZSM-5 coated micromonoliths, after a conventional Pt ion-exchange process, was demonstrated in the combustion of traces of n-hexane (200 ppmV) in air.
Fil: Marin, Ingrid. Universidad de Zaragoza. Instituto de Nanociencia de Aragón; España
Fil: Adrover, María Esperanza. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Bahía Blanca. Planta Piloto de Ingeniería Química. Universidad Nacional del Sur. Planta Piloto de Ingeniería Química; Argentina
Fil: Vega,Didac. Universidad Politecnica de Catalunya; España
Fil: Urbiztondo, Miguel. Centro Universitario de la Defensa (cud); España
Fil: Pina, Maria Pilar. Universidad de Zaragoza. Instituto de Nanociencia de Aragón; España
Fil: Mallada, Reyes. Universidad de Zaragoza. Instituto de Nanociencia de Aragón; España
Fil: Santamaría, Jesús. Universidad de Zaragoza. Instituto de Nanociencia de Aragón; España
description This paper describes the preparation of a ZSM-5 zeolite layer onto conventional Si wafers and Si micromonoliths, by using microwave-assisted seeded hydrothermal synthesis. A homogeneous ZSM-5 zeolite layer up to 680 nm was obtained over the external surface of a Si micromonolith (surface to volume ratio >300,000 m-1) after only 4 min of hydrothermal synthesis at 453 K. As a proof of concept, the catalytic activity of the prepared ZSM-5 coated micromonoliths, after a conventional Pt ion-exchange process, was demonstrated in the combustion of traces of n-hexane (200 ppmV) in air.
publishDate 2012
dc.date.none.fl_str_mv 2012-04
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/53507
Marin, Ingrid; Adrover, María Esperanza; Vega,Didac; Urbiztondo, Miguel; Pina, Maria Pilar; et al.; Fast microwave synthesis of Pt-MFI zeolite coatings on silicon micromonoliths: Application to VOC catalytic combustion; De Gruyter; Green Processing and Synthesis; 1; 2; 4-2012; 169-174
2191-9542
2191-9550
CONICET Digital
CONICET
url http://hdl.handle.net/11336/53507
identifier_str_mv Marin, Ingrid; Adrover, María Esperanza; Vega,Didac; Urbiztondo, Miguel; Pina, Maria Pilar; et al.; Fast microwave synthesis of Pt-MFI zeolite coatings on silicon micromonoliths: Application to VOC catalytic combustion; De Gruyter; Green Processing and Synthesis; 1; 2; 4-2012; 169-174
2191-9542
2191-9550
CONICET Digital
CONICET
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/doi/10.1515/gps-2012-0006
info:eu-repo/semantics/altIdentifier/url/https://www.degruyter.com/view/j/gps.2012.1.issue-2/gps-2012-0006/gps-2012-0006.xml
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
dc.publisher.none.fl_str_mv De Gruyter
publisher.none.fl_str_mv De Gruyter
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
_version_ 1848598087111540736
score 12.976206

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