PVD TiN and CrN Coated Austempered Ductile Iron: Analysis of Processing Parameters Influence on Coating Characteristics and Substrate Microstructure

Autores
Colombo, Diego Alejandro; Echeverría, María Dolores; Moncada, Osvaldo Julio; Massone, Juan Miguel
Año de publicación
2012
Idioma
inglés
Tipo de recurso
artículo
Estado
versión publicada
Descripción
This work studies the influence of the PVD processing parameters on the characteristics of TiN and CrN coatings deposited on ADI substrates, austempered at 360ºC, with different nodule counts and surface roughnesses. Coatings were applied by arc ion plating using an industrial reactor and different sets of parameters, with BIAS voltages, arc currents, chamber pressures and substrate temperatures varying from -100 to -250 V, 60 to 65 A, 0.7 to 2.8 Pa and 280 to 450ºC, respectively. The effect of the different depositions conditions on the substrates microstructure was also analyzed. The existing phases, preferred orientation, surface topography, film thickness, hardness and adhesion of each coating were determined. The retained austenite content and hardness of each substrate were computed before and after coating deposition.The results obtained indicate that the different deposition conditions and coating materials evaluated do not generate significant changes neither in the resulting topography nor in the coating adhesion, which can be related to indices between HF1 and HF2. Coating adhesion was not affected by different substrate roughnesses. The combined reduction of BIAS voltage, arc current and chamber pressure leads to a decrease of TiN growth rate and hardness, while high substrate temperatures promotes an increase in TiN and CrN growth rates. Substrate temperatures around 300ºC with deposition times of up to 240 min do not promote noticeable changes on the ausferritic microstructure,while temperatures of 400ºC and above translate into a clear microstructural deterioration, even for short deposition times.
Fil: Colombo, Diego Alejandro. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina. Universidad Nacional de Mar del Plata. Facultad de Ingeniería; Argentina
Fil: Echeverría, María Dolores. Universidad Nacional de Mar del Plata. Facultad de Ingeniería; Argentina
Fil: Moncada, Osvaldo Julio. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina. Universidad Nacional de Mar del Plata. Facultad de Ingeniería; Argentina
Fil: Massone, Juan Miguel. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
Materia
AUSTEMPERED DUCTILE IRON
TiN
CrN
PVD PROCESSING PARAMETERS
Nivel de accesibilidad
acceso abierto
Condiciones de uso
https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
Repositorio
CONICET Digital (CONICET)
Institución
Consejo Nacional de Investigaciones Científicas y Técnicas
OAI Identificador
oai:ri.conicet.gov.ar:11336/275042
Acceder
id CONICETDig_0b34f26d57d8d8d1ccced471d69c88ba
oai_identifier_str oai:ri.conicet.gov.ar:11336/275042
network_acronym_str CONICETDig
repository_id_str 3498
network_name_str CONICET Digital (CONICET)
spelling PVD TiN and CrN Coated Austempered Ductile Iron: Analysis of Processing Parameters Influence on Coating Characteristics and Substrate MicrostructureColombo, Diego AlejandroEcheverría, María DoloresMoncada, Osvaldo JulioMassone, Juan MiguelAUSTEMPERED DUCTILE IRONTiNCrNPVD PROCESSING PARAMETERShttps://purl.org/becyt/ford/2.5https://purl.org/becyt/ford/2This work studies the influence of the PVD processing parameters on the characteristics of TiN and CrN coatings deposited on ADI substrates, austempered at 360ºC, with different nodule counts and surface roughnesses. Coatings were applied by arc ion plating using an industrial reactor and different sets of parameters, with BIAS voltages, arc currents, chamber pressures and substrate temperatures varying from -100 to -250 V, 60 to 65 A, 0.7 to 2.8 Pa and 280 to 450ºC, respectively. The effect of the different depositions conditions on the substrates microstructure was also analyzed. The existing phases, preferred orientation, surface topography, film thickness, hardness and adhesion of each coating were determined. The retained austenite content and hardness of each substrate were computed before and after coating deposition.The results obtained indicate that the different deposition conditions and coating materials evaluated do not generate significant changes neither in the resulting topography nor in the coating adhesion, which can be related to indices between HF1 and HF2. Coating adhesion was not affected by different substrate roughnesses. The combined reduction of BIAS voltage, arc current and chamber pressure leads to a decrease of TiN growth rate and hardness, while high substrate temperatures promotes an increase in TiN and CrN growth rates. Substrate temperatures around 300ºC with deposition times of up to 240 min do not promote noticeable changes on the ausferritic microstructure,while temperatures of 400ºC and above translate into a clear microstructural deterioration, even for short deposition times.Fil: Colombo, Diego Alejandro. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina. Universidad Nacional de Mar del Plata. Facultad de Ingeniería; ArgentinaFil: Echeverría, María Dolores. Universidad Nacional de Mar del Plata. Facultad de Ingeniería; ArgentinaFil: Moncada, Osvaldo Julio. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina. Universidad Nacional de Mar del Plata. Facultad de Ingeniería; ArgentinaFil: Massone, Juan Miguel. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; ArgentinaIron Steel Inst Japan Keidanren Kaikan2012-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfapplication/pdfhttp://hdl.handle.net/11336/275042Colombo, Diego Alejandro; Echeverría, María Dolores; Moncada, Osvaldo Julio; Massone, Juan Miguel; PVD TiN and CrN Coated Austempered Ductile Iron: Analysis of Processing Parameters Influence on Coating Characteristics and Substrate Microstructure; Iron Steel Inst Japan Keidanren Kaikan; ISIJ International; 52; 1; 1-2012; 121-1260915-1559CONICET DigitalCONICETenginfo:eu-repo/semantics/altIdentifier/url/https://www.jstage.jst.go.jp/article/isijinternational/52/1/52_1_121/_articleinfo:eu-repo/semantics/altIdentifier/doi/10.2355/isijinternational.52.121info:eu-repo/semantics/openAccesshttps://creativecommons.org/licenses/by-nc-nd/2.5/ar/reponame:CONICET Digital (CONICET)instname:Consejo Nacional de Investigaciones Científicas y Técnicas2025-12-03T08:42:15Zoai:ri.conicet.gov.ar:11336/275042instacron:CONICETInstitucionalhttp://ri.conicet.gov.ar/Organismo científico-tecnológicoNo correspondehttp://ri.conicet.gov.ar/oai/requestdasensio@conicet.gov.ar; lcarlino@conicet.gov.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:34982025-12-03 08:42:15.434CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicasfalse
dc.title.none.fl_str_mv PVD TiN and CrN Coated Austempered Ductile Iron: Analysis of Processing Parameters Influence on Coating Characteristics and Substrate Microstructure
title PVD TiN and CrN Coated Austempered Ductile Iron: Analysis of Processing Parameters Influence on Coating Characteristics and Substrate Microstructure
spellingShingle PVD TiN and CrN Coated Austempered Ductile Iron: Analysis of Processing Parameters Influence on Coating Characteristics and Substrate Microstructure
Colombo, Diego Alejandro
AUSTEMPERED DUCTILE IRON
TiN
CrN
PVD PROCESSING PARAMETERS
title_short PVD TiN and CrN Coated Austempered Ductile Iron: Analysis of Processing Parameters Influence on Coating Characteristics and Substrate Microstructure
title_full PVD TiN and CrN Coated Austempered Ductile Iron: Analysis of Processing Parameters Influence on Coating Characteristics and Substrate Microstructure
title_fullStr PVD TiN and CrN Coated Austempered Ductile Iron: Analysis of Processing Parameters Influence on Coating Characteristics and Substrate Microstructure
title_full_unstemmed PVD TiN and CrN Coated Austempered Ductile Iron: Analysis of Processing Parameters Influence on Coating Characteristics and Substrate Microstructure
title_sort PVD TiN and CrN Coated Austempered Ductile Iron: Analysis of Processing Parameters Influence on Coating Characteristics and Substrate Microstructure
dc.creator.none.fl_str_mv Colombo, Diego Alejandro
Echeverría, María Dolores
Moncada, Osvaldo Julio
Massone, Juan Miguel
author Colombo, Diego Alejandro
author_facet Colombo, Diego Alejandro
Echeverría, María Dolores
Moncada, Osvaldo Julio
Massone, Juan Miguel
author_role author
author2 Echeverría, María Dolores
Moncada, Osvaldo Julio
Massone, Juan Miguel
author2_role author
author
author
dc.subject.none.fl_str_mv AUSTEMPERED DUCTILE IRON
TiN
CrN
PVD PROCESSING PARAMETERS
topic AUSTEMPERED DUCTILE IRON
TiN
CrN
PVD PROCESSING PARAMETERS
purl_subject.fl_str_mv https://purl.org/becyt/ford/2.5
https://purl.org/becyt/ford/2
dc.description.none.fl_txt_mv This work studies the influence of the PVD processing parameters on the characteristics of TiN and CrN coatings deposited on ADI substrates, austempered at 360ºC, with different nodule counts and surface roughnesses. Coatings were applied by arc ion plating using an industrial reactor and different sets of parameters, with BIAS voltages, arc currents, chamber pressures and substrate temperatures varying from -100 to -250 V, 60 to 65 A, 0.7 to 2.8 Pa and 280 to 450ºC, respectively. The effect of the different depositions conditions on the substrates microstructure was also analyzed. The existing phases, preferred orientation, surface topography, film thickness, hardness and adhesion of each coating were determined. The retained austenite content and hardness of each substrate were computed before and after coating deposition.The results obtained indicate that the different deposition conditions and coating materials evaluated do not generate significant changes neither in the resulting topography nor in the coating adhesion, which can be related to indices between HF1 and HF2. Coating adhesion was not affected by different substrate roughnesses. The combined reduction of BIAS voltage, arc current and chamber pressure leads to a decrease of TiN growth rate and hardness, while high substrate temperatures promotes an increase in TiN and CrN growth rates. Substrate temperatures around 300ºC with deposition times of up to 240 min do not promote noticeable changes on the ausferritic microstructure,while temperatures of 400ºC and above translate into a clear microstructural deterioration, even for short deposition times.
Fil: Colombo, Diego Alejandro. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina. Universidad Nacional de Mar del Plata. Facultad de Ingeniería; Argentina
Fil: Echeverría, María Dolores. Universidad Nacional de Mar del Plata. Facultad de Ingeniería; Argentina
Fil: Moncada, Osvaldo Julio. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina. Universidad Nacional de Mar del Plata. Facultad de Ingeniería; Argentina
Fil: Massone, Juan Miguel. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentina
description This work studies the influence of the PVD processing parameters on the characteristics of TiN and CrN coatings deposited on ADI substrates, austempered at 360ºC, with different nodule counts and surface roughnesses. Coatings were applied by arc ion plating using an industrial reactor and different sets of parameters, with BIAS voltages, arc currents, chamber pressures and substrate temperatures varying from -100 to -250 V, 60 to 65 A, 0.7 to 2.8 Pa and 280 to 450ºC, respectively. The effect of the different depositions conditions on the substrates microstructure was also analyzed. The existing phases, preferred orientation, surface topography, film thickness, hardness and adhesion of each coating were determined. The retained austenite content and hardness of each substrate were computed before and after coating deposition.The results obtained indicate that the different deposition conditions and coating materials evaluated do not generate significant changes neither in the resulting topography nor in the coating adhesion, which can be related to indices between HF1 and HF2. Coating adhesion was not affected by different substrate roughnesses. The combined reduction of BIAS voltage, arc current and chamber pressure leads to a decrease of TiN growth rate and hardness, while high substrate temperatures promotes an increase in TiN and CrN growth rates. Substrate temperatures around 300ºC with deposition times of up to 240 min do not promote noticeable changes on the ausferritic microstructure,while temperatures of 400ºC and above translate into a clear microstructural deterioration, even for short deposition times.
publishDate 2012
dc.date.none.fl_str_mv 2012-01
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/resource_type/c_6501
info:ar-repo/semantics/articulo
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/11336/275042
Colombo, Diego Alejandro; Echeverría, María Dolores; Moncada, Osvaldo Julio; Massone, Juan Miguel; PVD TiN and CrN Coated Austempered Ductile Iron: Analysis of Processing Parameters Influence on Coating Characteristics and Substrate Microstructure; Iron Steel Inst Japan Keidanren Kaikan; ISIJ International; 52; 1; 1-2012; 121-126
0915-1559
CONICET Digital
CONICET
url http://hdl.handle.net/11336/275042
identifier_str_mv Colombo, Diego Alejandro; Echeverría, María Dolores; Moncada, Osvaldo Julio; Massone, Juan Miguel; PVD TiN and CrN Coated Austempered Ductile Iron: Analysis of Processing Parameters Influence on Coating Characteristics and Substrate Microstructure; Iron Steel Inst Japan Keidanren Kaikan; ISIJ International; 52; 1; 1-2012; 121-126
0915-1559
CONICET Digital
CONICET
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/url/https://www.jstage.jst.go.jp/article/isijinternational/52/1/52_1_121/_article
info:eu-repo/semantics/altIdentifier/doi/10.2355/isijinternational.52.121
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
eu_rights_str_mv openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
dc.format.none.fl_str_mv application/pdf
application/pdf
application/pdf
dc.publisher.none.fl_str_mv Iron Steel Inst Japan Keidanren Kaikan
publisher.none.fl_str_mv Iron Steel Inst Japan Keidanren Kaikan
dc.source.none.fl_str_mv reponame:CONICET Digital (CONICET)
instname:Consejo Nacional de Investigaciones Científicas y Técnicas
reponame_str CONICET Digital (CONICET)
collection CONICET Digital (CONICET)
instname_str Consejo Nacional de Investigaciones Científicas y Técnicas
repository.name.fl_str_mv CONICET Digital (CONICET) - Consejo Nacional de Investigaciones Científicas y Técnicas
repository.mail.fl_str_mv dasensio@conicet.gov.ar; lcarlino@conicet.gov.ar
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score 12.913667

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